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71.
Nonlinear Dynamics - In this paper, amplitude death (AD) is investigated theoretically and numerically in N globally delay-coupled fractional-order oscillators. Due to the presence of... 相似文献
72.
This study developed an open‐tubular capillary electrochromatography protocol for the analysis of antipyretic analgesic drugs, which used a multifunctional homopolymer as coating. A controlled/living radical polymerization strategy was adopted to obtain poly(N‐acryloxysuccinimide) with a tunable chain‐length. The homopolymer coating enhanced the separation performance by contributing to the hydrophobic and hydrogen‐bonding interactions between the analytes and the homopolymer. The effect of polymer chain‐length and buffer pH and concentration on the separation efficiency was evaluated. In this approach, baseline separation of the three test drugs was achieved within 15 min. The repeatability of the prepared homopolymer coating was investigated, with the relative standard deviations < 2.88% observed in intra‐ and interday runs. Good linearity in the 5–800 µM range (R2 ≥ 0.998) demonstrates that accurate quantitative analysis of real samples was achieved. Moreover, the proposed assay was used to quantify the three drugs (aminopyrine, 4‐aminoantipyrine, and phenacetin) in urine samples, achieving recovery rates between 92.1 and 108.7%. This promising methodology may be used for the analysis of drugs in real bio‐samples and for the development of unique homopolymer coatings for open‐tubular capillary electrochromatography systems. 相似文献
73.
74.
Chen Chao-Yue Qiao Yu Zhang Lei Wang Xin Yang Ting-Hai 《Research on Chemical Intermediates》2020,46(9):4079-4089
Research on Chemical Intermediates - When synthesizing cyclohexane-annulated pyrazolones from a cyclohexonedicarboxylate derivative with phenylhydrazine under the catalysis of sulfuric acid in the... 相似文献
75.
Qian Yi Qiao Peng Li Long Han Haoyue Zhao Rongmin Zhang Haiming 《Journal of Thermal Analysis and Calorimetry》2020,142(1):425-435
Journal of Thermal Analysis and Calorimetry - In this article, a pillared layered antimony hydroxide (Sb-LH) material has been prepared by the hydrothermal method. X-ray diffraction,... 相似文献
76.
77.
增广Lü系统是仅含有两个控制参数的三维混沌系统,可产生一个伪四翼吸引子.利用混沌反控制方法,通过在增广Lü系统中引入一个简单的线性状态控制器,提出了一个新三维混沌系统——广义增广Lü系统.新系统实现了一个真正的具有复合结构的四翼吸引子,它包含了两个镜像对称的子系统.理论分析、数值仿真和电路实验证明了广义增广Lü系统四翼吸引子的存在性,也阐述了广义增广Lü系统有着较增广Lü系统更加丰富的动力学特性.
关键词:
广义增广Lü系统
四翼吸引子
数值仿真
电路实验 相似文献
78.
利用Nd: YAG脉冲激光在空气中烧蚀金属Cu靶,获得等离子体光谱;采用改变离焦量的方法,研究了离焦量的变化对谱线结构及谱线强度的影响;分析了离焦量分别为1mm、0mm和-2mm时,沿靶面法线方向不同空间距离处电子温度的演化规律;并对等离子体光谱的特性和产生机制进行了讨论. 结果表明,谱线结构、谱线强度和等离子体的电子温度都与离焦量的变化密切相关,聚焦点在-2mm处CuⅠ谱线相对强度出现峰值,电子温度数值最大;聚焦点在-0.5mm和-1.0mm附近谱线相对强度遽然降低的现象是由于等离子体的屏蔽效应造成的. 相似文献
79.
Formation of the intermediate semiconductor larger for the Ohmic contact to silicon carbide using Germanium implantation 下载免费PDF全文
By formation of an intermediate semiconductor layer (ISL) with a
narrow band gap at the metallic contact/SiC interface, this paper
realises a new method to fabricate the low-resistance Ohmic contacts
for SiC. An array of transfer length method (TLM) test patterns is
formed on N-wells created by P+ ion implantation into
Si-faced p-type 4H-SiC epilayer. The ISL of nickel-metal Ohmic
contacts to n-type 4H-SiC could be formed by using Germanium ion
implantation into SiC. The specific contact resistance ρc as low as 4.23× 10-5~Ωega \cdotcm2 is
achieved after annealing in N2 at 800~°C for 3~min,
which is much lower than that (>900~°C) in the typical SiC
metallisation process. The sheet resistance Rsh of the
implanted layers is 1.5~kΩega /\Box. The technique for
converting photoresist into nanocrystalline graphite is used to
protect the SiC surface in the annealing after Ge+ ion
implantations. 相似文献
80.
Hongjun Liu Hongying Wang Xiaoli Li Yishan Wang Wei Zhao Chi Ruan 《Optics Communications》2009,282(9):1858-1860
Stacking chirped pulse optical parametric amplification based on a home-built Yb3+-doped mode-locked fiber laser and an all-fiber pulse stacker has been demonstrated. Energic 11 mJ shaped pulses with pulse duration of 2.3 ns and a net total gain of higher than 1.1 × 107 at fluctuation less than 2% rms are achieved by optical parametric amplification pumped by a Q-switched Nd:YAG frequency-doubled laser, which provides a simple and efficient amplification scheme for temporally shaped pulses by stacking chirped pulse. 相似文献