火焰原子吸收光谱法测定磁化杯中铅、镉和铁

本文研究了火焰原子吸收光谱法测定磁化杯陶瓷内胆中Ｐｈ、Ｃｄ和Ｆｅ含量的方法。样品经粉碎，用硝酸－高氯酸混合液进行消解后测定。本法灵敏度高，干扰少，简单，快速，具有良好的精密度和准确度，其相对标准偏差分别为Ｐｂ３．９９％，Ｃｄ１０．７％，Ｆｅ０．９％。回收率Ｐｂ１００．６１％，Ｃｄ１０１．１８％，Ｆｅ１０２．４％。     

Interfacial effects on stress distribution in model composites

Raman mechanical spectroscopy was used to examine interfacial effects on the stress distribution in model polydiacetylene fiber/epoxy composites. Epoxy release agents were coated on fiber surfaces to modify the interfacial adhesion properties. The modified fiber surfaces were then characterized by scanning electron microscopy and x-ray photoelectron spectroscopy as well as optical microscopy. No difference in the maximum stress value or stress distribution was observed for the two types of fibers, coated or uncoated, used in composites. This suggests that adhesion properties at the composite interface do not affect tensile stress transfer efficiency nor, therefore, the composite tensile modulus along the fiber axis direction in uniaxial composites. Experimental data were also compared with theoretical calculations assuming perfect bonding between fiber and matrix, and idealized frictional force transfer mechanism at the fiber–matrix interface.     

InAs/GaAs自组织量子点的DLTS谱

将DLTS用于对InAs/GaAsQD结构样品的测量,测定了QD能级发射载流子的热激活能;获得了QD能级俘获电子过程伴随有多声子发射(MPE)、QD能级存在一定程度的展宽、以及在某些特定的生长条件下,存在亚稳生长构形的实验证据.结果表明:DLTS在QD体系的研究中有其特有的功能     

延长速调管使用寿命的方法

描述了一种延长EPR波谱仪中速调管使用寿命的方法.根据这种方法,只要正确地调谐微波桥的工作状态和适当地调整功率电平器的功率校正电平.即使对于已经严重老化的速调管仍然可以继续使用一段时间,维持仪器的正常运行.     

短脉冲载荷下金属材料的层裂破坏

 本文用点炮加载聚酯薄膜飞片撞击金属靶材料，飞片速度0.714~2.24 km/s，脉冲宽度40~80 ns，击靶压力为2.280~11.952 GPa。在回收的铝、铜和钢靶样品上观察到层裂现象。通过金相分析发现它们的破坏方式与在一般较长脉冲加载下的破坏方式相似，铝和铜以延性方式破坏；钢则以脆性方式破坏。一维和二维数值模拟结果表明通常的几种层裂判据在这个应力、应变和应变率范围内也基本上适用。     

CLIFFORD MARTINGALES Φ-EQUIVALENCE BETWEEN S（f） AND f^＊

ＣＬＩＦＦＯＲＤＭＡＲＴＩＮＧＡＬＥＳΦ－ＥＱＵＩＶＡＬＥＮＣＥＢＥＴＷＥＥＮＳ（ｆ）ＡＮＤｆ￥ＬＯＮＧＲＵＬＩＮ；ＱＩＡＮＴＡＯ（ＩｎｓｔｉｔｕｔｅｏｆＭａｔｈｅｍａｔｉｃｓ，ＡｃａｄｅｍｉａＳｉｎｉｃａ，Ｂｅｉｊｉｎｇ１０００８０，Ｃｈｉｎａ．）...     

一种新的$1/f$过程小波模型

给出了一种新的二进小波1/f过程模型,从理论上证明了一类谱指数为H的近似1/f过程可通过一簇平稳随机过程产生.由于所提方法利用了1/f过程小波系数的相关性,因而有效地减少了合成1/f过程的谱误差.数值实验结果表明,新模型很好地改进了已有模型.     

基于矩阵初等变换的n元函数极值的快速判别法

给出了 n元函数极值的一个充分条件 ,并结合矩阵的初等变换建立了 n元函数极值的一种快速判别法 ,最后给出了一个例子     

Synthesis and optoelectronic properties of silole‐containing polyfluorenes with binary structures

2,5‐Bis(2‐bromofluorene‐7‐yl)silole was prepared by a modified one‐pot synthesis with a reverse addition procedure, from which novel silole‐containing polyfluorenes with binary random and alternating structures (silole contents between 4.5 and 25% and high M_w up to 509 kDa were successfully synthesized. The well‐defined repeating unit of the alternating copolymer comprises a terfluorene and a silole ring. Optoelectronic properties including UV absorption, electrochemistry, photoluminescence (PL), and electroluminescence (EL) of the copolymers were examined. The different excitation energy transfers from fluorene to silole of the copolymers in solution and in the solid state were compared. The films of the copolymers showed silole‐dominant green emissions with high absolute PL quantum yields up to 83%. EL devices of the copolymers with a configuration of ITO/PEDOT/copolymer/Ba/Al displayed exclusive silole emissions peaked at around 543 nm and the highest EL efficiency was achieved with the alternating copolymer. Using the alternating copolymer and poly(9,9‐dioctylfluorene) as the blend‐type emissive layer, a maximum external quantum efficiency of 1.99% (four times to that of the neat film) was realized, which was a high efficiency so far reported for silole‐containing polymers. © 2007 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 45: 756–767, 2007     

On Two Parallel Matched Gratings Demodulation Method of Fiber Grating Strain Sensor

The method of demodulation with two parallel matched fiber Bragg gratings( FBGs)system is introduced to enlarge the range of strain that can be detected by the FBG sensor system.