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111.
Cr-doped mullites were prepared from single-phase precursors containing up to 9.60 wt% Cr2O3 using a sol-gel technique followed by thermal treatment. Particle induced X-ray emission spectroscopy and X-ray powder diffraction were used to characterize the samples. Mullites were orthorhombic, space group Pbam. Cr doping caused the increase of unit-cell parameters. Strongest expansion was noticed along c-axis followed by a and b (Δc/c=0.089, Δa/a=0.061, Δb/b=0.045% per mole Cr2O3). A second phase, namely θ-(Al,Cr)2O3, was revealed by XRD in the sample containing 9.60 wt% Cr2O3. The structure of mullites was refined by the Rietveld method, location of Cr3+ was performed by the EPR spectroscopy. At low chromium doping level (Cr2O3 content less than ∼5 wt%) Cr3+ ions were substituted for Al3+ in the AlO6 octahedra of the mullite structure (M1 site). For higher doping level, Cr3+ ions were additionally substituted for Al3+ in the AlO6 octahedra of the second phase [θ-(Al,Cr)2O3 at 1400 °C, or α-(Al,Cr)2O3 at 1600 °C] which segregated in the system. Substitution of Cr3+ for Al3+ on M1 site in the mullite structure resulted in increase of average distances in (M1)O6 octahedron and decrease of average distances in T*O4 tetrahedron, while average distances in TO4 tetrahedron stayed almost constant. 相似文献
112.
113.
Peter C. Bell 《The Journal of the Operational Research Society》1989,40(7):615-624
Many writers and practitioners have mentioned the difficulties that result from randomness in visual interactive simulation or animated simulation modelling. This paper discusses the use of VIS to model transient system behaviour, and proposes some approaches to stochastic VIS modelling which may be helpful in overcoming the difficulties. 相似文献
114.
Peter Schatte 《Mathematische Nachrichten》1989,140(1):249-250
115.
Phil Diamond Peter Kloeden Victor Kozyakin Alexei Pokrovskii 《Mathematische Nachrichten》1998,191(1):59-81
The finiteness of computer arithmetic can lead to some dramatic differences between the behaviour of a continuous dynamical system and a computer simulation. A thorough rigorous theoretical analysis of what may or what does happen is usually extremely difficult and to date little has been done even in relatively simple contexts. The comparative behaviour of a rotation mapping in the plane and on a uniform lattice in the plane is one such example. Simulations show that the rounding operator applied to a planar rotation mapping more or less preserves the qualitative behaviour of the original mapping, whereas the application of the truncation operator to a planar rotation can lead to quite different dynamical features. In this paper a theoretical justification of the properties of the planar rotation mappings under truncation to a, uniform integer lattice is provided, in particular properties of boundedness and dissipativity are investigated. 相似文献
116.
I Cserpan M Kalman M L Tj?rnhammar A Simoncsits 《Acta chemica Scandinavica (Copenhagen, Denmark : 1989)》1991,45(3):265-272
A general method to convert single-stranded, chemically synthesized oligonucleotides into cloned duplexes is described. Oligonucleotides supplied with 3'-terminal extensions that are complementary to 3'-protruding ends obtained by certain restriction enzymes can be cloned either directly or with the help of an adapter molecule into double-stranded vectors. Two methods have also been developed for consecutive cloning applications. According to these methods, the synthetic oligonucleotides (and their enzymatically prepared complementary strands) are joined, one after the other, inside a cloning vector, each joining requiring one cloning step. Synthetic genes are thus built up from oligonucleotides corresponding to only one strand of the DNA. The sequential assembly of the cloned duplex takes place in the 5' to 3' direction. Each oligonucleotide is supplied with a four-nucleotide-long 3'-terminal extension, but this sequence is eliminated when the joining takes place, leaving no limiting sequence between the oligonucleotides. The two consecutive cloning methods, the adapter and the polycloning site methods, are illustrated by the assembly of short artificial genes. 相似文献
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Peter Wiesen 《Angewandte Chemie (Weinheim an der Bergstrasse, Germany)》1994,106(6):731-731