Banach空间中N阶脉冲积分-微分方程边值问题的解

运用Monch不动点定理，获得了Banach空间中一类N阶非线性混合型脉冲积分-微分方程边值问题解的存在性．最后给出一个三阶无穷脉冲积分-微分方程边值问题的例子来说明文中所给的条件是合理的．     

C60基Ebselen衍生物：合成及尤其对鼠胸腺细胞增强保护效应

丙二酸酯衍生物2用2-氯硒基苯甲酰氯和2-(2-胺基乙氧基)乙醇为原料，经三步合成制得。2与C₆₀的Bingel环加成反应制得C₆₀基Ebselen衍生物3，产率为42% (基于已反应的C₆₀)，¹HNMR、¹³CNMR、IR、FAB-MS和元素分析鉴定了其结构。为了证实3对鼠胸腺细胞的活力具有增强效应，C₆₀衍生物4和2被选择，并采用与3相同的方法来处理鼠胸腺细胞，结果显示：3处理组的MTT(OD)值(0.335 ± 0.021)高于4处理组(MTT(OD): 0.283 ± 0.031)和2处理组(MTT(OD):0.247 ± 0.025)，表明3在促进鼠胸腺细胞活力方面优于2 和 4。     

Arsenic Speciation in Sargassum fusiforme by Microwave-Assisted Extraction and LC-ICP-MS

Sargassum fusiforme, the common Chinese edible seaweeds, was investigated for total arsenic concentration by ICP-MS and for individual arsenic species by LC-ICP-MS. For this purpose, a microwave-assisted procedure was used for the extraction of arsenic species in freeze-dried seaweed and an analytical procedure for the sensitive and efficient speciation of the arsenic species As(III), dimethylarsinic acid, monomethyl arsonic acid, As(V), arsenobetaine and arsenocholine was optimized. Arsenic compounds were extracted from the seaweed with a methanol/water mixture; the extracts were evaporated to dryness, redissolved in water, and chromatographed on an anion exchange column. The arsenic species in Sargassum fusiforme are abundant. In some sample, the majority of arsenic compounds detected in the extracts were inorganic species, with a predominance of As (V). In addition, some significant amounts of unidentified arsenic compounds were also observed in the extracts.

     

基于完备IMTL代数的L模糊粗糙集

IMTL代数是一类重要的非经典逻辑代数,基于IMTL代数的L模糊粗糙集可以刻画信息系统中具有不完备性、模糊性与不可比较性的信息.本文讨论了基于完备IMTL代数的L模糊粗糙集的表示定理,还讨论了此种L模糊粗糙集的上下近似算子的性质以及近似算子的公理化定义方法.     

Synthesis and characterization of star graft copolymers with asymmetric mixed “V‐shaped” side chains via “click” chemistry on a hyperbranched polyglycerol core

The star graft copolymers composed of hyperbranched polyglycerol (HPG) as core and well defined asymmetric mixed “V‐shaped” identical polystyrene (PS) and poly(tert‐butyl acrylate) as side chains were synthesized via the “click” chemistry. The V‐shaped side chain bearing a “clickable” alkyne group at the conjunction point of two blocks was first prepared through the combination of anionic polymerization of styrene (St) and atom transfer radical polymerization of tert‐butyl acrylate (tBA) monomer, and then “click” chemistry was conducted between the alkyne groups on the side chains and azide groups on HPG core. The obtained star graft copolymers and intermediates were characterized by gel permeation chromatography (GPC), GPC equipped with a multiangle laser‐light scattering detector (GPC‐MALLS), nuclear magnetic resonance spectroscopy and fourier transform infrared. © 2009 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 47: 1308–1316, 2009     

Magnetically tunable silicon-ferrite photonic crystals for terahertz circulator

The gyromagnetic properties of ferrite materials and the nonreciprocal property of a silicon-ferrite photonic crystal cavity are investigated in the terahertz region. Through the structure optimization and analysis of defect mode coupling, we design a magnetically tunable circulator, of which central operating frequency can be tuned from 180 to 205 GHz and the maximum isolation is 65.2 dB. Moreover, the further study shows that the gyrotropy, dispersion, and ferromagnetic loss of ferrite materials under the different external magnetic fields greatly affect the transmission and isolation property of this device. This circulator is flexible to realize functions of controllable splitting, routing, filtering and isolation by changing the external magnetic field for the THz applications.     

单晶Si Nd∶YAG激光连续退火的数值计算

应用固相外延模型来模拟单晶Si的连续Nd∶YAG激光退火过程,在低功率密度连续激光退火下,用准静态模型模拟辐照区向非辐照区的径向传导散热.在数值计算中,应用部分线性法处理非线性非齐次热传导方程,得到相应的隐格式差分方程,再用追赶法求解隐格式差分方程,得出绝热边界条件下的温度的时间和空间分布,从而得出激光退火的再结晶厚度.当激光波长λ=1.06μm、功率密度i0=700W/cm2,预热温度T0=523K时,经过0.7秒,表面温度度升到1 290K左右,再结晶厚度约为0.5μm.     

有限维模李超代数$W(m,n,l,\underline{t})$的$\Theta$-型导子与导子超代数

本文总设$F$是$p>2$的域,我们在域$F$上构造了有限维模李超代数$W(m,n,l,\underline{t})$, 定义了$W(m,n,l,\underline{t})$的$\Theta$-型导子,进而确定了它导子超代数.