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961.
This article describes the technique of fast atom bombardment mass spectrometry (FAB MS) and its applications to the analysis of organometallic and coordination complexes. Sections on ion generation and matrices are followed by a Periodic Group-based review of FAB MS results obtained from Transition Metal and Main Group compounds, organometallic cluster carbonyls and their derivatives, and salts of poly-oxo-anions. The literature has been surveyed from 1981 to approximately mid-1986. 相似文献
962.
Stephen J. Gardiner 《Advances in Mathematics》2007,214(1):417-436
This paper answers a question of Fuglede about minimal positive harmonic functions associated with irregular boundary points. As a consequence, an old and central problem of fine potential theory, concerning the Riesz decomposition, is resolved. Namely, it is shown that, on certain fine domains, there exist positive finely superharmonic functions which do not admit any positive finely harmonic minorant and yet are not fine potentials. 相似文献
963.
A. Bartnik H. Fiedorowicz R. Jarocki L. Juha J. Kostecki R. Rakowski M. Szczurek 《Applied physics. B, Lasers and optics》2006,82(4):529-532
The first results of experiments on direct photo-etching of heated PTFE using a 10 Hz X-ray source based on a laser-irradiated gas puff target are presented. X-ray radiation in the wavelength range from 6 to 20 nm was produced as a result of irradiation of a double-stream gas puff target with Nd:YAG laser pulses of energy 0.8 J and time duration 3 ns. The resulting X-ray pulses with energy of about 100–200 mJ were used to irradiate samples of PTFE to create microstructures by direct photo-etching. Strong enhancement of the photo-etching process was observed for samples heated up to 300 °C. PACS 52.38.Ph; 81.65.Cf; 61.82.Pv 相似文献
964.
The possibility of ferromagnetic (FM) and antiferromagnetic (AFM) phase transitions in symmetric nuclear matter is analyzed
within the framework of a Fermi liquid theory with effective Gogny interaction. It is shown that, at some critical density,
nuclear matter with the D1S effective force undergoes a phase transition to the AFM spin state (opposite directions of neutron
and proton spins). The self-consistent equations of spin-polarized nuclear matter with the D1S force have no solutions corresponding
to FM spin ordering (the same direction of neutron and proton spins) and, hence, the FM transition does not appear. The AFM
spin polarization parameter is found for zero and finite temperature. It is shown that the AFM spin polarization parameter
of partially polarized nuclear matter at low enough temperatures increases with temperature. The entropy of the AFM spin state
for some temperature range is larger than the entropy of the normal state. Nevertheless, the free energy of the AFM spin state
is always less than the free energy of the normal state, and the AFM spin-polarized state is preferable for all temperatures
below the critical temperature.
The text was submitted by the authors in English. 相似文献
965.
966.
Ph. Laurent M. Abgrall Ch. Jentsch P. Lemonde G. Santarelli A. Clairon I. Maksimovic S. Bize Ch. Salomon D. Blonde J.F. Vega O. Grosjean F. Picard M. Saccoccio M. Chaubet N. Ladiette L. Guillet I. Zenone Ch. Delaroche Ch. Sirmain 《Applied physics. B, Lasers and optics》2006,84(4):683-690
In this paper we describe the cold atom clock PHARAO, designed for microgravity operation. All elements of the PHARAO engineering model have been manufactured and delivered to CNES, the French space agency. We present the clock design, its main characteristics, and initial science operation. PHARAO is one of the main components of the Atomic Clock Ensemble in Space payload that is scheduled to fly on board the International Space Station in 2010. PACS 07.87.+v; 06.30.Ft; 95.55.Sh; 32.80.Pj 相似文献
967.
We report a highly-efficient, high-power, single-frequency Nd:YVO4 master-oscillator power-amplifier with near-diffraction-limited output beam quality. A diode-pumped Nd:YVO4 ring laser incorporating a passive method for suppressing axial-mode-hopping was employed as the master-oscillator, and was amplified by a three-stage diode-end-pumped Nd:YVO4 amplifier, yielding 79 W of output with an extraction efficiency of 29%. The overall power gain was 15 dB for an input power from the master-oscillator of 2.4 W, and the M2 parameter was less than 1.5 at the maximum power. The prospects for a further increase of power and brightness via this approach are considered. PACS 42.55.Xi; 42.60.Da; 42.60.Jf 相似文献
968.
J. Bartella K. Kastner K. Röll und K. -H. Schuller 《Fresenius' Journal of Analytical Chemistry》1987,329(2-3):289-291
Summary Besides functional behaviour of coatings their resistivity against corroding attack is a crucial criterion for quality. The application of special corroding and abrading tests yields after short times predictions about stability of the product in practical use. A number of tests have been applied to thin magnetic storage media. Besides tests of function and visual observations with light- and scanning electron microscopes, AES- and XPS-investigations were applied to discuss corrosion resistivity. 相似文献
969.
Cynthia J. Burrows Richard A. Sauter 《Journal of inclusion phenomena and macrocyclic chemistry》1987,5(1):117-121
New synthetic hosts have been designed incorporating two molecules of cholic acid linked by a rigid diamine. Proton NMR studies indicate that the compounds exist in a rigid conformation with the steroid hydroxyl groups intramolecularly hydrogen-bonded. Heat or addition of methanol leads to conformational isomerism due to insertion of methanol into the cavity.A preliminary report of this work was presented at the 4th International Symposium on Inclusion Phenomena, July 20–25, 1986, Lancaster, U.K. 相似文献
970.
The trisilanol 1,3,5‐(HOi‐Bu2Si)3C6H3 ( 7 ), prepared in three steps from 1,3,5‐tribromobenzene via the intermediates 1,3,5‐(Hi‐Bu2Si)3C6H3 ( 8 ) and 1,3,5‐(Cli‐Bu2Si)3C6H3 ( 9 ) forms an equimolar complex with trans‐bis(4‐pyridyl)ethylene (bpe), 7 ·bpe, whose structure was investigated by X‐ray crystallography. The hydrogen‐bonded network features a number of SiO? H(H)Si and SiO? H hydrogen bridges. Evidence was found for cooperative strengthening within the sequential hydrogen bonds. Copyright © 2007 John Wiley & Sons, Ltd. 相似文献