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31.
Oriňák Andrej Arlinghaus Heinrich Frank Vering Guido Justinová Martina Oriňáková Renáta Turčániová L’udmila Halama Maroš 《平面色谱法杂志一现代薄层色谱法》2003,16(1):23-27
JPC – Journal of Planar Chromatography – Modern TLC - Two interfaces have been tested for coupling thin-layer chromatography (TLC) with time-of-flight secondary-ion mass spectrometry... 相似文献
32.
The terminology ‘ID frequency’(w ID) is proposed after analyzing the 1D active photonic crystal based on the transfer matrix method. The relationship between wID and the structure parameters of the photonic crystal is investigated. 相似文献
33.
Elastic electron scattering on the exotic light nucleus28S is investigated in the plane wave Born approximation. The variation of the squared form factors of28S with momentum transfer is compared with that of32S. It is found that the behavior of the form factors near the second minimum (with a moderate momentum transfer) is sensitive
to the alteration of the charge density distribution of halo protons in28S. This indicates that elastic electron scattering can be a good probe of the structure of proton-halo nuclei. 相似文献
34.
本文测定了几种二茂铁有机锡衍生物的119Sn,13C NMR谱。对其中几种衍生物的13C NMR谱进行了归属,从而进一步验证了这类化合物的结构。着重讨论了结构如化合物中取代基X的改变对119Sn化学位移的影响。并对结构如
类化合物N→Sn异侧配位的问题进行了讨论。 相似文献
35.
C.J. Lu H.M. Shen S.B. Ren Y.N. Wang 《Applied Physics A: Materials Science & Processing》1997,65(4-5):395-401
3 thin films is systematically studied by using X-ray diffraction (XRD). The PbTiO3 thin films with different average grain sizes were prepared on various substrates by a sol-gel process. The films on NaCl
and fused glass are randomly grain-oriented, while those on (111)Pt/Ti/SiO2/Si are highly {100} cubic index grain-oriented . It is found from the XRD patterns of the films on NaCl that with decreasing
average grain size from 230 to 80 nm, the intensities of high h index (h>l) peaks (hkl), such as (100), (110), (200), (201),
(210), (211), etc., decrease rapidly and ultimately disappear, whereas another set of peaks (lkh), including (001), (002),
(102), (112), etc., are still intense. This interesting result suggests that at grain size below a certain critical size an
increasing number of grains no longer show 90°-domains, which is confirmed by TEM observations. Meanwhile, X-ray evidence
of such a grain-size-related absence of 90°-domains is also found for PbTiO3 films on Pt(111) and fused-glass substrates. The volume fractions of single-domain grains (without 90°-domains) in the films
are estimated from their XRD patterns. By combining SEM and TEM investigations, the critical grain size for the formation
of 90°-domains is further determined to be near 200 nm.
Received: 19 December 1996/Accepted: 24 March 1997 相似文献
36.
In this paper, we prove a sharpening of large deviation for increments of Brownian motion in (p,r)-capacity and Hölder norm case. As an application, we obtain a functional modulus of continuity for (p,r)-capacity in the stronger topology. 相似文献
37.
38.
Huang JM Yang CS Zhao R Takahashi H Fukuyama Y 《Chemical & pharmaceutical bulletin》2004,52(1):104-107
Seven new seco-prezizaane-type sesquiterpenes were isolated from the methanol extract of the pericarps of Illicium merrillianum. Their structures were elucidated as 3-deoxypseudoanisatin (1), 2beta-hydroxy-3,6-dedioxypseudoanisatin (2), 8alpha-hydroxy-10-deoxycyclomerrillianolide (3), 10beta-hydroxypseudoanisatin (4), 10beta-hydroxycyclopseudoanisatin (5), 1,6-dihydroxy-3-deoxyminwanensin (6), and 8-deoxymerrilliortholactone (7) by analyses of their spectroscopic data and chemical transformation. Compounds 4 and 5 as well as 6 and 7 coexist as a keto/acetal equilibrated mixture in methanol solution. 相似文献
39.
本文就薄膜法制样、用X-射线荧光谱法分析稀土样品时,试样面积和厚度对分析结果产生的影响作了定量研究,提出的有关分析条件和参数用于实际样品分析中,获得了满意的分析结果。 相似文献
40.