多层球对高斯波束散射的德拜级数研究

基于广义洛伦兹-米氏理论,利用多层球粒子散射系数的德拜级数展开公式,提出了一种新的研究多层球粒子对高斯波束散射的方法。计算结果与已有的广义洛伦兹-米氏理论算法的计算结果吻合得很好。利用该方法有效分离了折射率分布满足指数变化规律的多层球粒子对高斯波束散射的远区散射场中多阶彩虹的干涉强度分布。数值模拟了双层球的归一化双一阶彩虹强度分布以及各层的一阶彩虹艾里结构。最后分析讨论了高斯波束的入射位置和束腰半径对多层球单阶彩虹强度分布的影响。     

用于显示的透射型法布里-珀罗光调制器

提出了一种用于显示的,基于透射型法布里-珀罗干涉的微机电系统(MEMS)光学调制器。基于多光束干涉原理分析了调制器的光学特性,推导出了调制器结构的特征参量。分析表明,当调制器的腔长为cλ/4时,透射光可以实现暗态显示;当调制器的腔长取为零或cλ/2时,透射光可以实现亮态显示。通过控制法布里-珀罗腔长,就可实现调制器的明暗调制。理论上证明了该调制器用于显示的可行性。设计了一种基于微机电系统的透射型法布里-珀罗光学调制器结构,该调制器的理论衬比度达到150。仿真结果表明,该调制器具有2.4 V的低电压静电驱动性能。     

Metal-free cascade boron-heteroatom addition and alkylation with diazo compounds

Transition metal-catalyzed carbene transfer reaction is one of the most notable advances for C-C bond formation reactionsduring the past decade,which has been widely employed in the preparation of C3-substituted indoles,Here,we described an efficient exa mple of catalyst-and metal-free aminobo ration of alkynes and C—C bond formation with diazo compounds to produce C3-substituted indoles,Diverse alkynyla nilines and diazo compounds ca n be utilized for this tandem transfo rmation under mild reaction conditions,re sulting in broad functional group co mpatibility.Additionally,this metal-free strategy can be extended to construct substituted benzofurans.     

SQUID用于铍材残余应力检测的计算机模拟

依据SMM-601型超导量子干涉显微镜检测部分构建计算模型,采用电磁场有限元方法分析了残余应力引起的非磁性金属材料铍电导率变化对超导量子干涉仪(SQUID)检测信号的影响,并讨论了该方法实际应用于非磁性金属材料残余应力检测的条件和可能性。     

基于FPGA的DDS设计方法

介绍了一种基于FPGA的DDS设计方法,结合DDS的原理,给出了具体设计程序以及仿真波形。基于FPGA的DDS与传统的专业DDS芯片相比具有电路简单、输出波形调整灵活以及性价比高等特点。     

Ameliorating the interfacial issues of all-solid-state lithium metal batteries by constructing polymer/inorganic composite electrolyte

Lithium metal is one of the most promising anodes for next-generation batteries due to its high capacity and low reduction potential.However,the notorious Li de...     

加强物理实验改革培养学生创新能力

本文阐述了物理实验在培养创新能力方面的重要作用,针对物理实验存在的问题提出了改革措施,从而达到培养学生创新能力的目的。     

酶提取-单颗粒电感耦合等离子质谱法分析樱桃番茄纳米银颗粒及其吸收规律研究

为探究复合保鲜涂膜中AgNPs的迁移情况,采用酶提取的前处理方式,结合单颗粒电感耦合等离子体质谱（SP-ICP-MS）,考察了前处理方式、驻留时间、校准方式以及Ag+浓度等条件对AgNPs准确测定的影响。结果表明：0.1 g樱桃番茄样品在柠檬酸盐体系下使用0.2 g的R-10离析酶可达到消解最适酶剂量;当驻留时间小于100 μs时,测定结果有较好的积分条件以及较高的信背比;采用AgNP尺寸方式进行校准比单独用Ag+标准溶液校准方式的颗粒尺寸测定结果更加准确。采用该方法测定樱桃番茄中加标AgNPs颗粒回收率达到88.9%,粒径实测值为47.8±0.3 nm,粒径检出限为13 nm,颗粒浓度检出限为 7.5×104 particles/L。通过将樱桃番茄暴露于AgNPs涂膜中来探究AgNPs迁移行为,复合保鲜涂膜后的樱桃番茄通过三次洗涤后能够在表面去除大部分AgNPs,但仍有少量AgNPs穿过果表皮浸入果肉组织。该方法灵敏度高,操作简单,能够为揭示AgNPs在农产品及农业生产中的风险提供可靠、准确的表征方法。     

某些酚类的高温液相色谱行为

建立了高温液相色谱系统,在高温条件下,采用甲醇-水作为流动相,在Polymerx RP-1聚合物(PSDVB)色谱柱上考察了6种酚类样品的色谱行为.实验条件:温度40～160 ℃,流速0.2～5.5 mL/min,流动相中甲醇浓度范围40%～80%.考察了温度、流速和流动相组成对酚类样品的保留、分辨、柱效和系统压力的影响,探讨了酚类样品在聚合物柱上的热力学行为.温度升高2.35℃大约相当于流动相中甲醇浓度增加1%,可以通过改变色谱柱温度调节样品保留和改变选择性.柱温升高,降低了流动相的粘度,允许在高温条件下使用较高的流速实现快速分离.在160℃、V(甲醇):V(水)=40:60,为流动相和3 mL/min流速条件下,可于2.5 min内实现6种酚类的完全分离.     

Sizes,Components, Crystalline Structure,and Thermal Properties of Starches from Sweet Potato Varieties Originating from Different Countries

Sweet potato is a root tuber crop and an important starch source. There are hundreds of sweet potato varieties planted widely in the world. Starches from varieties with different genotype types and originating from different countries have not been compared for their physicochemical properties. In the research, starches from 44 sweet potato varieties originating from 15 countries but planted in the same growing conditions were investigated for their physicochemical properties to reveal the similarities and differences in varieties. The results showed that the 44 starches had granule size (D[4,3]) from 8.01 to 15.30 μm. Starches had different iodine absorption properties with OD680 from 0.259 to 0.382 and OD620/550 from 1.142 to 1.237. The 44 starches had apparent amylose content from 19.2% to 29.2% and true amylose content from 14.2% to 20.2%. The starches exhibited A-, C_A-, C_C-, or C_B-type X-ray diffraction patterns. The thermograms of 44 starches exhibited one-, two-, or three-peak curves, leading to a significantly different gelatinization temperature range from 13.1 to 29.2 °C. The significantly different starch properties divide the 44 sweet potato varieties into different groups due to their different genotype backgrounds. The research offers references for the utilization of sweet potato germplasm.