由拟从属定义的单叶函数的逆在$k$次根变换下的Fekete-Szego问题

本文在逆函数$n$次根变换的条件下,利用拟从属定义了一个单叶解析函数类,估计了它的Fekete-Szeg\"o泛函.     

高阶加权微分算子谱的离散性

本文研究了加权的高阶微分算子的谱. 利用分解的方法和不等式的估计, 得到了一些高阶对称微分算子的任何自共轭扩张的谱离散的充分条件, 推广了 Pfeiffer , Sun, Glazman 等人的结果,利用这些结果可以判别某些微分算子谱的离散性.     

一类由从属关系定义的m-折对称双单叶函数的系数估计及Fekte-Szego不等式

本文研究了一类由从属关系定义的$m$-折对称双单叶函数的系数估计及Fekte-Szego不等式,所得结果改进或推广了已有部分作者的结论.     

海藻酸钙多孔微球-白芨多糖复合止血粉的制备及止血性能评价

海藻酸盐具有良好的生物相容性、可降解性、止血、抗菌、促愈合等特性,而中药白芨中的白芨多糖具有收敛止血、消肿生肌的功效。用海藻酸盐和白芨多糖为原料,采用冷冻干燥技术制备海藻酸钙多孔微球-白芨多糖复合止血粉,对其吸水速率进行考核,并采用体外凝血和动物出血模型实验进行止血性能评价。结果表明,致孔剂的添加量为0.5%的海藻酸钙多孔微球,当其与白芨多糖的质量比1:1时制备的止血粉的止血效果最好。     

DMSO-enhanced MALDI MS imaging with normalization against a deuterated standard for relative quantification of dasatinib in serial mouse pharmacology studies

Matrix-assisted laser desorption/ionization mass spectrometry imaging is an emerging powerful technique in drug metabolism and pharmacokinetics research. Despite recent progress in mass-spectrometry-based localization and relative quantification of small-molecule drugs and their metabolites in tissue, improved methods for drug extraction/ionization are required. Furthermore, relative quantification of drugs by mass spectrometry imaging in larger rodent cohorts is a necessary proof-of-concept study to demonstrate the utility of such a workflow in an industrial setting. Using as an example the tyrosine kinase inhibitor dasatinib, a leukemia drug, we demonstrate that inclusion of dimethyl sulfoxide in standard matrix solutions significantly improves ion intensity in mass spectrometry images and reveals enrichment of the drug in mouse kidney medulla. We furthermore show in a time-course study in multiple mice that normalization against a deuterated internal standard, dasatinib-D ₈, which is applied together with the matrix, makes possible relative quantification of the drug that correlates well with canonical liquid chromatography–tandem mass spectrometry based drug quantification.     

多层环形钢板式阻尼器钢板厚度对其性能影响的实验研究

多层环形钢板式隔振器是一种新型全金属隔振器。适用于重载高速、高低温及大温差等工况下的阻尼减振。本文对该隔振器的结构特点及制备方法进行了研究。主要分析了钢板厚度对隔振器性能的影响,制备出了具有不同结构形式和性能特点的样件,对样件进行了动静态实验研究;获得了钢板厚度不同时隔振器的弹性迟滞回线、隔振器系统频响特性、传递率及固有频率。研究结果表明:钢板厚度是影响隔振器性能的主要几何参数。改变钢板厚度,能够使隔振器具有不同的弹性阻尼性能和能量耗散性能,该结果对实际应用具有重要价值。     

离子液体的辐射效应研究进展

离子液体(ILs)具有低挥发性和化学稳定性,在萃取金属离子方面有着优异的表现,被认为是乏燃料后处理中的新一代绿色溶剂.然而在萃取放射性核素过程中,离子液体将处于强辐射场,因此离子液体辐射效应研究是其实际应用的前提.本文综述了国内外关于离子液体的辐射效应研究进展,包括辐照对离子液体结构和性质的影响,离子液体的脉冲辐解和激光光解研究,离子液体辐解产物的分析及其对核素萃取的影响等研究进展,并对今后该领域的研究方向进行了展望.     

Short range order of amorphous polymers derived by WAXS

Summary Radial difference distribution functions were calculated for PC anda-PS in a temperature range from 293 K to 455 K using wide angle X-ray scattering. Corrections of experimental scattering curves were examined. An assignment for some distances to intra- and intermolecular correlations was made. Next neighbour distances obtained from RDDFs are in good agreement with theoretically computed distances.

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Zusammenfassung Radiale Dichtedifferenzfunktionen für PC anda-PS werden im Temperaturbereich zwischen 393 K und 563 K aus Röntgenweitwinkel-Messungen berechnet. Die erforderlichen Korrekturen der experimentellen Intensitätsverteilung werden sorgfältig überprüft. Für einige Abstände kann eine erste Zuordnung ihres inter- und intramolekularen Ursprungs gegeben werden. Die Abstandswerte für die nächsten Nachbarn aus der RDDF stimmen mit den theoretisch berechneten Werten sehr gut überein.