固体渗硼的铬不锈钢组织和性能

为增进不锈钢性能,进行了不锈钢固体渗硼试验。结果表明;渗层表面形成了FeB、Fe_zB相。并随工艺变化可调整其相对含量。此渗层可以极大地提高耐磨性。但耐蚀性能降低。     

Qualitative and Quantitative Analysis of Alkaloids in Cortex Phellodendri by HPLC-ESI-MS/MS and HPLC-DAD

A combined method of high performance liquid chromatograph-elecrtrospray-ionization mass spectrometer(HPLC-ESI-MS/MS) coupled with a photodiode array detector(HPLC-DAD) and principal component analysis(PCA) was applied to the qualitative and quantitative analyses of alkaloids in Cortex Phellodendri(CP) samples, and to the differentiation of two species of CP, Cortex Phellodendri Chinensis(CPC) and Cortex Phellodendri Amurensis(CPA). Twenty-two peaks appeared in the HPLC-MS base peak chromatogram of CP detec...     

原子吸收光谱法测定12种中成药的10种无机元素

本文测定了12种中成药中10种无机元素,证明中成药含有丰富的无机元素,探讨了无机元素与中药的药效关系,结果表明中成药中的无机元素与药效有一定的关连。并且无机元素含量的多少也与药效有密切关系,为了保证中成药的药效,无机元素的含量多少也应该有合理的控制线,控制线的制订有待今后探讨。     

EAST 2kW/4K氦制冷机检漏及真空系统运行情况

介绍EAST超导托卡马克2kW/4K氦制冷机的检漏方法及检漏过程,制冷机的真空系统及运行情况,指出关于大型氦低温系统检漏要注意的一些问题。     

Spectroscopic characteristics of Yb^3＋：LiLa（WO4）2 crystal

The spectroscopic characterization and fluorescence dynamics of Yb^3＋：LiLa（WO4）2 crystal are investigated. The Yb^3＋：LiLa（W04）2 crystal exhibits a broad absorption and emission spectral bands, large absorption and emission cross sections, and moderate fluorescence lifetime. Blue light emission around 480 nm is observed at 10 K and is demonstrated through cooperative upconversion from the deexcitation of excited Yb^3＋-Yb^3＋ pairs.     

Hyperspectral imaging technology for determination of dichlorvos residue on the surface of navel orange

A hyperspectral imaging system is developed to detect dichlorvos residue on the surface of navel orange.After acquiring hyperspectral images of 400 navel oranges,the actual content of dichlorvos residue is measured by gas chromatography.Optimal wavelengths are extracted using the regression coefficients of partial least squares （PLS）,and a PLS model with 12 factors is established.In the prediction set of 0.2282 11.652-mg/kg pesticide residue,the correlation coefficient and the root mean standard error are 0.8320 and 1.3416,respectively.The hyperspectral imaging technology can meet the requirement of online fast nondestructive detection.     

Solid-phase Synthesis of Diethyl Trans-1-Aklenephosphonates Using Polymer-bound α-Diethoxyphosphoryl Methyl Selenide

Polymer-supported organic reagents have been applied to the rapid preparation of smallorganic molecules because they can provide attractive and practical methods forcombinatorial chemistry and solid-phase synthesis1. Vinylphosphonates bearing anelectron withdrawing groups at the α-position are versatile intermediates for the synthesisof some hetero- and carbocyclic compounds2. Many methods have been developed forpreparing their parent compounds, 1-alkenephosphonates. Among those methods, anim…     

一种寻求层状流动新解的方法

复杂层状流动是流体力学中的一类典型的流动。一般而言，流体力学中有两种特殊的流动：一种是Beltrami流动，另一种就是层状流动。对于前者，已经讨论过很多；但是后者的精确解却很难获得，这是因为很难解这种流动的Navier-Stokes方程或Euler方程。从不可压缩条件出发，如果让速度的形式满足一些特殊的条件，可以得到关于这种流动的某些新的精确解，例如发现一种间歇流精确解。     

Simultaneous spectrophotometric determination of four preservatives in foodstuffs by multivariate calibration and artificial neural networks

Benzoic acid(BA),methylparaben(MP),propylparaben(PP)and sorbic acid(SA)are food preservatives,and they have well defined UV spectra.However,their spectra overlap seriously,and it is difficult to determine them individually from their mixtures without preseparation.In this paper,seven different chemometric approaches were applied to resolve the overlapping spectra and to determine these compounds simultaneously.With respect to the criteria of%relative prediction error(RPE)and%recovery, principal component...     

DIAGNOSTICS OF ARC PLASMA BY MOIRE DEFLECTOMETRY

This paper presents a new method to diagnose the welding arc temperaturefield on the basis of plasma physics,Talbot effect and Moire techniques.This method hasadvantages of immunity to mechanical shock and vibration,tunable sensitivity and conside-rable simple optical system.