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951.
Summary N-Benzoylphenylhydroxylarnine complexes of some metals have been investigated by HPLC. The green chromium complex formed by this reagent shows conclusive evidence of the presence of geometrical isomers. It is photosensitive and changes to a brown modification when irradiated with ultra violet or visible light. Elution behaviour of the complexes has been studied with different solvent mixtures. Attempts have been made to characterize the complexes from different measurements.
Untersuchung von isomeren Chrom-N-benzoylphenylhydroxylaminaten durch HPLC相似文献
952.
F. F. Dedus L. I. Kulikova S. A. Makhortykh N. N. Nazipova A. N. Pankratov R. K. Tetuev 《Moscow University Computational Mathematics and Cybernetics》2007,31(2):49-53
The analysis problem for genetic sequences is formulated from the viewpoint of modern mathematical and information approaches. Statistical, correlative, entropic, and spectral approaches are considered. A brief introduction into the background of the problem is given. Genesis of a new interdisciplinary subject area, bioinformatics, a science considering application of computer methods in biological studies, is analyzed. New approaches to studying macromolecular systems on the basis of combined spectral-analytic technologies are proposed. Estimates of the algorithmic complexity of implementation of the proposed approaches are presented. 相似文献
953.
954.
The performance of high power transistor devices is intimately connected to the substrate thermal conductivity. In this study, the relationship between thermal conductivity and dislocation density is examined using the 3 omega technique and free standing HVPE GaN substrates. Dislocation density is measured using imaging cathodoluminescence. In a low dislocation density regime below 105 cm−2, the thermal conductivity appears to plateau out near 230 W/K m and can be altered by the presence of isotopic defects and point defects. For high dislocation densities the thermal conductivity is severely degraded due to phonon scattering from dislocations. These results are applied to the design of homoepitaxially and heteroepitaxially grown HEMT devices and the efficiency of heat extraction and the influence of lateral heat spreading on device performance are compared. 相似文献
955.
K. Kosmidou F. Pasiouras M. Doumpos C. Zopounidis 《Central European Journal of Operations Research》2006,14(1):25-44
Further consolidation takes place not only among UK banks but also across borders, since some banks see size as a key factor
in remaining competitive in international markets. Therefore, it is interesting to investigate the effectiveness and performance
of UK banks. Based on their assets, banks are distinguished into small and large ones and a classification of UK banks in
a multivariate environment for the period 1998–2002 takes place. The PAIRCLAS multicriteria methodology is employed to investigate
the performance of UK small and large banks over multiple criteria, such as asset quality, capital adequacy, liquidity and
efficiency/profitability. A comparison with discriminant analysis (DA) and logistic regression (LR) facilitates the investigation
of the relative performance of PAIRCLAS against them. The results of the study determine the key factors that specify the
classification of a bank as small or large and provide us with the responsible banking decision makers for future readjustments. 相似文献
956.
M.C. Robinson D.J. Morris P.D. Hayenga J.H. Cho C.D. Richards R.F. Richards D.F. Bahr 《Applied Physics A: Materials Science & Processing》2006,85(2):135-140
Piezoelectric membranes have been fabricated that incorporate a gold bottom electrode with an adhesion layer of titanium–tungsten (10:90 wt. %). For solution-deposited acetic acid based lead zirconate titanate (HoAc-PZT) with a Zr:Ti ratio of 40:60, the film’s average piezoelectric coefficient, e31, is -5.31 C/m2, with a dielectric constant of 814 at 200 Hz, which is similar to values for platinum bottom electrodes. The PZT structure remains columnar on both types of bottom electrodes. Initial fabrication attempts resulted in cracking that initiated in the PZT layer of the structure. X-ray photoelectron spectroscopy was utilized to establish how processing affects diffusion throughout the composite membrane structure. Crack-free membranes were fabricated and tested. This paper discusses the performance properties and piezoelectric fatigue results for these membranes. PACS 77.84.-s; 77.84.Lf 相似文献
957.
G. F. Brand 《International Journal of Infrared and Millimeter Waves》2006,27(11):1445-1456
In this paper we evaluate methods for calculating dispersion relations for waves with wavelengths of the order of hundreds
of nanometres propagating in square waveguides with imperfectly conducting walls. The methods considered here are based on
those used previously for rectangular dielectric waveguides. 相似文献
958.
959.
960.
S. Barth H. R. Ott F. N. Gygax B. Hitti E. Lippelt A. Schenck Z. Fisk 《Hyperfine Interactions》1989,50(1-4):709-716
μ+ SR-measurements in transversally applied magnetic fields of 2000 G and 4000 G on heavy-electron single crystal U2Zn17 are presented. They reveal that at least two types of interstitial sites are occupied by the positive muons. One of these
sites (1/3, 2/3, 5/6) could be identified via induced local dipolar fields which aboveT
N=9.7 K can exactly be derived from the magnetic susceptibility. The corresponding component of the μ+-signal exhibits a steplike decrease by about 40% atT
N which is caused by the onset of a very broad distribution of static internal magnetic fields (ΔB≈1000 G) with zero average. Such a field distribution is in distinct contrast to dipolar-field calculations performed for
the simple antiferromagnetic structure deduced from neutron diffraction. The remaining 60% of the muons contributing to this
component belowT
N are subject to a narrow static field distribution (ΔB≈1 G). The induced dipolar fields at the site (1/3, 2/3, 5/6) are temperature-independent belowT
N. A weak dipolar coupling to the U-moments renders similar observations for muons occupying the second type of interstitial
impossible. 相似文献