A method to quantitatively estimate rainfall rate above water surface based on different spectra shapes generated by rainfall

A method combined with the nonlinear least-square regression to quantitatively estimate rainfall rate over water surface from the different spectrum shapes generated by rainfall in some frequency bands was presented.About 2000 min spectrum data generated by rainfall have been collected in an open-lake in Xiamen city.As a result,the spectrum shape in 15-30 kHz is fitted to log-linear law which allows classification of rain into three categories from the spectrum slope:no rain,drizzle(rainfall rate>10 mm/h)and heavy rain(rainfall rate>10 mm/h).Then,rainfall detection is made and rainfall rate is quantified in drizzle time with Logistic model in the frequency bands of 2-15 kHz,and the rainfall rate in heavy rainfall also quantified with log-linear regression.Finally,all measured spectrum data are used to calculate rainfall rate with the algorithm.The results show that the estimated rainfall rates are comparably coincident with the synchronously measured ones.The average error of accumulative rainfall per min is only l%-4%.     

H9N2亚型禽流感病毒细胞适应株细胞致病性和HA、NA基因序列分析

对分离自中国南方的H9N2亚型禽流感病毒A/Chicken/Guangxi/KMⅢ/99(H9N2)进行了MDCK细胞的连续传代和NA基因序列的初步分析.研究发现,病毒接种细胞36 h左右出现细胞病变(CPE),细胞肿胀变圆,聚集,脱落.流感病毒经MDCK细胞连续传代19代后,HA效价与亲代病毒相当.将传代获得的第19代病毒进行基因克隆,与亲代病毒进行序列比较,发现经传代后其HA1羧基端的分子特征是:R-S-S-R,仍属于非低致病力毒株.     

Antitumor Comparison of Three α-N-Heterocyclic Thiosemicarbazone Derivatives'Crystal Structures of Bis(2-acetylpyridine)thiocarbonohydrazone and Bis(imidazole-2-carboxaldehyde)thiocarbonohydrazone

T A series of ligands,HL1(2-acetylpyridine thiosemicarbazone),H2L2(bis(2-acetylpyridine)thiocarbonohydrazone)and H2L3(bis(imidazole-2-earboxaldehyde)thiocarbonohydrazone)was synthesized.H2L2 and H2L3 were characterized by elemental analysis,IR spectra and singlecrystal X-ray diffraction studies.Hydrogen bonds link different components to stabilize the crystal structure in the two ligands.To comprehend the structure-activity relationship well,the three ligands are all tested against human K562 leucocythemia cell line with IC50 analysis.Different substituent groups on the ligands show different levels of antitumor activity.By comparison with the other species studied,H2L2 with thiocarbonohydrazone along with 2-acetylpyridine is the most active compound with ICs0=2.48 μM.     

新型胃动力药盐酸伊托必利的结构分析

本文以ＵＶ、ＦＴＩＲ、＾１Ｈ－ＮＭＲ、＾１３Ｃ－ＮＭＲ、ＦＡＢＭＳ等现代分析手段，对国内试制的新型胃动力药盐酸伊托必利的化学结构进行了分析鉴定。根据谱带与结构的对应关系，确证其结构与国外已报道的结构一致并对上述各种谱的谱带进行了全面的归属     

内蒙古段黄河水系放射性水平调查研究

给出了内蒙古段黄河水平中总α，总β，＾９０Ｓｒ，＾１３７Ｃｓ，＾４０Ｋ，＾３Ｈ，＾２１０Ｐｂ，＾２１０Ｐｏ，＾２３８Ｕ，＾２３２Ｔｈ、＾２２６Ｒａ放射性水平，结果基本为正常水平，找出了污染源，为内蒙古段黄河水中放射性监督监测建立了全面的背景材料。     

Tb(III) Speciation in Human Blood Plasma by Computer Simulation

With the wide application of rare earth fertilizer and medicines1, more and more rare earths enter into environment, and also into human body via food chain. Now it is very urgent to study the biological effect of rare earths on human health and environment. After entering into human body by whatever route, lanthanide ions are transported to secondary deposition sites mainly via the plasma in the blood stream. So it is very important to study lanthanides speciation in human blood plasma. Becau…     

Jordan标准形定理的初等变换证明

本文对 Jordan标准形定理给出了一种使用初等变换的证明 ,直观意义明显、易于理解 ,可用于线性代数教学 .     

高功率毫米波圆波导TM01—TE11模式变换分析

 在数值研究高功率毫米波TM₀₁—TE₁₁光滑弯曲圆波导模式变换的基础上，对弯曲波导的几何结构进行了优化分析。在模式耦合理论的基础上，优化出了比较好的几何结构，并发现了圆波导半径、弯曲圆波导曲率和频率以及频带宽度之间的变化规律。以此数据设计的模式变换器的转换效率可达99%，带宽超过29.8%。     

具有渐近平均跟踪性质的系统

简记渐近平均跟踪性质为AASP.对于紧致度量空间上的连续映射f,证明了:(1)f有AASP当且仅当其逆极限空间上的移位映射有AASP;(2)若f有AASP且是等度连续的,则f是极小同胚.此外,讨论了AASP的拓扑共轭不变性.     

Synthesis, structural characterization and properties of a 3D infinitely extended structural rare earth coordination compound of K3{[Sm(H2O)7]2Na[α-SiW11O39Sm(H2O)4]2}·14 H2O

A 3D infinitely extended structural rare earth coordination compound with a formula of K3{[Sm(H2O)7]2Na[α-SiW11O39Sm(H2O)4]2}·14H2O has been synthesized by reaction of Sm2O3, HClO4, NaOH with α-K8SiW11O39·nH2O, and characterized by IR,UV spectra, ICP, TG-DTA, cyclic voltammetry, variable-temperature magnetic susceptibility and X-ray single-crystal diffraction.X-ray single-crystal diffraction indicates that the title compound crystallizes in a triclinic lattice, Pī space group, with a=1.2462(3) nm, b=1.2652(3) nm,c=1.8420(4) nm,α=87.45(3)°,β=79.91(3)°,γ=82.57(3)°,Z=1, R1=0.0778,wR2=0.1610.Structural analysis reveals that Sm3+(1) coordination cation has incorporated into the vacant site of [α-SiW11O39]8- entity,forming the [α-SiW11O39Sm(H2O)4]5- subunit.The two adjacent [α-SiW11O39Sm(H2O)4]5- subunits are combined with each other through two Sm(1)-O-W bridges accompanying the formation of dimmer structural unit [α-SiW11O39Sm(H2O)4]210- of the title compound.The neighboring dimmer structural units [α-SiW11O39Sm(H2O)4]210- are linked to form the 1D chainlike structure by means of two Sm3+(2) and a Na+(1) coordination cations.The K+(1) cations connect the 1D packing chains constructing the 2D netlike structure, and adjacent netlike layers are also grafted by K+(2) cations to build the novel 3D infinitely extended structure.The result of TG-DTA curves manifests that the decomposition temperature of the title polyanionic framework is 554℃.The cyclic voltammetry measurements show that the title polyanion has the two-step redox processes in aqueous solution with pH=3.1.Variable temperature magnetic susceptibility indicates the title compound obeys the Cruie-Weiss Law in the higher temperature range from 110 to 300 K, while in the lower temperature range from 2 to 110 K the comparatively strong antiferromagnetism interactions can be observed.