Co含量对Pr10Fe74-xCo10+xC4B4 (x=0,2,4,6,8) 快淬条带的磁性能的影响

用快淬方法制备了Pr10Fe74-xCo10+xC4B4 (x=0,2,4,6,8) 条带,研究了成分和工艺对条带磁性能的影响.实验发现,当x=2,带速是20 m·s-1时,条带的磁性能最佳,其剩磁Jr=0.94 T,矫顽力μ0 iHc=0.96 T,最大磁能积 (BH)max=127.32 kJ·m-3.通过Henkel-plot分析,发现x=2,带速为20 m·s-1的样品中的晶间交换作用最强,因而能获得最佳的磁性能.     

Infrared absorption line intensities forU(5) model of linear triatomic molecules

The symmetry of the rotation-vibration spectra for linear triatomic molecules is described by means of the groupU(5). The rotation-vibration levels of linear triatomic molecules HCN and COS are calculated. The infrared absorption line intensities are calculated for the COS molecule. The results are in good agreement with the experimental values.     

改进的QuEChERS结合超高效液相色谱-串联质谱法快速测定地表水中双酚类物质

建立了同时测定地表水中8种双酚类物质(BPs)的超高效液相色谱-串联质谱(UPLC-MS/MS)分析方法.方法 基于QuEChERS处理技术,选用乙酸乙酯为提取剂,从基质效应(ME)和萃取回收率(RE)两方面对过程效率(PE)进行优化,确定了50 mg N-丙基乙二胺(PSA)和50 mg石墨化炭黑(GCB)混合吸附剂...     

稀土Ce3+对盐胁迫下螺旋藻生理特性的影响

以非洲乍得湖钝顶螺旋藻为实验材料,在0.3 mol.L-1NaCl胁迫下,通过生理学方法研究了不同浓度Ce3+对螺旋藻生长的影响。结果表明:Ce3+浓度在8.104～16.208μmol.L-1之间时,促进了螺旋藻的生长以及叶绿素a的合成;Ce3+浓度在16.208～48.62μmol.L-1之间时,促进可溶性蛋白的合成;Ce3+浓度为8.104μmol.L-1时藻体MDA含量最高,之后MDA含量随着Ce3+处理浓度的增加逐步降低。这说明Ce3+在一定的浓度范围内可减轻NaCl对螺旋藻的胁迫作用,促进螺旋藻可溶性蛋白和叶绿素a的积累,降低藻细胞MDA的浓度,高浓度Ce3+则会与NaCl协同、抑制螺旋藻的生长。     

Assessment of trace elements characteristics and human health risk of exposure to ambient PM2.5 in Hangzhou,China

A method for simultaneously determining the trace elements in particulate matter (PM) (PM2.5) by inductively coupled plasma mass spectrometry was established. The PM2.5-loaded filter samples were digested under the optimised conditions including a mixture of HNO₃–HCl–HF with ultrasonication proceeding at 70°C for 2 h. Recoveries of 90.83–103.33% were achieved for 20 elements (Co, Sr, Ag, Cd, Sb, La, Ce, Sm, W etc.) in NIST standard reference material 1648a (urban PM). PM2.5 samples were collected at urban site in Hangzhou from August 2015 to November 2015. PM2.5 concentrations of 15% sampling days exceeded the daily limitation and the mean concentrations of PM2.5 from August to November reached the 66.4% of the limitation. PM2.5 concentrations in summer were higher than that in autumn. The concentration of Zn was highest, following with Al, Pb, Mn, Cu and As. Significant enrichment was observed in Mn, Zn, Pb, Ag, V, Ni, Cu, As, Se, Hg, Co, Cd and W, which was probably induced by vehicular exhaust, oil and residual fuel combustion and industrial emissions. The daily mass concentrations of PM2.5 and elements fluctuated significantly. Rainfall could significantly reduce the concentration of Ti, Mn, Cu, Zn, As, Se, Hg, Sr, Ag, Cd, Sb, La, Ce, Sm and Pb, and the risk levels of carcinogenic elements and non-carcinogenic elements in rain day were significantly lower (43.7–81.4%) than those in non-rain day. The risk levels of Co, Cd and As could lead to adverse health outcomes through the respiratory system, which should deserve more attention, while the risk levels of Ni and non-carcinogenic elements (Hg, Mn, Cu, Zn, Pb, V) were under average risk acceptance.     

Lévy噪声与周期力共同驱动下的螺旋波动力学

研究加性Lévy噪声与周期外力对FitzHugh-Nagumo可激系统中螺旋波动力学行为的影响.螺旋波波头的运动随外力周期在一定范围内呈规则变化,该规则变化可用相应的傅立叶谱理解,维持该规则变化的是锁频行为.Lévy噪声序列中包含着小概率的大尺度噪声,螺旋波波头运动改变主要来自于它们的影响,本文指出Lévy噪声对波头运动的影响也依赖于外力周期的取值.在适当的参数取值下,Lévy噪声的存在也能导致螺旋波的消失,这为螺旋波的控制、消除提供了一种方法.分析了系统周期与外力周期的锁定行为,给出了不同噪声强度下的Arnold舌,指出随机共振行为的存在.     

液相微萃取-高效液相色谱法测定尿样中的利多卡因

应用液相微萃取与高效液相色谱联用技术快速分析尿样中的利多卡因。考察了萃取溶剂、体积、萃取时间及料液pH值对液相微萃取的影响,建立了液相微萃取与高效液相色谱联用技术分析尿样中利多卡因的方法。优化的实验条件为：料液pH值12．0,萃取溶剂为5μL邻苯二甲酸二丁醅,萃取时间40min,搅拌速度80r／min。方法的线性范围为0．2-5mg／L;检出限为0．1mg／L;相对标准偏差小于6．3％。通过液相微萃取后,能有效地去除检测尿样中利多卡因的干扰物质,获得了较高的选择性。该方法简便、快速、灵敏、消耗有机溶剂少,是尿样中利多卡因检测的一种有效方法。     

Complex Dynamics of an Impulsive Control System in which Predator Species Share a Common Prey

In an ecosystem, multiple predator species often share a common prey and the interactions between the predators are neutral. In view of this fact, we propose a three-species prey-predator system with the functional responses and impulsive controls to model the process of pest management. It is proved that the system has a locally stable pest-eradication periodic solution under the assumption that the impulsive period is less than some critical value. In particular, two single control strategies (biological control alone or chemical control alone) are proposed. Finally, we compare three pest control strategies and find that if we choose narrow-spectrum pesticides that are targeted to a specific pest’s life cycle to kill the pest, then the combined strategy is preferable. Numerical results show that our system has complex dynamics including period-doubling bifurcation, quasi-periodic oscillation, chaos, intermittency and crises. This work is supported by National Natural Science Foundation of China (10171106).     

100kev,20mA多磁极会切场离子源的研制与调试

一、引 言 在科学技术领域中,离子源的应用越来越广泛,形成了一门独立的学科——离子应用科学。尤其是70年代以来由于离子注入技术应用到材料表面改性的研究取得进展,从而使离子注入技术得到发展。 离子注入材料表面改性是一门新技术,它的优点是离子注入不通过加热形成特定的原子混合,又能快速引入晶格缺陷,从而改变金属的微观结构及相成分,最后导致金属宏观性质的改变。     

SG－1FEL放大器实验中的频率和功率测量

介绍了曙光一号自由电子激光（ＳＧ－１ＦＥＬ）放大器实验中对输出微波功率高达１４０ＭＷ的信号的频率和功率的测量。分析了ｘ射线和微波器件（定向耦合器、衰减器）的窄脉冲响应对测试结果的影响。