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Conclusions Reaction between equimolecular amounts of an alkyl bis-1-aziridinylphosphinite and phenol leads to an alkyl phenyl 1-aziridinylphosphonite, the addition of sulfur to which gives an alkyl phenyl 1-aziridinylphosphonothioate.Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 4, pp. 881–883, April, 1969.We thank L. Kulakova for determining the IR spectra. 相似文献
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V. P. Gubskaya L. N. Islamova G. M. Fazleeva Sh. K. Latypov A. F. Saifina A. T. Gubaidullin D. R. Sharafutdinova I. A. Nuretdinov O. G. Sinyashin 《Russian Chemical Bulletin》2016,65(6):1556-1565
New chromatographically pure monoand hexamethanofullerenes C60 and C70 containing active allylic groups were synthesized by Bingel—Hirsch reaction. These compounds are promising for the studies of biological activity, as well as for obtaining on their basis new fullerenecontaining materials. The purity and composition of the synthesized compounds were confirmed by MALDI-TOF mass spectrometry and HPLC, their structure was established by 1H and 13C NMR spectroscopy and X-ray diffraction. 相似文献
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Gubskaya VP Berezhnaya LSh Gubaidullin AT Faingold II Kotelnikova RA Konovalova NP Morozov VI Litvinov IA Nuretdinov IA 《Organic & biomolecular chemistry》2007,5(6):976-981
Two nitroxide methanofullerenes was synthesized for the first time, and their structures and biological activities studied. It was shown by X-ray single crystal analysis that the methanofullerene with two nitroxide groups forms a 1 : 2 inclusion complex with chloroform and has a nearly tetrahedral (diamond-like) arrangement of fullerene-fullerene interactions in the crystal. For the first time, it has been found that malonate nitroxide methanofullerene in combination with the known anticancer drug cyclophosphamide (CPA) shows high antitumor activity against leukemia P-388. 相似文献
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D. R. Sharafutdinova I. Kh. Rizvanov G. M. Fazleeva V. P. Gubskaya I. A. Nuretdinov 《Journal of Analytical Chemistry》2011,66(14):1441-1444
Some compounds containing mono- and polynitroxide radicals have been investigated and characterized by electron ionization
(EI), chemical ionization (CI), and matrix-assisted laser desorption-ionization (MALDI) mass spectrometry. Some characteristics
of the mass spectra of these radicals are demonstrated. It was found that, under CI and MALDI conditions, ions [M+nH]+ are formed along with monoprotonated molecules [M+H]+, depending on the type of the radical n = 2–5. 相似文献