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141.
T. Minamisono Y. Nojiri K. Matsuta T. Iwayama M. Fujinaga 《Hyperfine Interactions》1987,34(1-4):299-302
Hyperfine magnetic fields in a single crystal Fe were measured by use of asymmetric decay and NMR detection of spin polarized -emitting12N. 相似文献
142.
Shuntaro Mataka Kazufumi Takahashi Yukihiro Yamada Masashi Tashiro 《Journal of heterocyclic chemistry》1979,16(5):1009-1015
The reaction of sulfur nitride (1) with acetylenes (2a-m) was carried out in refluxing toluene to give 1,2,5-thiadiazoles (3a-m) as a major product. 相似文献
143.
M. Tanigaki M. Matsui M. Mihara M. Mori M. Tanaka T. Yanagisawa T. Ohtsubo T. Izumikawa A. Kitagawa M. Fukuda K. Matsuta Y. Nojiri T. Minamisono 《Hyperfine Interactions》1993,78(1-4):105-110
The magnetic moment of15O(I=1/2–,T
1/2=122 s) has been measured precisely by use of the -NMR detection of15O in TiO2 as, |(15O; 1/2–)|=0.71951 (12) µN. The effective nucleon mass in the nuclei around mass number 16 was discussed using the isoscalar moment deduced in connection with the magnetic moment of15N. 相似文献
144.
New determination of quadrupole coupling constants of Li isotopes in single crystals LiIO3 andLiNbO3
T. Minamisono T. Ohtsubo Y. Nakayama S. Fukuda T. Izumikawa M. Tanigaki M. Matsui S. Takeda N. Nakamura M. Fukuda K. Matsuta Y. Nojiri 《Hyperfine Interactions》1993,78(1-4):159-163
Quadrupole effects in NMR spectra of8Li(I
=2+;T
1/2=0.84 s) in LiIO3 andLiNbO3 single crystals have been detected by use of a modified -NMR. The coupling constants for both crystals are in agreement with known ones. Field gradients in the crystals were measured by detecting pulsed-Fourier transformed NMR of7Li. The quadrupole moments deduced from both samples agree, and|Q(8Li; 2+)|=32.7±0.6 mb has been determined. 相似文献
145.
T. Ohtsubo K. Matsuda T. Araki M. Mori M. Fukuda K. Matsuta Y. Nojiri T. Minamisono 《Hyperfine Interactions》1993,78(1-4):439-443
NMR spectra of12B in Pt (fcc) metal were observed by use of the -NMR detection method. A sharp single line was observed by use of an annealed Pt foil for the implantation medium. The dipolar broadening has been determined to be 332±30 Hz (HWHM). 相似文献
146.
Development of a laser ablation-hollow cathode glow discharge emission source and the application to the analysis of steel samples. 总被引:1,自引:0,他引:1
A novel atomic emission spectrometry comprising laser ablation as a sampling source and hollow cathode plasma for the excitation of ablated sample atoms is proposed. In this arrangement, a conventional Grimm-type discharge lamp is employed, but the polarity of the power supply is reversed so that the cylindrical hollow tube acts as a cathode and the glow discharge plasma is produced within this tube. A laser is irradiated to introduce sample atoms into the discharge plasma. Ablated atoms are excited by collisions with electrons and gas species, and emit characteristic radiation upon de-excitation. The experiments were conducted only in an atmosphere of helium gas so as to avoid a rapid erosion of the cathode hollow tube. Phase-sensitive detection with a lock-in amplifier was utilized to reject the continuous background emission of the plasma gas and emissions of sputtered atoms from the tube material. The unique feature of this technique is that the sampling and excitation processes can be controlled independently. The proposed technique was employed for the determination of Cr, Mn, and Ni in low-alloyed steel samples. The obtained concentrations are in good agreement with the reported values. The relative standard deviation (RSD), a measure of the analytical precision, was estimated to be 2-9% for Cr, 3-4% for Mn, and 4-11% for Ni determination. 相似文献
147.
Dongol KG Matsubara K Mataka S Thiemann T 《Chemical communications (Cambridge, England)》2002,(24):3060-3061
With ease, eta 6-dihydronaphthalene tricarbonylchromium(0) complexes undergo a triple arylation with concomitant ring closure, when submitted to Heck reactions under 'Jeffery conditions'. 相似文献
148.
Shuntaro Mataka Kazufumi Takahashi Masashi Tashiro 《Journal of heterocyclic chemistry》1981,18(6):1073-1075
The reaction of 3,4-dibenzoyl-1-methyl-2,5-diphenylpyrrole ( 1 ) and -1-phenylpyrazole ( 2 ) with methylamines ( 3a-c ) afforded pyrrolo[3,4-c]pyridine ( 4 ), and isomeric 2H-pyrazolo[3,4-c]pyridines ( 5a-c ) and [4,3-c]pyridines ( 6a-c ), respectively. 相似文献
149.
Matsuta K. Hashimoto K. Kudo S. Arimura K. Mihara M. Fukuda M. Minamisono T. 《Hyperfine Interactions》2001,136(3-8):503-507
The line widths of the β-NMR spectra of the short-lived β emitters 8Li and 12N implanted in a single crystal of Al have been measured precisely for the first time as a function of crystal orientation.
The NMR line widths were compared with the theoretical van Vleck values of the dipolar broadening. As a result, it was found
that 8Li mainly sits in substitutional sites, while 12N sits in tetrahedral interstitial sites, in Al.
This revised version was published online in September 2006 with corrections to the Cover Date. 相似文献
150.
Nojiri Y. Ishiga K. Onishi T. Sasaki M. Ohsumi F. Kawa T. Mihara M. Fukuda M. Matsuta K. Minamisono T. 《Hyperfine Interactions》1999,120(1-8):415-418
Hyperfine interactions of 8Li impurity nucleus imbedded in ferromagnetic Ni metal were studied using the β-NMR technique. Two kinds of hyperfine fields
B82 were found, corresponding to two different final sites of Li atoms in the Ni lattice. The nuclear spin-lattice relaxation
times T1 of 8Li in Ni were also determined for each field. Temperature dependencies of B82 and T1 were observed to deduce these values at T=0 K that can be compared with those calculated recently by Akai et al.
This revised version was published online in August 2006 with corrections to the Cover Date. 相似文献