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101.
Bahia Abbas Moussa Hanaa M.A. Hashem Marianne Alphonse Mahrouse Sally Tarek Mahmoud 《Biomedical chromatography : BMC》2019,33(8)
Grapefruit juice inhibits esterase enzyme. Therefore, a possible interaction with ester prodrugs should be taken into consideration. In this study, the influence of grapefruit juice on sacubitril (SAC) rat liver S9 activation by esterase enzyme was evaluated. An RP‐HPLC method was developed and validated for estimation of SAC in rat liver S9 fraction using a C18 Cyano column as stationary phase and acetonitrile–sodium di‐hydrogen phosphate buffer (0.02 m , pH 4 adjusted by o‐phosphoric acid, 40:60, v/v), as mobile phase at a flow rate of 1 mL/min and UV detection at 254 nm. The method was successfully applied to an in vitro study in which SAC was incubated with rat liver S9 fraction prepared from rats that had previously ingested grapefruit juice for a week. The calculated SAC concentration after incubation was compared with that of SAC incubated with rat liver S9 fraction from the rat control group. The statistical significance between the results of test and control incubation sets was assessed. In conclusion, the current study demonstrated that grapefruit juice decreased SAC hydrolysis, hence delaying its activation to sacubitrilat (active form) in gut lumen. Based on this food–drug interaction, it may be required that grapefruit juice should be consumed with caution in patients receiving SAC. 相似文献
102.
Thiosemicarbazide copper (II) complexes; [Cu2(HL1)2(H2O)2Cl2].H2O (1) and [Cu2(HL2)2(H2O)2Cl2].2H2O (2) (where H2L1 = 2-picolinoyl-N-(pyridin-2-yl)hydrazine-1-carbothioamide and H2L2 = 2-(2-(2-aminothiazol-4-yl)acetyl)-N-(pyridin-2-yl)hydrazine-1-carbothioamide) have been synthesized and characterized. Analytical and spectroscopic data revealed that ligands behaves as monobasic tetradentate with octahedral geometry. In addition, the optimized geometry of the ligands and their complexes was approved with the Jaguar 9.1 program in the Schrödinger set using DFT (density functional theory) to predict chemical processes and to estimate the properties of the material made by the hybrid functional density system B3LYP. Furthermore, the thermal degradation curves of complexes were discussed in order to determine the kinetic and thermodynamic parameters by various approaches. Additionally, the antioxidant (using the DPPH and SOD methods) and the antibacterial potency of the compounds were examined. Also, docking study of ligands and their complexes was carried out against Staphylococcus aureus gram +ve, gram -ve bacterial strains of Escherichia coli and Candida albicans using the XP glide protocol of Schrödinger suite. 相似文献
103.
To study different functionalities of the PWR-900 MW(e) reactor core, an electronic model of Simulation Program with Integrated Circuit Enfesied (PSPICE) for electronic circuit design was adopted to model the mathematical models. A classical breadboard electronically simulates the physical terminal characteristics of each network. The electronic simulator, parity simulator, for reactor core can simulate six-delayed neutron groups, single prompt neutron, neutron source, fuel channel, the coolant, reactor poisons, temperature feedback, control rods, safety rods, and boron injection. Positive/negative step or sin reactivity functions are two case studies were analyzed. The obtained results were found to be in a good agreement with the available data of El-Dabaa PWR 900 MW(e) basic simulator. 相似文献
104.
This paper presents a new general method for solving the pressure-diffusion equation in cylindrically radial composite reservoirs, where the rock and fluid properties may change radially as a function ofr. Composite systems, such as formations with wellbore filtrate invasion and reservoirs with peripheral water encroachment, can be encountered as a result of drilling, secondary oil recovery, and water influx.The new solution method utilizes the reflection and transmission concept of electromagnetics to solve fluid flow problems in three-dimensional cylindrically radial reservoirs, where heterogeneity is in only one direction. The Green's function for a point source in a three-dimensional radially composite system is developed by using the reflection and transmission method. The method as well as the point source solution are sufficiently general that they may be applied to similar fluid flow and well testing problems involving single-phase flow. 相似文献
105.
Tarek Sayed Ahmed 《Mathematical Logic Quarterly》2006,52(1):106-112
SC, CA, QA and QEA denote the classes of Pinter's substitution algebras, Tarski's cylindric algebras, Halmos' quasi‐polyadic algebras and quasi‐polyadic equality algebras, respectively. Let ω ≤ α < β and let K ∈ {SC,CA,QA,QEA}. We show that the class of α ‐dimensional neat reducts of algebras in Kβ is not elementary. This solves a problem in [3]. Also our result generalizes results proved in [2] and [3]. (© 2006 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim) 相似文献
106.
M. Tarek M. Zaki M. H. Fawzy M. Mokhtar Assey 《Fresenius' Journal of Analytical Chemistry》1988,330(2):155-157
Summary Some tertiary amines and alkaloides were determined by reaction with methyl iodide at 43 °C. The produced quaternary ammonium iodide salts were potentiometrically titrated with standard silver nitrate solution using either the iodide or silver/sulfide ion-selective electrode. The effects of solvent, temperature and time of reaction were examined. An average recovery of 99.0% and 98.9% with standard deviations of 0.73 and 0.52 were obtained for the studied amines and alkaloides, respectively.
Verwendung der Iodid-bzw. Silber/Sulfid-selektiven Elektrode zur Bestimmung einiger tertiärer Amine und Alkaloide相似文献
107.
M. Tarek M. Zaki L. F. M. Esmail A. Y. El-Sayed 《Fresenius' Journal of Analytical Chemistry》1988,331(6):607-610
Summary Simple and highly sensitive fluorimetric methods for iron determination are described. The methods are based on quenching the fluorescence of an aqueous morin solution or zinc-morin-Triton X-100 ternary system. The fluorescence emission is measured at 500 and 503 nm (wavelength of excitation 420 and 433 nm) for morin and the ternary system, respectively. The quenching calibration graphs are linear over the range 0–250 and 0–55 ng Fe/ml and the iron detection limits are 20 and 5 ng/ml using morin and zinc-morin-Triton X-100 system, respectively. The influence of experimental variables such as pH, reagent and surfactant concentrations, temperature, standing time and diverse ions are studied to obtain the optimum conditions. The method has been applied to the determination of iron in aluminium metal.
Fluorimetrische Eisen(III)-bestimmung durch Luminescenzlöschung des Systems Zink-Morin-Triton X-100相似文献
108.
Fatimetou mint El Mounir 《Positivity》2007,11(3):485-495
We give here some characterizations for normality and nuclearity of convex cones. We obtain a sufficient condition for weakly
normal cone to be normal (respectively nuclear).
Work partially supported by FNARS, Project 003. 相似文献
109.
We construct a dual semigroup of kernels associated to a semidynamical system. The above semigroup is in duality with the deterministic semigroup defined by Koopmann. We also prove the existence of right dual process associated to a semidynamical system. 相似文献
110.
Chemical and Physical Analysis of Acetate-Oxide Sol-Gel Processing Routes for the Y-Ba-Cu-O System 总被引:2,自引:0,他引:2
Tarek?MouganieEmail author Michelle?A.?Moram Joy?Sumner Bartek?A.?Glowacki Bart?Schoofs Isabel?Van?Driessche Serge?Hoste 《Journal of Sol-Gel Science and Technology》2005,36(1):87-94
The formation of three sols by fluorine-free aqueous and non-aqueous processes were analyzed and modified to vary the chemical properties of the sols (inks) to suit a variety of deposition processes such as dip-coating and ink-jet coating/printing. Ink-jet printing requires high wetting angles; choosing the right complexing agents to modify the ink allows the formation of droplets with high wetting angles on the surface. Dip-coating and ink-jet coating require low wetting angles; additives added to the sols reduce wetting angles to 10∘ and allow complete coverage of the substrate surface. The deposition theories and requirements are briefly discussed, as are some initial tests with the printing and converting of the developed superconducting inks. 相似文献