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Maurice Dörr Sebastian Lips Prof. Dr. Carlos Alberto Martínez-Huitle Dr. Dieter Schollmeyer Prof. Dr. Robert Franke Prof. Dr. Siegfried R. Waldvogel 《Chemistry (Weinheim an der Bergstrasse, Germany)》2019,25(33):7835-7838
We report an innovative, sustainable and straightforward protocol for the synthesis of N,N-diarylamides equipped with nonprotected hydroxyl groups by using electrosynthesis. The concept allows the application of various substrates furnishing diarylamides with yields up to 57 % within a single and direct electrolytic protocol. The method is thereby easy to conduct in an undivided cell with constant current conditions offering a versatile and short-cut alternative to conventional pathways. 相似文献
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Perfluorocongressane was synthesized using elemental fluorine and characterized by mass spectra, (19)F NMR, and X-ray crystallography. 相似文献
65.
TXRF has been applied in combination with VPD to the analysis of trace impurities in the native oxide layer of Si wafer surfaces down to the range of 10(8) atoms. cm(-2). Proper quantification of VPD/TXRF data requires calibration with microdroplet standard reference wafers. The precision of calibration function has been evaluated and found to allow quantification at a high level of 3 sigma confidence with microdroplet standard reference. 相似文献
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Siegfried Steiner 《manuscripta mathematica》1985,52(1-3):21-35
It is well known (and rather trivial to prove) that the square F2 of a Finsler norm F:TM on a differentiable manifold M is differentiable at the zero section if and only if F is the norm function of a Riemannian metric. However, the corresponding question for a general p-areal on M is far less trivial to settle and leads to interesting algebraic and combinatorial problems concerning multiquadratic forms. For p=2, the results are closely related to known properties of the curvature tensor of a Riemannian metric. 相似文献
68.
We consider a class of elliptic inclusions under Dirichlet boundary conditions involving multifunctions of Clarke's generalized gradient. Under conditions given in terms of the first eigenvalue as well as the Fu?ik spectrum of the p ‐Laplacian we prove the existence of a positive, a negative and a sign‐changing solution. Our approach is based on variational methods for nonsmooth functionals (nonsmooth critical point theory, second deformation lemma), and comparison principles for multivalued elliptic problems. In particular, the existence of extremal constant‐sign solutions plays a key role in the proof of sign‐changing solutions (© 2010 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim) 相似文献
69.
Siegfried Cools Bram Reps Wim Vanroose 《Numerical Linear Algebra with Applications》2014,21(4):513-533
In this paper, we construct and analyze a level‐dependent coarse grid correction scheme for indefinite Helmholtz problems. This adapted multigrid (MG) method is capable of solving the Helmholtz equation on the finest grid using a series of MG cycles with a grid‐dependent complex shift, leading to a stable correction scheme on all levels. It is rigorously shown that the adaptation of the complex shift throughout the MG cycle maintains the functionality of the two‐grid correction scheme, as no smooth modes are amplified in or added to the error. In addition, a sufficiently smoothing relaxation scheme should be applied to ensure damping of the oscillatory error components. Numerical experiments on various benchmark problems show the method to be competitive with or even outperform the current state‐of‐the‐art MG‐preconditioned Krylov methods, for example, complex shifted Laplacian preconditioned flexible GMRES. Copyright © 2013 John Wiley & Sons, Ltd. 相似文献
70.
Qamrul Hasan Ansari Siegfried Schaible Jen-Chih Yao 《Journal of Global Optimization》2002,22(1-4):3-16
In this paper, we introduce the system of generalized vector equilibrium problems which includes as special cases the system of generalized implicit vector variational inequality problems, the system of generalized vector variational and variational-like inequality problems and the system of vector equilibrium problems. By using a maximal element theorem, we establish existence results for a solution of these systems. As an application, we derive existence results for a solution of a more general Nash equilibrium problem for vector-valued functions. 相似文献