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The ultrafast dynamics of polybutadiene have been studied using ultrafast optical-Kerr-effect spectroscopy. The data are compared with measurements on 1,3- and 1,4-pentadiene. The two diene derivatives have quite distinct subpicosecond dynamics, with an important contribution from an intramolecular torsional mode in the 1,4-derivative. The main part of the polymer spectral density can be assigned, by analogy with the data for 1,4-pentadiene, to intramolecular torsional motion about carbon–carbon single bonds. The picosecond diffusive orientational relaxation times of the dienes are not well described by simple hydrodynamics. 相似文献
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The assumption that the same universal scale of time applies for different physical laws depends uponthe hypothesis that there is a unique universal scale of time in the universe. Intrinsic to that hypothesis is the assumption that if extraneous factors that affect physical clocks and processes that run on different physical principles could be removed, all clocks are synchronizable with one another. The consequences of that hypothesis not being true are considered. It was found thatclock asynchrony implies that: (1) a mass variation theory is probable; (2) there is a need for multiple clocks; and (3) t in the equations of physics is referring to clocks rather than time such that the properties of time are reduced to its direction (as characterized by thermodynamics and cosmology). 相似文献
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Stephen P. Watson Richard D. Wilson Duncan B. Judd Stephen A. Richards 《Tetrahedron letters》1997,38(52):179-9068
The development of a novel solid phase synthesis of some 5-aminopyrazoles and derivatives is described. Reaction of hydrazines with solid supported β-keto-nitrile (1) affords 5-aminopyrazoles (2) the amino group of which is readily acylated or sulphonylated. Generation of the solid supported β-keto-nitrile (1) is non trivial and represents a key step in the overall synthesis. 相似文献
889.
Stephen F. Austin 《Journal of voice》1997,11(2):212-221
The present study addresses two questions: (a) Is the action and/orposture of the velopharyngeal valve conducive to allow significant resonance during Western tradition classical singing? (b) How do the actions of the velo-pharyngeal valve observed in this style of singing compare with normal speech? A photodetector system was used to observe the area function of the velopharyngeal port during speech and classical style singing. Identical speech samples were produced by each subject in a normal speaking voice and then in the low, medium, and high singing ranges. Results indicate that in these four singers the velopharyngeal port was closed significantly longer in singing than in speaking samples. The amount of time the velopharyngeal port was opened was greatest in speech and diminished as the singer ascended in pitch. In the high voice condition, little or no opening of the velopharyngeal port was measured. 相似文献
890.
We present a general modeling approach to crew rostering and its application to computer-assisted generation of rotation-based rosters (or rotas) at the London Underground. Our goals were flexibility, speed, and optimality, and our approach is unique in that it achieves all three. Flexibility was important because requirements at the Underground are evolving and because specialized approaches in the literature did not meet our flexibility-implied need to use standard solvers. We decompose crew rostering into stages that can each be solved with a standard commercial MILP solver. Using a 167 MHz Sun UltraSparc 1 and CPLEX 4.0 MILP solver, we obtained high-quality rosters in runtimes ranging from a few seconds to a few minutes within 2% of optimality. Input data were takes from different depots with crew sizes ranging from 30–150 drivers, i.e., with number of duties ranging from about 200–1000. Using an argument based on decomposition and aggregation, we prove the optimality of our approach for the overall crew rostering problem. 相似文献