顶空气相色谱法测定甲氧苄啶中的残留丙烯腈

采用顶空进样模式,以HP-624毛细管色谱柱为分离柱,二甲亚砜为溶剂,氮气作载气,FID为检测器,用气相色谱法测定甲氧苄啶中的残留丙烯腈。丙烯腈的线性范围为0．25～200．10μg,相关系数为0．9999,检出限为0.05μg,测定结果的相对标准偏差为3．4％,平均回收率为100．5％。     

ZTGC-900D型气相色谱仪的常见故障及其排除

介绍ZTGC-900D型气相色谱仪使用过程中出现的几起故障,对故障进行分析、诊断,提出了故障的排除方法。     

THE UNCONDITIONAL STABILITY FOR THE HYPERNEUTRAL TYPE CONSTANT LINEAR CONTROL SYSTEM WITH DELAYS

With great developments of 8cience and technology exten8ion of system scale and variousapplication of computer, control 8ystem become expansive and sophisticated in the structureproperty About the stable questions of the delny type and the delay neutral type continuouscontrol sy8tem, many good result8 bave been establi8hed by many authors, but we seldom 8eethe studying of the unconditional stability problem for the hyperneutral type. In this paper,applying to the frequency domain method and th…     

浅海多径时延估计的功率谱加权自相关方法

针对浅海近距离时倒谱多径时延峰变弱难以提取的问题,提出了一种功率谱加权自相关多径时延估计方法。该方法采用FFT估计信号功率谱,对功率谱取1-α次幂(0<α<1),再进行IFFT变换,对其实部进行峰值检测获得多径时延估计。根据目标能量通过特性在正横前递增正横后递减的特点,在已检测时延前后一定区间内搜索下一个时延值,实现多径时延的自动提取.理论分析表明,多径时延估计的倒谱法与自相关法都可以看作功率谱加权自相关法的特例.海试数据处理与基于Bellhop射线模型的仿真计算表明,该方法在近距离时多径时延峰比倒谱法更清晰,输出信噪比提高了3~4 dB.采用该方法自动提取的海底反射多径时延用于单个水听器对目标距离的估计,与GPS测量距离基本相符,验证了方法的有效性.     

位错载氢运动对材料氢脆行为的影响

位错载氢运动会导致金属结构材料中氢原子的再分布和氢损伤的加剧,但目前仍缺乏相关实验数据支撑。本文首先对比了高锰钢预充氢后在四种应变速率（1×10^–3 s^–1,1×10^–4 s^–1,1×10^–5 s^–1和1×10^–6 s^–1）下的断口特征,随后结合理论计算探究了不同应变速率下位错载氢对金属材料氢脆行为的影响。结果表明较慢应变速率（1×10^–5 s^–1 and 1×10^–6 s^–1）下拉伸的试样具有比较快应变速率（1×10^–3 s^–1 和 1×10^–4 s^–1）拉伸时更高的氢脆敏感性和更大的断口脆性区面积。这是因为较慢应变速率下拉伸时,氢可以随位错运动,导致在塑性变形过程中形成更大的氢原子扩散距离和脆性区深度。此外,在更慢的应变速率（1×10^–6 s^–1）下,晶界处可以富集更多的氢,导致断口具有最大的脆性区面积。但是由于塑性变形过程中形成大量对氢原子具有强束缚作用的缺陷,导致实际位错载氢运动距离远低于理论位错载氢运动距离。

     

工程力学矢量的规范表示与弹性力学的不变性

通过引入规范变换, 消除了工程力学矢量数学表示上的物理缺陷, 使规范化力学矢量与力学张量具有物理上的等价表示, 从而奠定了不变性弹性力学的基础. 为它在不同坐标下的具体应用提供了理论保障.     

ZnWO4:Cr3+晶体的光谱

采用提拉法生长出不同掺杂浓度的ZnWO4:Cr3+单晶.该材料在912nm处形成宽带荧光发射.激发峰随掺杂浓度的加大而向短波方向移动.在发射带晶体的吸收低,有可能作为在800-1000nm可调谐激光工作介质.     

A note on the inventory models for deteriorating items with ramp type demand rate

In this research we study the inventory models for deteriorating items with ramp type demand rate. We first clearly point out some questionable results that appeared in (Mandal, B., Pal, A.K., 1998. Order level inventory system with ramp type demand rate for deteriorating items. Journal of Interdisciplinary Mathematics 1, 49–66 and Wu, K.S., Ouyang, L.Y., 2000. A replenishment policy for deteriorating items with ramp type demand rate (Short Communication). Proceedings of National Science Council ROC (A) 24, 279–286). And then resolve the similar problem by offering a rigorous and efficient method to derive the optimal solution. In addition, we also propose an extended inventory model with ramp type demand rate and its optimal feasible solution to amend the incompleteness in the previous work. Moreover, we also proposed a very good inventory replenishment policy for this kind of inventory model. We believe that our work will provide a solid foundation for the further study of this sort of important inventory models with ramp type demand rate.     

内调制光电探测器光生电压的模型分析

针对栅压对内调制光电探测器耦合区的影响，以及横向发生的抽取效应对受光结的影响，从描述探测器的泊松方程、电流方程和连续性方程出发，通过计算输出电流Id，得出了内调制光电探测器受光结光生电压Vop，与栅压Vg的函数关系式，并依此建立了模型，该模型与实验结果基本吻合．由于该模型采用了电路形式，可以用PSPICE等软件进行模拟，这为研究内调制光电探测器的内部性质提供了理论基础．     

Consistency of the generalized MLE of a joint distribution function with multivariate interval-censored data

Wong and Yu [Generalized MLE of a joint distribution function with multivariate interval-censored data, J. Multivariate Anal. 69 (1999) 155-166] discussed generalized maximum likelihood estimation of the joint distribution function of a multivariate random vector whose coordinates are subject to interval censoring. They established uniform consistency of the generalized MLE (GMLE) of the distribution function under the assumption that the random vector is independent of the censoring vector and that both of the vector distributions are discrete. We relax these assumptions and establish consistency results of the GMLE under a multivariate mixed case interval censorship model. van der Vaart and Wellner [Preservation theorems for Glivenko-Cantelli and uniform Glivenko-Cantelli class, in: E. Gine, D.M. Mason, J.A. Wellner (Eds.), High Dimensional Probability, vol. II, Birkhäuser, Boston, 2000, pp. 115-133] and Yu [Consistency of the generalized MLE with multivariate mixed case interval-censored data, Ph.D Dissertation, Binghamton University, 2000] independently proved strong consistency of the GMLE in the L₁(μ)-topology, where μ is a measure derived from the joint distribution of the censoring variables. We establish strong consistency of the GMLE in the topologies of weak convergence and pointwise convergence, and eventually uniform convergence under appropriate distributional assumptions and regularity conditions.