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41.
Titanium dioxide was deposited from aqueous suspension onto cellulosic surfaces.Titania was sourced from Degussa (P25TM,70:30 anatase:rutile).Dry uptake of particles was shown to be rapid and dominant with one-third of the deposition occurring in less than 30 s and over one-half in the first minute.Isotherms were recorded to compare the rate of titanium deposition on dry and pre-wetted cotton.In the dry case uptake reached a maximum in 30 min whereas in the pre-wetted case the uptake was seen to continue beyond 180 min.A broad trend of higher deposition occurring at lower pH was seen,corresponding to the region where surface charges were opposite and thus attractive.Dry pickup was less significant at high pH.The response to varying ionic strength was complex and was attributed to the combined effect of charge screening,particle aggregation and consequent particle entrapment or occlusion.Titania deposition into the interstices of woven cotton sheets resulted in the formation of inorganic,nanoparticulate skeletons which could be isolated by controlled combustion of the cellulose and thus cotton was suggested to have potential for the templated synthesis of high surface area semiconductor materials. 相似文献
42.
T Madhusoodhanan Samit Mandal MP Sathyavathiamma Ramani NG Puttaswamy TS Mudhole A Mandal DK Avasthi R Shyam SK Datta 《Pramana》1999,53(3):541-544
The inclusive and exclusive measurements were carried out for 7Li projectile breakup on 27Al target at 48 MeV. In the inclusive data we have observed a broad peak around the beam velocity for alphas and tritons.
The exclusive data for alpha-triton coincidences show good agreement with the post-form DWBA theory of breakup reactions. 相似文献
43.
Anand Srivastav Hartmut Schroeter Christoph Michel 《Annals of Operations Research》2001,107(1-4):321-338
In this paper we study the problem of finding placement tours for pick-and-place robots, also known as the printed circuit board assembly problem with m positions on a board, n bins containing m components and n locations for the bins. In the standard model where the working time of the robot is proportional to the distances travelled, the general problem appears as a combination of the travelling salesman problem and the matching problem, and for m=n we have an Euclidean, bipartite travelling salesman problem. We give a polynomial-time algorithm which achieves an approximation guarantee of 3+. An important special instance of the problem is the case of a fixed assignment of bins to bin-locations. This appears as a special case of a bipartite TSP satisfying the quadrangle inequality and given some fixed matching arcs. We obtain a 1.8 factor approximation with the stacker crane algorithm of Frederikson, Hecht and Kim. For the general bipartite case we also show a 2.0 factor approximation algorithm which is based on a new insertion technique for bipartite TSPs with quadrangle inequality. Implementations and experiments on real-world as well as random point configurations conclude this paper. 相似文献
44.
Michael Schroeter 《合成通讯》2013,43(16):2203-2212
The unexpected occurrence of ketones 9 and 16 in addition to expected alcohols 5 and 15 in the synthesis of sesquiterpenes salsolenketone 1 and salsolene oxide 2 during Grignard reactions of the corresponding aldehydes with bromoalkenes under air‐ and water‐free conditions by the Meerwein–Ponndorf–Verley–Oppenauer reaction is reported. The product distribution could be influenced by the amounts of aldehyde used. 相似文献
45.
H. Schroeter 《Acta Mathematica》1884,5(1):205-208
Ohne Zusammenfassung
Auszug aus einem Schreiben an Herrn G. Mittag-Leffler. 相似文献
46.
47.
Detlef Schröder Katrin Schroeter Waltraud Zummack Helmut Schwarz 《Journal of the American Society for Mass Spectrometry》1999,10(9):878-882
Charge reversal (+CR−) of cations to anions can be used to structurally differentiate isomeric C6H5+ and C6H6+· hydrocarbon ions by means of tandem mass spectrometry. In view of the manifold of possible isomers, only a few prototype precursors are examined. Thus, charge inversion demonstrates that electron ionization of 2,4-hexadiyne yields an intact molecular ion, whereas the charge inversion spectra of C6H6+· obtained from benzene, 1,5-hexadiyne, and fulvene are identical within experimental error. Similarly, the +CR− spectrum of the C6H5+ cation generated by dissociative ionization of 2,4-hexadiyne is significantly different from the +CR− spectrum of C6H5+ obtained from iodobenzene, suggesting the formation of a 2,4-hexadiynyl cation from the former precursor. Although charge inversion of cations to anions has a low efficiency and requires large precursor ion fluxes, the particular value of this method is that the spectra may not just differ in fragment ion intensities, but these differences can directly be related to the underlying ion structures. 相似文献
48.