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苯并噻唑重氮氨基偶氮苯与汞(Ⅱ)的显色反应及其应用 总被引:26,自引:2,他引:24
报道了新试剂苯并噻唑重氮氨基偶氮苯的合成及其与汞(Ⅱ)的显色反应,在TritonX-100存在下弱碱性介质中,试剂与汞形成2:1的橙红色络合物,最大吸收波长位于520nm处,表观摩尔吸光系数为1.51×10^5L.mol^-1.cm^-1。汞量在0~1.2mg/L范围内遵守比尔定律,直接应用于废水中微量汞的测定,结果满意。 相似文献
44.
All-optical wavelength conversion of 10-Gb/s signal based on four-wave mixing is experimentally demonstrated in a 30-m-long dispersion-flattened microstructure fiber with small positive dispersion. For an average pump power of 26 dBm, the conversion efficiency was around -19.5 dB with the fluctuation less than ±1.4 dB, covering a conversion bandwidth of 20 nm. The eye diagram of the converted signal shows good eye opening. 相似文献
45.
In this paper, optical limiting property in a magnetic fluid film is studied. The relationship between the emergent power and the incident power is investigated experimentally and theoretically. It is found that the limiting threshold is linear with the diaphragm aperture which accord with the theoretical prediction. The external magnetic field will affect the limiting property, and increase the limiting threshold. 相似文献
46.
Wei Mingjun Zhu Wanzhen 《Annals of Differential Equations》2007,23(4):511-518
In this paper we consider the system of classical particles coupled with a Klein-Gordon field in two dimensions.We establish a-priori-bounds on the solutions of this system with initial data satisfying a size restriction derived from conservation of energy.This result,together with the smoothing of"velocity averaging",yields the existence of global weak solutions to the corresponding restricted initial value problem.The size restriction is necessary since energy of the system is indefinite.Finally,we show that the weak solutions preserve the total mass. 相似文献
47.
A delayed stage-structured predator–prey model with non-monotone functional responses is proposed. It is assumed that immature individuals and mature individuals of the predator are divided by a fixed age, and that immature predators do not have the ability to attack prey. Some new and interesting sufficient conditions are obtained for the global existence of multiple positive periodic solutions of the stage-structured predator–prey model. Our method is based on Mawhin’s coincidence degree and novel estimation techniques for the a priori bounds of unknown solutions to Lx = λNx. An example is given to illustrate the feasibility of our main result. 相似文献
48.
The feature selection consists of obtaining a subset of these features to optimally realize the task without the irrelevant
ones. Since it can provide faster and cost-effective learning machines and also improve the prediction performance of the
predictors, it is a crucial step in machine learning. The feature selection methods using support machines have obtained satisfactory
results, but the noises and outliers often reduce the performance. In this paper, we propose a feature selection approach
using fuzzy support vector machines and compare it with the previous work, the results of experiments on the UCI data sets
show that feature selection using fuzzy SVM obtains better results than using SVM. 相似文献
49.
对交流电场下双巯基烷烃硫醇自组装分子膜的阻抗谱进行了研究.利用汞金属作为衬底,制备出双巯基烷烃硫醇自组装分子膜,并通过交流频谱仪对其进行频谱的扫描.明确了膜的作用范围为阻抗谱中频部分为了解释该阻抗谱,提出了一种串联的等效电路来进行了拟合,并与其他的模型进行比较.同时,观察到在损耗谱中损耗峰随硫醇碳链原子数的增加而向低频方向移动并得出双巯基硫醇(C6-C10)在交流电场下的激活能为23~39 meV. 相似文献
50.