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981.
982.
983.
A high-performance liquid chromatographic procedure was developed for the quantitation of homoharringtonine in plasma. Harringtonine was used as an internal standard, and 1 ml of sample was required. The single-step extraction with dichloromethane resulted in almost 100% recovery for homoharringtonine and harringtonine. Analysis was performed on a reversed-phase CN column with amperometric detection. Chromatography was completed in 12 min. At an oxidation potential of +1.0 V, the detection limit was 1 ng/ml at a signal-to-noise ratio of 2. The mean analytical recovery for homoharringtonine was 99.5%. The within-run precision and between-run precision were both less than 11%. The method is equally applicable for plasma or serum, and it has been demonstrated to be applicable for study of the pharmacokinetics of homoharringtonine in patients suffering from acute non-lymphocytic leukaemia. 相似文献
984.
E. Mathieu Y. Foucher P. Dellamonica J. P. Daures 《Methodology and Computing in Applied Probability》2007,9(3):389-397
In AIDS control, physicians have a growing need to use pragmatically useful and interpretable tools in their daily medical
taking care of patients. Semi-Markov process seems to be well adapted to model the evolution of HIV-1 infected patients. In
this study, we introduce and define a non homogeneous semi-Markov (NHSM) model in continuous time. Then the problem of finding
the equations that describe the biological evolution of patient is studied and the interval transition probabilities are computed.
A parametric approach is used and the maximum likelihood estimators of the process are given. A Monte Carlo algorithm is presented
for realizing non homogeneous semi-Markov trajectories. As results, interval transition probabilities are computed for distinct
times and follow-up has an impact on the evolution of patients.
相似文献
985.
T. Hansel J. Müller C. Falldorf C. von Kopylow W. Jüptner R. Grunwald G. Steinmeyer U. Griebner 《Applied physics. B, Lasers and optics》2007,89(4):513-516
Digital holographic shape measurements using femtosecond laser pulses are reported. For contouring of very fast moving objects,
the simultaneous generation of at least two spectrally separated ultrashort pulses is required. To deliver this particular
spectral signature at high pulse energies, a chirped-pulse Ti:sapphire laser amplifier was modified to emit two spectrally
separated pulses with energies above 1 μJ each. The wavelength separation of these pulses was adjustable within the 50 nm
gain bandwidth, cutting out two distinct wavelength peaks by a variable double-slit assembly in a prism sequence. A Michelson-type
interferometer was employed to perform the two-wavelength contouring. The phases of the holograms and the phase differences
are calculated numerically, which allow us to deduce the contour lines of the topology of the object. The suitability of the
light source for digital holography is demonstrated with contouring of stationary objects and the potential for high-speed
applications is indicated.
PACS 42.40.-i; 42.60.By 相似文献
986.
A. M. Kharitonov 《Thermophysics and Aeromechanics》2007,14(1):3-11
Sergey Alekseevich Khristianovich is one of the famous Russian mechanical engineers of the 20th century together with N.E.
Zhukovsky, S.A. Chaplygin, N.E. Kochin, and others. He made an immense contribution to some aspects of mechanics, such as
aerogasdynamics, rock mechanics, theory of plasticity, filtration theory, and environmental power engineering. All this was
preceded by a long, hard, and fruitful life full of outstanding events. 相似文献
987.
988.
There are many advantages in being able to perform positron annihilation lifetime spectroscopy (PALS) using a variable energy positron beam, the most obvious being the easy identification of different defect types at different depths. The difficulty in conducting variable energy (VE) PALS studies lies in the fact that a “start” signal is required to signal the entry of the positron into the target. Two methods have been used to overcome this problem, namely the bunching technique, which employs radio frequency (RF) cavities and choppers, and secondly the use of secondary electrons emitted from the target. The latter technique is in terms of experimental complexity much simpler, but has in the past suffered from poor time resolution (typically ∼500 ps). In this work, we present a series of computer simulations of a design based on the secondary electron emission from thin C-foils in transmission mode which shows that significant improvements in time resolution can be made with resolutions ∼200 ps being in principle possible. 相似文献
989.
Masanobu Haraguchi David F. P. Pile Toshihiro Okamoto Masuo Fukui Dmitri K. Gramotnev 《Optical Review》2006,13(4):228-230
We have numerically shown the existence of coupled wedge plasmons (CWPs) which propagates along a nano gap of a twin metal
wedge. The CWPs are formed by wedge plasmons which can interact with each other. The dispersion relations of the wavenumber,
propagation distance, and beam area of CWPs, are described and show that the characteristics of CWPs are similar to those
of wedge plasmons and of gap plasmons. We also propose a new plasmon waveguide composed of twin metal wedges with a nano gap. 相似文献
990.
V. P. Nekhoroshev Yu. P. Turov A. V. Nekhorosheva V. D. Ogorodnikov K. N. Gaevoi 《Russian Journal of Applied Chemistry》2006,79(5):833-840
The composition and structure of low-molecular-weight products of thermal oxidative degradation of atactic polypropylene were studied. 相似文献