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91.
M. Kh. Mamarakhmonov M. A. Ashirmatov Kh. M. Shakhidoyatov 《Chemistry of Heterocyclic Compounds》2001,37(8):993-996
Semiempirical quantum-chemical calculations have been carried out of the molecules of 2-oxopyrimidinones-4. The geometry and electronic structures and the stabilities of the tautomeric forms have been analyzed. 相似文献
92.
Kh. M. Shakhidoyatov N. I. Mukarramov F. R. Utaeva 《Chemistry of Natural Compounds》2008,44(5):625-629
The reaction of deoxypeganine (DOP) (1) and its hydrochloride (DOP·HCl) (2) with N-bromosuccinimide and a nitrating mixture was studied. It was found that bromination of DOP occurred at C-4 and the
aromatic ring. Nitration of DOP·HCl produced either 6-nitro- or 6,8-dinitro-deoxypeganines and 6-nitrodeoxyvasicinone or their
mixture in various ratios depending on the substrate:nitrating mixture ratio. 6Hand 6-Br-deoxypeganines were transformed into
the 4-hydroxy derivatives, 6H(Br) peganols or deoxyvasicinones. A method for qualitative and quantitative analysis of the
pure compounds and the mixture of reaction products using HPTLC was developed.
Translated from Khimiya Prirodnykh Soedinenii, No. 5, pp. 505–509, September-October, 2008. Original article submitted March
26, 2008. 相似文献
93.
The effects on the radiation response of Harwell polymethylmethacrylate (PMMA) dosimeters of dose-rate, radiation type, temperature during irradiation and post-irradiation storage, and post-irradiation stability, are of importance to the operators of commercial irradiation facilities.
This paper describes recent studies of the effects of some of these parameters on the radiation response of Harwell Red 4034, Amber 3042, and Gammachrome YR Perspex dosimeters, and provides data on batch to batch variation and shelf-life. 相似文献
94.
N. P. Abdullaev U. S. Makhmudov B. Tashkhodzhaev G. Genzhemuratova M. G. Levkovich Kh. M. Shakhidoyatov 《Chemistry of Natural Compounds》2009,45(6):837-843
N-Acyl cytisine derivatives were synthesized by acylation with acetic anhydride; benzoyl and o-bromo- and p-nitrobenzoyl chlorides; and crotonyl and cinnamoyl chlorides. The structures of the synthesized compounds were studied using
IR, PMR, and x-ray structure analysis (XSA). PMR spectra of the N-acylcytisines in solution typically had two rotational isomers around the N12–CO bond. Conformational analysis was performed
using XSA for the position of the acyl group relative to the cytisine core. Bond lengths and angles of the acyl groups involved
in the conjugation were analyzed. 相似文献
95.
96.
R. Sh. Kuryazov N. S. Mukhamedov Kh. M. Shakhidoyatov 《Chemistry of Heterocyclic Compounds》2009,45(12):1508-1514
The corresponding 6-chlorosulfonylquinazoline-2,4-diones were synthesized by the reactions of 1-methylquinazoline-2,4-dione
and its 3-alkyl-substituted derivatives with chlorosulfonic acid. Treatment of the products with nucleophilic agents (water
or ammonia, aliphatic and cyclic amines) gave 2,4-dioxoquinazolin-6-sulfonic acids or their amides. 相似文献
97.
T. F. Ibragimov M. G. Levkovich V. A. Saprykina Kh. M. Shakhidoyatov 《Chemistry of Natural Compounds》2010,46(5):767-770
N-Chloroacetylcytisine was synthesized by acylation of (–)-cytisine. Stable Z- and E-conformers with respect to rotational isomerism around the N-12–CO bond were found in PMR spectra at room temperature. The
point at which PMR resonances of the Z- and E-conformers coalesced upon heating was measured. The transition barrier between the conformers was estimated. 相似文献
98.
Ch. Sh. Kadyrov S. T. Akramov Kh. M. Shakhidoyatov N. P. Abdullaev O. G. Patseva 《Chemistry of Natural Compounds》1979,15(6):709-711
The growth-regulating activity of bis-quaternary salts of the pyrrolizidine series has been studied. It has been established that they possess a retardant activity which depends on the presence of the quaternary nitrogen atom, the acid residue of the molecule, and its configuration. 相似文献
99.
M. Shodiev B. A. Urakov N. I. Mukarramov Kh. M. Shakhidoyatov 《Chemistry of Heterocyclic Compounds》1993,29(11):1358-1360
The reaction of 6-oxo-, thioxo-2,3-dimethylthieno[2,3-d]pyrimidin-4-ones with electrophilic agents was studied. It was shown that during nitration these compounds undergo electrophilic unco-substitution forming 3-nitro- and 2-nitro-6-oxo- and 2,3-dinitro-6-thioxothieno[2,3-d]pyrimidin-4-ones, respectively; the reaction of these compounds with bromine proceeds in other directions.Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 11, pp. 1574–1576, November, 1993. 相似文献
100.