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91.
Mohd Rushdi Abu Bakar Zoltan Kalman Nagy Christopher David Rielly 《Journal of Thermal Analysis and Calorimetry》2010,99(2):609-619
A combination of differential scanning calorimetry and hot-stage microscopy with image analysis has been used to investigate
the polymorphism of sulfathiazole. The use of light intensity profiles obtained from the HSM images, as an alternative way
to present results of the HSM analysis, was found to be useful in describing and verifying thermal events. The approach provides
a unique insight into the polymorphic transformations and thermal behaviour exhibited by this compound. The results of the
experiments show that sulfathiazole tends to crystallise as mixtures of polymorphs, even though the literature methods for
producing pure polymorph were followed. 相似文献
92.
A novel method for nonlinear fractional partial differential equations: Combination of DTM and generalized Taylor's formula 总被引:1,自引:0,他引:1
In this article, a novel numerical method is proposed for nonlinear partial differential equations with space- and time-fractional derivatives. This method is based on the two-dimensional differential transform method (DTM) and generalized Taylor's formula. The fractional derivatives are considered in the Caputo sense. Several illustrative examples are given to demonstrate the effectiveness of the present method. Results obtained using the scheme presented here agree well with the analytical solutions and the numerical results presented elsewhere. Results also show that the numerical scheme is very effective and convenient for solving nonlinear partial differential equations of fractional order. 相似文献
93.
JPC – Journal of Planar Chromatography – Modern TLC - A simple and precise high-performance thin-layer chromatographic (HPTLC) method has been established for simultaneous analysis of... 相似文献
94.
A right module $M$ over an associative ring $R$ with unity is a $QTAG$-module if every finitely generated submodule of any homomorphic image of $M$ is a direct sum of uniserial modules. This article considers the closure of $h$-pure-$S$-high submodules of $QTAG$-modules. Here, we determine all submodules $S$ of a $QTAG$-module $M$ such that each closure of $h$-pure-$S$-high submodule of $M$ is $h$-pure-$\overline{S}$-high in $\overline{M}$. A few results of this theme give a comparison of some elementary properties of $h$-pure-$S$-high and $S$-high submodules. 相似文献
95.
Hafedh Hajlaoui Soumaya Arraouadi Emira Noumi Kaïss Aouadi Mohd Adnan Mushtaq Ahmad Khan Adel Kadri Mejdi Snoussi 《Molecules (Basel, Switzerland)》2021,26(12)
Herbs and spices have been used since antiquity for their nutritional and health properties, as well as in traditional remedies for the prevention and treatment of many diseases. Therefore, this study aims to perform a chemical analysis of both essential oils (EOs) from the seeds of Carum carvi (C. carvi) and Coriandrum sativum (C. sativum) and evaluate their antioxidant, antimicrobial, anti-acetylcholinesterase, and antidiabetic activities alone and in combination. Results showed that the EOs mainly constitute monoterpenes with γ-terpinene (31.03%), β-pinene (18.77%), p-cymene (17.16%), and carvone (12.20%) being the major components present in C. carvi EO and linalool (76.41%), γ-terpinene (5.35%), and α-pinene (4.44%) in C. sativum EO. In comparison to standards, statistical analysis revealed that C. carvi EO showed high and significantly different (p < 0.05) antioxidant activity than C. sativum EO, but lower than the mixture. Moreover, the mixture exhibited two-times greater ferric ion reducing antioxidant power (FRAP) (IC50 = 11.33 ± 1.53 mg/mL) and equipotent chelating power (IC50 = 31.33 ± 0.47 mg/mL) than the corresponding references, and also potent activity against 2,2-diphenyl-1-picrylhydrazyl (DPPH) (IC50 = 19.00 ± 1.00 mg/mL), β-carotene (IC50 = 11.16 ± 0.84 mg/mL), and superoxide anion (IC50 = 10.33 ± 0.58 mg/mL) assays. Antimicrobial data revealed that single and mixture EOs were active against a panel of pathogenic microorganisms, and the mixture had the ability to kill more bacterial strains than each EO alone. Additionally, the anti-acetylcholinesterase and α-glucosidase inhibitory effect have been studied for the first time, highlighting the high inhibition effect of AChE by C. carvi (IC50 = 0.82 ± 0.05 mg/mL), and especially by C. sativum (IC50 = 0.68 ± 0.03 mg/mL), as well as the mixture (IC50 = 0.63 ± 0.02 mg/mL) compared to the reference drug, which are insignificantly different (p > 0.05). A high and equipotent antidiabetic activity was observed for the mixture (IC50 = 0.75 ± 0.15 mg/mL) when compared to the standard drug, acarbose, which is about nine times higher than each EO alone. Furthermore, pharmacokinetic analysis provides some useful insights into designing new drugs with favorable drug likeness and safety profiles based on a C. carvi and C. sativum EO mixture. In summary, the results of this study revealed that the combination of these EOs may be recommended for further food, therapeutic, and pharmaceutical applications, and can be utilized as medicine to inhibit several diseases. 相似文献
96.
Abd Elmoneim O. Elkhalifa Eyad Al-Shammari Mohd Adnan Jerold C. Alcantara Khalid Mehmood Nagat Elzein Eltoum Amir Mahgoub Awadelkareem Mushtaq Ahmad Khan Syed Amir Ashraf 《Molecules (Basel, Switzerland)》2021,26(12)
Abelmoschus esculentus (Okra) is an important vegetable crop, widely cultivated around the world due to its high nutritional significance along with several health benefits. Different parts of okra including its mucilage have been currently studied for its role in various therapeutic applications. Therefore, we aimed to develop and characterize the okra mucilage biopolymer (OMB) for its physicochemical properties as well as to evaluate its in vitro antidiabetic activity. The characterization of OMB using Fourier-transform infrared spectroscopy (FT-IR) revealed that okra mucilage containing polysaccharides lies in the bandwidth of 3279 and 1030 cm−1, which constitutes the fingerprint region of the spectrum. In addition, physicochemical parameters such as percentage yield, percentage solubility, and swelling index were found to be 2.66%, 96.9%, and 5, respectively. A mineral analysis of newly developed biopolymers showed a substantial amount of calcium (412 mg/100 g), potassium (418 mg/100 g), phosphorus (60 mg/100 g), iron (47 mg/100 g), zinc (16 mg/100 g), and sodium (9 mg/100 g). The significant antidiabetic potential of OMB was demonstrated using α-amylase and α-glucosidase enzyme inhibitory assay. Further investigations are required to explore the newly developed biopolymer for its toxicity, efficacy, and its possible utilization in food, nutraceutical, as well as pharmaceutical industries. 相似文献
97.
The densities (ρ), viscosities (η), refractive indices (nD), and speeds of sound (u), of binary mixtures of pyridine with 1-hexanol, 1-heptanol, 1-octanol and 1-decanol, including those of pure liquids, were measured over the entire composition range at 303.15 K and atmospheric pressure. From these experimental data, the values of excess molar volumes (VE), deviations in isentropic compressibilities (Δks), viscosities (Δh), molar refractions (ΔRm), apparent and partial molar volumes (Vf,2 and ), apparent and partial molar compressibilities (Kf,2 and ), of alkanols in pyridine and their corresponding deviations (ΔV and ΔK) were calculated. The variations of these parameters with composition of the mixtures suggest that the strength of interactions in these mixtures follow the order: 1-hexanol>1-heptanol>1-octanol>1-decanol. All the excess and deviation functions were fitted to Redlich-Kister polynomial equation to determine the fitting coefficients and the standard deviations. 相似文献
98.
In this article, we implement relatively new analytical techniques, the variational iteration method and the Adomian decomposition method, for solving nonlinear partial differential equations of fractional order. The fractional derivatives are described in the Caputo sense. The two methods in applied mathematics can be used as alternative methods for obtaining analytic and approximate solutions for different types of fractional differential equations. In these schemes, the solution takes the form of a convergent series with easily computable components. Numerical results show that the two approaches are easy to implement and accurate when applied to partial differential equations of fractional order. 相似文献
99.
Nadjette Debbouche Shaher Momani Adel Ouannas Mohd Taib Shatnawi Giuseppe Grassi Zohir Dibi Iqbal M. Batiha 《Entropy (Basel, Switzerland)》2021,23(3)
This article investigates a non-equilibrium chaotic system in view of commensurate and incommensurate fractional orders and with only one signum function. By varying some values of the fractional-order derivative together with some parameter values of the proposed system, different dynamical behaviors of the system are explored and discussed via several numerical simulations. This system displays complex hidden dynamics such as inversion property, chaotic bursting oscillation, multistabilty, and coexisting attractors. Besides, by means of adapting certain controlled constants, it is shown that this system possesses a three-variable offset boosting system. In conformity with the performed simulations, it also turns out that the resultant hidden attractors can be distributively ordered in a grid of three dimensions, a lattice of two dimensions, a line of one dimension, and even arbitrariness in the phase space. Through considering the Caputo fractional-order operator in all performed simulations, phase portraits in two- and three-dimensional projections, Lyapunov exponents, and the bifurcation diagrams are numerically reported in this work as beneficial exit results. 相似文献
100.
Ismail A. Haj Waseem Hafiz Muhammad Ishtiaq Muhammad Jamal Sajjad Shaukat Khan Majid 《International Journal of Theoretical Physics》2021,60(5):1720-1741
International Journal of Theoretical Physics - Most of the enciphering structures are based on the transformation of mediums by describing the strict criteria. The presented article is based on... 相似文献