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Magnetic, granulometric and geochemical analyses were conducted on an intertidal sediment core from the Yangtze Estuary to evaluate the possibility of normalizing samples for particle size effects in a heavy metal pollution study by means of magnetic proxies. It has been found that the magnetic parameter XARM, indicating fine grained ferrimagnetic minerals, correlates well with the clay content and organic matter concentration of the sediments. XARM also shows significant relationship with heavy metals. Therefore XARM is proposed as a proxy for clay content in the sediments, and can be used to compensate for the particle size effect in sedimentary heavy metal records, where magnetic minerals are not subject to significant post-depositional alteration. 相似文献
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Shell Filling and Spin Effects in a Few Electron Quantum Dot 总被引:1,自引:0,他引:1
Tarucha S Austing DG Honda T van der Hage RJ Kouwenhoven LP 《Physical review letters》1996,77(17):3613-3616
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Summary Possible changes in chemical analysis as a result of the introduction of microprocessors are discussed. Many of the problems
associated with mini-computer systems for GC arise from putting too many facilities into small systems because of price constraints.
These should disappear with widespread use of microprocessors. The problems of inadequate or inappropriate software are a
little more intractable. However, the software industry has learnt a lot in the past decade and, while bad software continues
to be produced in some quantity, the tools to construct good programs are becoming readily available, and should give rise
to improved systems. 相似文献
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Ali HR Edwards HG Hargreaves MD Munshi T Scowen IJ Telford RJ 《Analytica chimica acta》2008,620(1-2):103-112
Knowledge and control of the polymorphic phases of chemical compounds are important aspects of drug development in the pharmaceutical industry. Salmeterol xinafoate, a long acting β-adrenergic receptor agonist, exists in two polymorphic Forms, I and II. Raman and near infrared spectra were obtained of these polymorphs at selected wavelengths in the range of 488–1064 nm; significant differences in the Raman and near-infrared spectra were apparent and key spectral marker bands have been identified for the vibrational spectroscopic characterisation of the individual polymorphs which were also characterised with X ray diffractometry. The solid-state transition of salmeterol xinafoate polymorphs was studied using simultaneous in situ portable Raman spectroscopy and differential scanning calorimetry isothermally between transitions. This method assisted in the unambiguous characterisation of the two polymorphic forms by providing a simultaneous probe of both the thermal and vibrational data. The study demonstrates the value of a rapid in situ analysis of a drug polymorph which can be of potential value for at-line in-process control. 相似文献