排序方式: 共有113条查询结果,搜索用时 15 毫秒
61.
Saeedi Mina Raeisi-Nafchi Maryam Sobhani Sepideh Mirfazli Seyedeh Sara Zardkanlou Mahsa Mojtabavi Somayeh Faramarzi Mohammad Ali Akbarzadeh Tahmineh 《Molecular diversity》2021,25(4):2399-2409
Molecular Diversity - In this work, various imidazo[1,2-a]pyridines linked to carbamate moiety were designed, synthesized, and evaluated for their α-glucosidase inhibitory activity. Among... 相似文献
62.
Aliakbar D. Khalaji Sepideh Maghsodlou Rad Gholamhossein Grivani Morteza Rezaei Kazuma Gotoh Hiroyuki Ishida 《中国化学》2011,29(8):1613-1616
Cobalt(III) complex [CoL3], where L=(5‐bromo‐2‐hydroxybenzyl‐2‐furylmethyl)imine, has been synthesized by reacting cobalt(II) nitrate with L. The complex has been characterized by elemental analysis and FT‐IR spectroscopy. The crystal structure of [CoL3] was determined by X‐ray crystallography from single crystal data. It crystallizes in the triclinic space group$ P {\bar 1} $ with unit cell parameters:a=9.6644(10) Å,b=11.5657(11) Å,c=16.5809(17) Å,α=102.833(4)°,β=102.999(3)°,γ=105.480(3)°,V=1659.9(3) Å3andZ=2. Thermal decomposition of [CoL3] was studied by thermogravimetry in order to evaluate its thermal stability and thermal decomposition pathways. 相似文献
63.
Sepideh Mirabi 《General Relativity and Gravitation》2013,45(12):2671-2682
In the present study we consider the Hamiltonian of the Dirac equation in curved space in fermi normal coordinates to first order in the Riemann tensor, including the corrections to the electromagnetic field. Then the energy level shifts by the local curvature for both relativistic and nonrelativistic levels in (Anti-)de Sitter space-time are calculated. 相似文献
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65.
Enzyme Free Electrochemiluminescence Sensor of Histamine Based on Graphite-carbon Nitride Nanosheets
Fazeleh Mesgari Foad Salehnia Sepideh Mohammad Beigi Morteza Hosseini Mohammad Reza Ganjali 《Electroanalysis》2022,34(4):659-666
The determination of histamine as one of the most important seafood poisoning compounds is essential nowadays. This paper reports a simple novel ECL sensor with g−C3N4 nanosheets (NSs) as an effective signal probe for the measurement of histamine without using any enzymatic reactions or complicated modifications. The ECL response of the sensor was linearly proportional to the concentration of histamine ranging from 1.0×10−7 to 7.5×10−4 mol/L, with a detection limit of 4.30×10−8 mol/L (R2=0.98401). The relative standard deviation (RSD) in repeatability and reproducibility tests were calculated to be 4.7 % and 3.6 % respectively. The presented sensor was successfully applied to the determination of histamine in canned tuna fish samples where it gave recoveries that ranged from 99.72 % to 101.96 % indicating that the method presented here is sensitive with high precision and is expected to have significant potential applications in clinical and the freshness quality of seafood. 相似文献
66.
Shirmehenji Reza Javanshir Sepideh Honarmand Moones 《Journal of Cluster Science》2021,32(5):1311-1323
Journal of Cluster Science - This study deals with producing selenium nanoparticles (SeNPs) by an economical and reliable process using a mining waste that contains significant amounts of selenium... 相似文献
67.
Sepideh Stewart Ralf Schmidt 《International Journal of Mathematical Education in Science & Technology》2017,48(8):S40-S49
ABSTRACTIn this study, we examined a mathematician and one of his students’ teaching journals and thought processes concurrently as the class was moving towards the proof of the Fundamental Theorem of Galois Theory. We employed Tall's framework of three worlds of mathematical thinking as well as Piaget's notion of accommodation to theoretically study the narratives. This paper reveals the pedagogical challenges of proving an elegant theory as the events unfolded. Although the mathematician was conscious of the students’ abilities as he carefully made the path accessible, the disparity between the mind of the mathematician and the student became apparent. 相似文献
68.
Trimellitic anhydride acid chloride (2) was obtained by the reaction of trimellitic anhydride (1) and excess amount of thionyl chloride. The acid chloride was reacted with 4,4′-diaminodiphenyl ether (3), and produced the monomer 4. Anthracene-9-carboxaldehyde (5) was reacted with sulfuryl chloride to produce anthracene-9-carboxylic acid chloride (6) in a quantitative yield. Through the reaction of 6 and 2,4,6-triamino-1,3,5-triazine (7), the monomer 8 was produced in high yield. Two monomers were characterized by 1H NMR and FT-IR spectroscopy, and then were used in the polymerization reaction. A new facile and rapid polycondensation reaction of the two monomers was performed by using a domestic microwave oven. The polymerization reaction proceeded rapidly, compared with the conventional solution polycondensation and was completed within 10 min, producing a photoactive poly(amide-imide) in a quantitative yield. The resulting polymer was characterized by IR, 1H NMR and TGA techniques. Thermogravimetric analysis indicated that polymer 9 was thermally stable in nitrogen atmosphere. In addition the initial decomposition temperature, 5% and 10% weight loss (T5, T10) were 284, 356 and 408 °C. The residual weight percent at 700 °C was 51.5%, which shows it is moderately thermally stable. Fluorescence properties of polymer 9 were investigated in several solvents. The ideal concentration of each case was determined by fluorescence self quenching phenomena. Also the self quenching mechanism was studied according to the specific behavior of the polymer in different solvents. 相似文献
69.
Shadpour E. Mallakpour Abdol‐Reza Hajipour Sepideh Khoee 《Journal of polymer science. Part A, Polymer chemistry》2000,38(7):1154-1160
A new facile and rapid polycondensation reaction of 4,4′‐(hexafluoroisopropylidene)‐N,N′‐bis(phthaloyl‐L‐leucine) diacid chloride (1) with several aromatic diamines, including benzidine (2a), 4,4′‐diaminodiphenyl methane (2b), 1,5‐diaminoanthraquinone (2c), 4,4′‐sulfonyldianiline (2d), 3,3′‐diaminobenzophenone (2e), P‐phenylenediamine (2f), 2,6‐diaminopyridine (2g), 4,4′‐diaminobenzophenone (2h), 2,4‐diaminotoluene (2i), and 4,4′‐diaminodiphenylether (2j), was developed with a domestic microwave oven in the presence of a small amount of a polar organic medium such as o‐cresol. The polymerization reactions proceeded rapidly compared to conventional solution polycondensation and finished within 12 min, producing a series of optically active poly(amide‐imide)s with quantitative yields and high inherent viscosities of 0.50–1.93 dL/g. All of the polymers were fully characterized by IR, elemental analyses, and specific rotation. Some structural characterization and physical properties of these optically active poly(amide‐imide)s are reported. © 2000 John Wiley & Sons, Inc. J Polym Sci A: Polym Chem 38: 1154–1160, 2000 相似文献
70.
Sarah Salloum Dr. Georg Bendt Dr. Markus Heidelmann Dr. Kateryna Loza Samaneh Bayesteh M. Sepideh Izadi Patrick Kawulok Dr. Ran He Dr. Heike Schlörb Dr. Nicolas Perez Dr. Heiko Reith Prof. Dr. Kornelius Nielsch Prof. Dr. Gabi Schierning Prof. Dr. Stephan Schulz 《ChemistryOpen》2021,10(2):189-198
The synthesis of phase-pure ternary solutions of tetradymite-type materials (BixSb1−x)2Te3 (x=0.25; 0.50; 0.75) in an ionic liquid approach has been carried out. The nanoparticles are characterized by means of energy-dispersive X-ray spectroscopy (EDX), powder X-ray diffraction (PXRD), scanning electron microscopy (SEM), and transmission electron microscopy. In addition, the role of different processing approaches on the thermoelectric properties - Seebeck coefficient as well as electrical and thermal conductivity - is demonstrated. 相似文献