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Mariana C. O. Monteiro Stefan Dieckhfer Tim Bobrowski Thomas Quast Davide Pavesi Marc T. M. Koper Wolfgang Schuhmann 《Chemical science》2021,12(47):15682
Large scale CO2 electrolysis can be achieved using gas diffusion electrodes (GDEs), and is an essential step towards broader implementation of carbon capture and utilization strategies. Different variables are known to affect the performance of GDEs. Especially regarding the catalyst loading, there are diverging trends reported in terms of activity and selectivity, e.g. for CO2 reduction to CO. We have used shear–force based Au nanoelectrode positioning and scanning electrochemical microscopy (SECM) in the surface-generation tip collection mode to evaluate the activity of Au GDEs for CO2 reduction as a function of catalyst loading and CO2 back pressure. Using a Au nanoelectrode, we have locally measured the amount of CO produced along a catalyst loading gradient under operando conditions. We observed that an optimum local loading of catalyst is necessary to achieve high activities. However, this optimum is directly dependent on the CO2 back pressure. Our work does not only present a tool to evaluate the activity of GDEs locally, it also allows drawing a more precise picture regarding the effect of catalyst loading and CO2 back pressure on their performance.Large scale CO2 electrolysis can be achieved using gas diffusion electrodes (GDEs), and is an essential step towards broader implementation of carbon capture and utilization strategies. 相似文献
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Femtosecond far-infrared radiation pulses in the THz spectral range were observed as a consequence of the energy modulation of 1.7 GeV electrons by femtosecond laser pulses in the BESSY storage ring in order to generate femtosecond x-ray pulses ("femtoslicing"). In addition to being crucial for diagnostics of the laser-electron interaction, the THz radiation itself is useful for experiments where intense ultrashort THz pulses of well-defined temporal and spectral characteristics are required. 相似文献
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Utilizing contrast-enhanced MR histology, individual cell bodies were identified in situ and compared one-to-one with conventional histology. The squid Lolliguncula brevis served as a model where the receptor cells of the proprioceptive neck receptor organ were labeled with paramagnetic cobalt(II) ions by conventional cobalt iontophoresis. Stimulated echo images were obtained using a 9.4 T magnet and followed by conventional histologic treatment and light microscopy. Images obtained from both these techniques match well and validate MR histology. 相似文献
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