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61.
Tianqing Jia Motoyoshi Baba Fuli Zhao Xiaojun Wu Masayuki Suzuki Zhizhan Xu 《Solid State Communications》2007,141(11):635-638
We present a simple route for ZnSe nanowire growth in the ablation crater on a ZnSe crystal surface. The crystal wafer, which was horizontally dipped in pure water, was irradiated by femtosecond laser pulses. No furnace, vacuum chamber or any metal catalyst were used in this experiment. The size of the nanowires is about 1-3 μm long and 50-150 nm in diameter. The growth rate is 1-3 μm/s, which is much higher than that achieved with molecular-beam epitaxy and chemical vapor deposition methods. Our discovery reveals a rapid and simple way to grow nanowires on designed micro-patterns, which may have potential applications in microscopic optoelectronics. 相似文献
62.
Hierarchical structure in polymer‐based drug delivery systems as probed by calorimetric measurements
Pascale Valot Nathalie Sintes‐Zydowicz Jean‐Marie Nedelec Mohamed Baba 《Journal of Polymer Science.Polymer Physics》2010,48(18):1939-1945
Thermoporosimetry (TPM), a differential scanning calorimetry technique that relies on the shift of transition temperatures caused by the confinement of liquids, was applied to elucidate the complex morphology of drug‐loaded polymeric microcapsules prepared by the emulsion solvent evaporation method. For the very first time, TPM has been applied simultaneously with two liquids as structural probes. It was found that Miglyol, which dissolves the selected drug (Ibuprofen), is confined inside vesicles having a mean radius of 26.3 nm, whereas water, which is the continuous phase, is trapped inside a swollen polymeric network of Eudragit with an average mesh radius of 1.7 nm. A proposed hierarchical structure is given, which predicts that Eudragit microcapsules are formed from a collection of inert oil vesicles partitioned by polymeric Eudragit membranes swollen by water. © 2010 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 48: 1939–1945, 2010 相似文献
63.
64.
A sensitive determination of gas chromatographic peak yields by a new radio-gas chromatograph equipped with a synchronized accumulating radioisotope detector is described. Peak yields could be easily determined by the radio-gas chromatograph using [3H]hexadecane or [3H]androstenedione as a standard substance. The usefulness of the determination of peak yields was demonstrated by optimizing the derivatization conditions of 6-keto-prostaglandin F1 alpha. 相似文献
65.
S. Banerjee S. N. Ganguli A. Gurtu R. Raghavan K. Shankar Y. Goldschmidt-Clermont R. T. Ross S. Squarcia K. Dziunikowska T. Haupt P. Girtler D. Kuhn G. Koul Devanand P. V. K. S. Baba Gian Singh K. W. J. Barnham J. Wells P. R. S. Wright F. Mandl M. Markytan M. Bardadin-Otwinowska M. Szczekowski 《Zeitschrift fur Physik C Particles and Fields》1986,31(3):409-416
Results are presented on inclusive production of ∑+(1385) and ∑?(1385) inK ? p interactions at 110 GeV/c. The inclusive and topological cross sections have been estimated and compared with published results at lower energies. The inclusive cross section of ∑+(1385) seems to decrease with c.m. energy, while that of the ∑?(1385) is nearly constant. The mean charged multiplicity associate to Σ(1385) increases with c.m. energy. The ∑+(1385) is produced both in the target fragmentation region and in the central region where ∑?(1385) is predominantly produced in the central region. Approximately 16% of the Λ's stem from the decay of ∑±(1385) and the kinematic distributions of these Λ's are not very different from the inclusive Λ's. 相似文献
66.
Jnn'ichi Toei Keizen Fujii Nobuyuki Baba 《Fresenius' Journal of Analytical Chemistry》1989,334(1):13-15
Summary A new type reaction valve for flow injection analysis has been developed. In a FIA system with this valve the injected sample is once passed into a loop of the valve, thereafter the valve is rotated to the next position. Therefore, the sample is retained in the loop in a stop-state for a long time and the next sample is introduced into another loop in the next position. When the valve is rotated for one round, the stopped sample in the fist loop is again passed into the detector flow cell. Thus, an analysis, which needs a long reaction time, can be performed with this valve with high precision.
Verbessertes Reaktionsventil für die Flie\injektionsanalyse相似文献
67.
Han-zhou Yu Jing Li Yan-Lin Ye Biao Yang Cheng-Jian Lin Hui-Ming Jia Jian-Ling Lou Xiao-Fei Yang T. Baba Qi-Te Li Yu-Cheng Ge Zhi-Huan Li Hui Hua Jin-Yan Xu Zai-Hong Yang Jun Feng Hong-Liang Zang Qiang Liu Wei Jiang Yang Liu Jing-Jing Li Wei Liu Shi-Wei Bai Jie Chen Jia-Xing Han Jia-Hao Chen Kai Ma Dong-Xi Wang Lei Yang Nan-Ru Ma LI-Jie Sun 《中国物理C(英文版)》2021,45(8):084002-084002-5
68.
Mahdi Rabbani Yongli Wang Reza Khoshkangini Hamed Jelodar Ruxin Zhao Sajjad Bagheri Baba Ahmadi Seyedvalyallah Ayobi 《Entropy (Basel, Switzerland)》2021,23(5)
Network anomaly detection systems (NADSs) play a significant role in every network defense system as they detect and prevent malicious activities. Therefore, this paper offers an exhaustive overview of different aspects of anomaly-based network intrusion detection systems (NIDSs). Additionally, contemporary malicious activities in network systems and the important properties of intrusion detection systems are discussed as well. The present survey explains important phases of NADSs, such as pre-processing, feature extraction and malicious behavior detection and recognition. In addition, with regard to the detection and recognition phase, recent machine learning approaches including supervised, unsupervised, new deep and ensemble learning techniques have been comprehensively discussed; moreover, some details about currently available benchmark datasets for training and evaluating machine learning techniques are provided by the researchers. In the end, potential challenges together with some future directions for machine learning-based NADSs are specified. 相似文献
69.
Hiroyuki Suga Satoshi Higuchi Daisuke Ishimoto Yuta Hashimoto Teruko Tsuchida Toshihide Baba 《Tetrahedron》2010,66(16):3070-6287
High enantioselectivities (94-96% ee) were obtained for the inverse electron-demand 1,3-dipolar cycloadditions between cyclohexyl vinyl ether and 2-benzopyrylium-4-olate generated via Rh2(OAc)4-catalyzed decomposition of o-methoxycarbonyl-α-diazoacetophenone. The reactions were effectively catalyzed by Eu(OTf)3, Ho(OTf)3, or Gd(OTf)3 complexes (10 mol %) of chiral 2,6-bis[(4S,5S)-4,5-diphenyl-2-oxazolinyl]pyridine. The reactions with the other electron-rich dipolarophiles such as allyl alcohol, 2,3-dihydrofuran, and butyl-tert-butyldimethylsilylketene acetal showed moderate enanantioselectivities (60-73% ee). Good to high enantioselectivities (73-97% ee) were also obtained for the cycloadditions between 3-acyl-2-benzopyrylium-4-olates, generated from methyl 2-(2-diazo-1,3-dioxoalkyl)benzoates and butyl or cyclohexyl vinyl ethers, in the presence of binaphthyldiimine (BINIM)-Ni(II) complexes (10 mol %). Under similar conditions, the reaction between methyl 2-(2-diazo-1,3-dioxohexyl)benzoate and 2,3-dihydrofuran was highly endo-selective, and moderately enantioselective (70% ee). For the BINIM-Ni(II)-catalyzed reactions of cyclohexyl vinyl ether, the use of an epoxyindanone as the 3-acyl-2-benzopyrylium-4-olate precursor revealed that the chiral Lewis acid can function as a catalyst for asymmetric induction. The scope of the cyclic carbonyl ylides was extended to those generated from 1-diazo-2,5-pentanedione derivatives, which were reacted with butyl or TBS vinyl ether and catalyzed using the (4S,5S)-Pybox-4,5-Ph2-Lu(OTf)3 complex to give good levels of asymmetric inductions (75-84% ee). 相似文献
70.
Haruka Baba 《Tetrahedron letters》2010,51(15):2063-4307
Treatment of alkylbenzenes with p-toluenesulfonamide and 1,3-diiodo-5,5-dimethylhydantoin (DIH) in a small amount of carbon tetrachloride at 60 °C gave the corresponding α-p-toluenesulfonylamido)alkylbenzenes in good to moderate yields. The present reaction is a simple method for the α-sulfonylamidation of the benzylic position in alkylbenzenes. 相似文献