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191.
Hans Richter 《Monatshefte für Mathematik》1941,50(1):14-26
Ohne ZusammenfassungMit einer Figur im Text. 相似文献
192.
193.
194.
195.
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197.
W. Richter 《Archive of Applied Mechanics (Ingenieur Archiv)》1940,11(6):437-450
Ohne Zusammenfassung 相似文献
198.
Paulo Debiagi Coskun Yildiz Marcel Richter Jochen Ströhle Bernd Epple Tiziano Faravelli Christian Hasse 《Proceedings of the Combustion Institute》2021,38(3):4053-4061
Coal combustion releases elevated amounts of pollutants to the atmosphere including SOX. During the pyrolysis step, sulfur present in the coal is released to the gas phase as many different chemical species such as H2S, COS, SO2, CS2, thiols and larger tars, also called SOX precursors, as they form SOX during combustion. Understanding the sulfur release process is crucial to the development of reliable kinetic models, which support the design of improved reactors for cleaner coal conversion processes. Sulfur release from two bituminous coals, Colombian hard coal (K1) and American high sulfur coal (U2), were studied in the present work. Low heating rate (LHR) experiments were performed in a thermogravimetric analyzer coupled with mass spectrometry (TG-MS), allowing to track the mass loss and the evolution of many volatile species (CO, CO2, CH4, SO2, H2S, COS, HCl and H2O). High heating rate (HHR) experiments were performed in an entrained flow reactor (drop-tube reactor – DTR), coupled with MS and nondispersive infrared sensor (NDIR). HHR experiments were complemented with CFD simulation of the multidimentional reacting flow field. A kinetic model of coal pyrolysis is employed to reproduce the experiments allowing a comprehensive assessment of the process. The suitability of this model is confirmed for LHR. The combination of HHR experiments with CFD simulations and kinetic modeling revealed the complexity of sulfur chemistry in coal combustion and allowed to better understand of the individual phenomena resulting in the formation of the different SOX precursors. LHR and HHR operating conditions lead to different distribution of sulfur species released, highly-dependent on the gas-phase temperature and residence time. Higher retention of total sulfur in char is observed at LHR (63%) when compared to HHR (37–44%), at 1273 K. These data support the development of reliable models with improved predictability. 相似文献
199.
Avinash Bhardwaj David Richter Manojkumar Chellamuthu Jonathan P. Rothstein 《Rheologica Acta》2007,46(6):861-875
The effect of initial microstructural deformation, alignment, and morphology on the response of wormlike micelle solutions
in transient uniaxial extensional flows is investigated using a pre-shear device attached to a filament stretching rheometer.
In filament stretching experiments, increasing the strength and the duration of the pre-shear just before stretch is found
to delay the onset of strain hardening. In these experiments, the wormlike micelle solution filaments fail through a rupture
near the axial midplane. The value of the elastic tensile stress at rupture is found to decrease with increasing pre-shear
rate and duration. The most dramatic effects are observed at shear rates for which shear banding has been independently observed.
The reduction in the strain hardening suggests that pre-shear before filament stretching might break down the wormlike micelles
reducing their size before stretch. Strain hardening is also observed in capillary breakup rheometry experiments; however,
the pre-sheared wormlike micelle solutions strain harden faster, achieve larger steady-state extensional viscosities and an
increase in the extensional relaxation time with increasing shear rate and duration. The difference between the response of
the wormlike micelles in filament stretching and capillary breakup experiments demonstrates the sensitivity of these self-assembling
micelle networks to pre-conditioning. 相似文献
200.
Denise Tofanello Gimenes Wallans Torres Pio dos Santos Rodrigo Alejandro Abarza Munoz Eduardo Mathias Richter 《Electrochemistry communications》2010,12(2):216-218
In this work, we describe for the first time the use of the internal standard method in flow injection analysis (FIA) with amperometric detection. The method is based on the application of sequential potential pulses to the working electrode in an electrochemical flow cell. The sequence of potential pulses is selected in such a way that the analyte and internal standard compound are detected and monitored individually and independently at the same working electrode. This approach compensates for random errors associated with variations of flow rate, injection volume, ionic strength difference between standards and samples, and accidental insertion or formation of air bubbles in the carrier stream. In addition, this method can overcome the major drawback of amperometric detection using solid electrodes, which is gradual electrode passivation. To illustrate the potential of this method, the flow-injection amperometric detection of uric acid using [Fe(CN)6]3? as an internal standard (IS) is presented as an example. 相似文献