SiO_2/间苯二酚杂化溶胶前驱体法制备SiO_2/SiC多孔纤维

本文采用溶胶-凝胶法制备间苯二酚/SiO_2杂化溶胶,拉丝法制取杂化纤维.并采用FT-IR、DSC、TG、XRD和SEM对杂化纤维进行了表征.结果表明,杂化纤维中部分间苯二酚与SiO_2形成共价键结构;杂化纤维呈非晶态.采用不同温度对杂化纤维进行热处理,得到的产物经1300 ℃处理后杂化纤维转变为SiO_2/SiC结晶性多孔纤维.     

界面对热沉用金刚石-Cu复合材料热导率的影响

用特殊粉末冶金技术制备了金刚石-Cu复合材料.用SEM、拉曼光谱、EDS分析了复合材料的界面状态,用激光闪光法测量复合材料常温下的热导率.结果表明:在最佳工艺参数下,复合材料热导率可达570W·m-1·K-1;烧结时添加适量的钴可极大促进金刚石与铜之间的粘结;钴向金刚石中的扩散及其在铜熔液中的固溶,使金刚石与铜之间形成过渡层;过渡层可增强金刚石与铜基体过渡界面的相容性,降低界面热阻;金刚石骨架的形成有助于获得超高热导率.     

Pointwise Estimate for Baskakov Operators

§ 1.Ｉｎｔｒｏｄｕｃｔｉｏｎ　Ｆｏｒｔｈｅｗｅｌｌ ｋｎｏｗｎＢｅｒｎｓｔｅｉｎｐｏｌｙｎｏｍｉａｌＢｎ(ｆ;ｘ) = ｎｋ=0ｆ ｋｎ ｐｎ,ｋ(ｘ) ,　ｐｎ ,ｋ(ｘ) =ｎｋ ｘｋ( 1 -ｘ) ｎ-ｋ,ＢｅｒｅｎｓａｎｄＬｏｒｅｎｔｚ[1]ｐｒｏｖｅｄｔｈａｔｆｏｒｆ∈Ｃ[0 ,1 ] ,0 <α<2 ,ｏｎｅｈａｓ｜ (Ｂｎｆ-ｆ) (ｘ) ｜=Ｏ ｘ( 1 -ｘ)ｎα/ 2 ω2 (ｆ;ｔ) =Ｏ(ｔα) . ( 1 .1 )Ｏｎｔｈｅｏｔｈｅｒｈａｎｄ ,ＤｉｔｚｉａｎａｎｄＴｏｔｉｋ[2 ]ｏｂｔａｉｎｅｄｔｈａｔｆｏｒｆ∈Ｃ[0 ,1 ] ,0 <α<2 ,ｏｎｅｈａｓ｜ (Ｂｎｆ -ｆ)…     

HPLC separation of triacylglycerol positional isomers on a polymeric ODS column

A polymeric ODS column was applied to the resolution of triacylglycerol positional isomers (TAG-PI), i.e. 1,3-dioleoyl-2-palmitoyl-glycerol (OPO) and 1,2-dioleoyl-3-palmitoyl-rac-glycerol (OOP), with a recycle HPLC system. To investigate the ODS column species and the column temperatures for the resolution of a TAG-PI pair, a mixture of OPO and OOP was subjected to an HPLC system equipped with a non-endcapped polymeric, endcapped monomeric, endcapped intermediate, or non-endcapped monomeric ODS column at three different column temperatures (40, 25, or 10 degrees C). Only the non-endcapped polymeric ODS column achieved the separation of OPO and OOP, and the lowest column temperature (10 degrees C) showed the best resolution for them. The other pair of TAG-PI, a mixture of 1,3-dipalmitoyl-2-oleoyl-glycerol (POP) and 1,2-dipalmitoyl-3-oleoyl-rac-glycerol (PPO) was also subjected to the system equipped with a non-endcapped polymeric or monomeric ODS column at five different column temperatures (40, 32, 25, 17, and 10 degrees C). Thus, POP and PPO were also separated on only the non-endcapped polymeric ODS column at 25 degrees C. However, no clear peak appeared at 10 degrees C. These results would indicate that the polymeric ODS stationary phase has an ability to recognize the structural differences between TAG-PI pairs. Also, the column temperature is a very important factor for separating the TAG-PI pair, and the optimal temperature would relate to the solubility of TAG-PI in the mobile phase. Furthermore, the recycle HPLC system provided measurements for the separation and analysis of TAG-PI pairs.     

两类正规化双全纯映照子族齐次展开式的精细估计

本文考虑C~n中单位多圆柱上和一般复Banach空间中单位球上的正规化双全纯α(0■α＜1)次的殆β(-π/2＜β＜π/2)型螺形映照以及α(0＜α＜1)次的β(-π/2＜β＜π/2)型螺形映照f(其中x=0是f(x)-x的k+1阶零点),研究了它们的构造,并得到其齐次展开式的精细估计．所得的结果推广了以前相应的结论．     

A remark on Nesterenko’s theorem for Ramanujan functions

We study the algebraic independence of values of the Ramanujan q-series $A_{2j+1}(q)=\sum_{n=1}^{\infty}n^{2j+1}q^{2n}/(1-q^{2n})$ or S _2j+1(q) (j≥0). It is proved that, for any distinct positive integers i, j satisfying $(i,j)\not=(1,3)$ and for any $q\in \overline{ \mathbb{Q}}$ with 0<|q|<1, the numbers A ₁(q), A _2i+1(q), A _2j+1(q) are algebraically independent over $\overline{ \mathbb{Q}}$ . Furthermore, the q-series A _2i+1(q) and A _2j+1(q) are algebraically dependent over $\overline{ \mathbb{Q}}(q)$ if and only if (i,j)=(1,3).