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A highly selective and sensitive second-derivative spectrophotometric determination of iron is based on the extraction of the ferroin-perchlorate ion-association complex into mesityl oxide. A linear calibration graph is obtained for iron in the range 0.5-50 mug in 100 ml of original aqueous phase, with a detection limit of 2 ng/ml. The method is precise and reliable and has been applied to the determination of iron in high-purity rare-earth oxides. 相似文献
33.
S. Sukumar Pradeep Kumar Sharma P. Govindan R. V. Subba Rao 《Journal of Radioanalytical and Nuclear Chemistry》2013,295(1):191-196
Acetohydroxamic acid (AHA) based uranium product purification process to remove plutonium was optimized. For this process, equilibrium data was generated to optimize AHA concentration and acidity of stripping agent/scrubbing agent. Two options namely (i) Pu complexation in aqueous phase followed by extraction and scrubbing ii) extraction followed by scrubbing with AHA were studied. Results of these studies indicate that U product obtained in AHA purification is near to the table top specification and also quantitative Pu recovery from the AHA strip product is possible by oxalate precipitation. 相似文献
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Rhodamine‐B has been proposed as a simple and sensitive colorimetric reagent for the estimation of sulphur dioxide in air. The air sample containing sulphur dioxide is passed through the absorbing solution of aqueous potassium iodate and N‐chlorosuccinimide to liberate iodine. The liberated iodine bleaches the pinkish red coloured rhodamine‐B dye, which measured at 555 nm. Beer's law was obeyed in the range of 0.5–5.0 μg, of sulphite per 25 mL (0.02–0.2 ppm) equivalent to 0.4–4.0 μg of sulphur dioxide (0.016–0.16 ppm). The molar absorptivity and Sandell's sensitivity were found to be 4.56 × 105 l mol?1 cm?1 and 0.00017 μg cm?2, respectively. The method has been suitably modified and successfully applied to the determination of sulphites in water after liberation of sulphur dioxide in acidic medium. 相似文献
37.
Michael A. Beckett David E. Hibbs Michael B. Hursthouse K. M. Abdul Malik Paul Owen K. Sukumar Varma 《Journal of chemical crystallography》1998,28(4):277-281
The title compound crystallizes in the triclinic space group
, with a = 14.458(6), b = 14.630(5), c = 14.721(8) Å, = 79.75(2), = 80.11(3), = 80.50(3)°, and Z = 2. The crystal structure consists of molecules of (Ph3SiO)3B and Ph3SiOH linked by an weak B···(silanol) acceptor-donor bond, additionally stabilized by OH(silanol)···O(siloxy) hydrogen bonds. The average B–O, Si–O distances and B–O–Si angle are 1.369, 1.649 Å and 137.2°, respectively. 相似文献
38.
C22N2O5H32,M
r
=404.5, monoclinic,C2,a=21.781(5),b=5.065(1),c=22.333(4)Å,=112.81(2)°,V=2271.1(9)Å3,D
calc=1.148 g cm3, (CuK
)=1.5418 Å,=5.89 cm–1,F(000)=848, room temperature,R=0.058 for 2178 unique reflections [I2.5(I)]. The peptide linkage is in thetrans conformation. The molecule adopts the-sheet structure. The crystal structure is stabilized by a three-dimensional network of N-HO and C-HO hydrogen bonds.DCB Contribution No. 813. 相似文献
39.
Si-Jie Yu Sreenivas R. Sukumar Andreas F. Koschan David L. Page Mongi A. Abidi 《Optics and Lasers in Engineering》2007,45(7):808-818
In this paper, we present our experience in building a mobile imaging system that incorporates multi-modality sensors for road surface mapping and inspection applications. Our proposed system leverages 3D laser-range sensors, video cameras, global positioning systems (GPS) and inertial measurement units (IMU) towards the generation of photo-realistic, geometrically accurate, geo-referenced 3D models of road surfaces. Based on our summary of the state-of-the-art systems for a road distress survey, we identify several challenges in the real-time deployment, integration and visualization of the multi-sensor data. Then, we present our data acquisition and processing algorithms as a novel two-stage automation procedure that can meet the accuracy requirements with real-time performance. We provide algorithms for 3D surface reconstruction to process the raw data and deliver detail preserving 3D models that possess accurate depth information for characterization and visualization of cracks as a significant improvement over contemporary commercial video-based vision systems. 相似文献
40.
Sukumar Basuli 《Zeitschrift für Angewandte Mathematik und Physik (ZAMP)》1961,12(4):357-362
Zusammenfassung Es werden die grossen Deformationen einer Kreisplatte unter zentrischer Einzellast nach der Methode vonBerger ermittelt. 相似文献