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91.
Katalin E. Kövér Dušan Uhr?&#x;n Victor J. Hruby 《Journal of magnetic resonance (San Diego, Calif. : 1997)》1998,130(2):162-168
A pulsed field gradient version of the sensitivity-enhanced 2D TOCSY experiment is proposed which yields high-quality spectra with improved sensitivity and a minimum of two scans pert1increment. For rapid acquisition of 1D TOCSY spectra, the 1D DPFGSE–TOCSY experiment was modified to include phase-encoded multiple-selective excitation followed by a simple spectral editing. Combination of these two building blocks is used in a sensitivity-enhanced 2D analog of the 3D TOCSY–TOCSY experiment which provides an efficient tool for resolving severely overlapped signals of oligomers in short experimental time. 相似文献
92.
超重元素(新核素)合成研究进展情况分析和展望 总被引:2,自引:0,他引:2
本文在介绍和分析国际、国内在超重元素(新核素)合成实验研究与理论研究进展情况的基础上对我国今后如何从理论与实验的结合上开展超重元素(核)合成研究工作提出一些看法和建议,提供讨论。 相似文献
93.
Olga Ordeig Craig E Banks Trevor J Davies F Javier del Campo Francesc Xavier Mu?oz Richard G Compton 《Analytical sciences》2006,22(5):679-683
Gold ultra-microelectrode arrays are used to explore the electrochemical oxidation of hydroxide ions and are shown to be analytical useful. Two types of ultra-microelectrode arrays are used; the first consist of 256 individual electrodes of 5 microm in radius, 170 of which are electrochemically active in a cubic arrangement which are separated from their nearest neighbour by a distance of 100 microm. The second array compromises 2597 electrodes of 2.5 microm in radius and of which 1550 of which are electrochemically active in a hexagonal arrangement separated by the nearest neighbour by 55 microm. Well defined voltammetric waves are found with peak currents proportional to the concentration of hydroxide ions in the range 50 microM to 1 mM. Detection limits of 20 microM using the 170 ultra-microelectrode and 10 microM with the 1550 ultra-microelectrode array are shown to be possible but with a higher sensitivity of 4 mA M(-1) observed using the 1550 ultra-microelectrode array compared to 1.2 mA M(-1) with the 170 ultra-microelectrode array. 相似文献
94.
Ivan Gutman Sabina Gojak Niko Radulovi? Boris Furtula 《Monatshefte für Chemie / Chemical Monthly》2006,46(2):277-284
In a recent work it was demonstrated that in linear hexagonal chains the distribution of π-electrons into rings (as computed
by means of the Randić–Balaban method) is uniform, irrespective of the nature of the terminal fragments. We now establish that an analogous, yet somewhat
more complex, uniformity in the π-electron distribution exists also in double linear hexagonal chains, as well as in some
other benzenoid systems. 相似文献
95.
Thin films of silicon oxynitride have largely replaced pure silicon oxide films as gate and tunnel oxide films in modern technology due to their superior properties in terms of efficiency as boron barrier, resistance to electrical stress and high dielectric strength. A single chamber system for plasma enhanced chemical vapor deposition was employed to deposit different films of SiOxNyHz with 0.85 < x < 1.91. All films were previously characterized by Rutherford back-scattering and infrared spectroscopy to determine the stoichiometry and the presence of various bonding configurations of constituent atoms. We used X-ray reflectivity to determine the electron density profile across the depth, and we showed that the top layer is densified. Moreover, grazing incidence small-angle X-ray scattering was used to study inhomogeneities (clustering) in the films, and it is shown that plate-like inhomogeneities exist in the top and sphere-like particles at the bottom part of the film. Their shape and size depend on the stoichiometry of the films. 相似文献
96.
Zhi-Hui Su Munehiro Okamoto Osamu Tominaga Katsumi Akita Noboru Kashiwai Y?ki Imura Tooru Ojika Yoshiyuki Nagahata Syozo Osawa 《Proceedings of the Japan Academy. Series B, Physical and biological sciences》2006,82(7):232-250
An approach to deduce the mechanism of stabilization of the hybrid-derived populations in the Ohomopterus ground beetles has been made by comparative studies on the phylogenetic trees of the mitochondrial and nuclear DNA. A phylogenetic tree based on the internal transcribed spacer (ITS) of nuclear ribosomal gene roughly reflects the relations of morphological species group, while mitochondrial NADH dehydrogenase subunit 5 (ND5) gene shows a considerable different topology on the tree; there exist several geographically-linked lineages, most of which consist of more than one species. These results suggest that the replacement of mitochondria has occurred widely in the Ohomopterus species. In most cases, hybridization is unidirectional, i.e., the species A (♂) hybridized with another species B (♀) and not vice versa, with accompanied replacement of mitochondria of A by those of B. The results also suggest that partial or complete occupation of the distribution territory by a hybrid-derived morphological species. The morphological appearance of the resultant hybrid-derivatives are recognized as that of the original species A. Emergence of a morphological new species from a hybrid-derived population has been exemplified. 相似文献
97.
Xiao-jing Cai Quan-sen Jiu Chun-yan Xue 《应用数学学报(英文版)》2007,23(4):637-650
In this paper,the Dirichlet problem of Stokes approximate of non-homogeneous incompressibleNavier-Stokes equations is studied.It is shown that there exist global weak solutions as well as global andunique strong solution for this problem,under the assumption that initial density ρ_0(x)is bounded away from0 and other appropriate assumptions(see Theorem 1 and Theorem 2).The semi-Galerkin method is applied toconstruct the approximate solutions and a prior estimates are made to elaborate upon the compactness of theapproximate solutions. 相似文献
98.
M. Smi?anská J. Hladky M. Novák M. Vecko A. N. Aleev V. A. Arefiev V. P. Balandin V. K. Berdyshev V. K. Birulev A. S. Chvyrov et al. 《Czechoslovak Journal of Physics》1990,40(12):1293-1305
We present results of the exclusive diffractive reaction np 0K0p at 0·08 < |t|< 0·53 GeV2/c2 and momenta between 30–70 GeV/c at the Serpukhov neutron beam. Thet-dependence is exp (Bt) withB= 11·4± 2·3 (GeV/c)–2 and it exhibits the diffractive minimum at ¦t¦ 0·28 GeV2/c2 for 0K0 massesM < 1·8 GeV/c2.B decreases with increasingM. Correlation with the beam direction is observed in the rest frame of the 0K0 system: the cross section rises for the forward-going 0. The rise is more pronounced for higherM. The cross section of reaction np 0K0p for 0<|t|< 0·53 GeV2/c2 is 10·3 ± 2·5 ± 2·8 b. 相似文献
99.
N. M. Agababyan I. V. Ajinenko Yu. A. Belokopytov K. S. Belous H. Boettcher F. Botterweck M. M. Chapkin P. V. Chliapnikov F. Crijns A. De Roeck E. A. De Wolf K. Dziunikowska A. M. F. Endler A. Eskreys Z. C. Garutchava P. van Hal T. Haupt A. I. Katargin W. Kittel S. S. Megrabyan F. Meijers A. B. Micha?owska V. I. Nikolaenko K. Olkiewicz V. M. Ronjin R. Rosmalen H. M. T. Saarikko L. Scholten E. K. Shabalina J. Stepaniak O. G. Tchikilev V. A. Uvarov F. Verbeure R. Wischnewski S. A. Zotkin Y. V. Yarba EHS-NA Collaboration 《Zeitschrift fur Physik C Particles and Fields》1990,46(3):387-395
We report on a study of ρ0, ρ+, ω, \(\bar K^{*0} (892)\) andK *0 (892) inclusive production in π+ p interactions at 250 GeV/c, for ρ+, \(\bar K^{*0} (892)\) for the first time in a π+ p experiment. The data are compared withK + p data in the same experiment, with results of other experiments and with quark-parton models. Interesting differences are found between ρ+,0 and ω production. 相似文献
100.