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Ali Morad Rashidi Roghaye Lotfi Amideddin Nouralishahi Mohammad Ali Khodagholi Masoud Zare Faeghe Eslamipour 《天然气化学杂志》2011,20(6):664-668
Nanoporous carbons were synthesized using furfuryl alcohol and sucrose as precursors and MCM-41 and mordenite as nanoporous templates.The produced nanoporous carbons were used as adsorbent for methane storage.The average pore diameter of the samples varied from 3.9 nm to 5.9 nm and the BET surface area varied from 320m2/g to 824m2/g.The volumetric adsorption experiments revealed that MCM-41 and sucrose had better performance compared with mordenite and furfuryl alcohol,correspondingly.Also,the effect of precursor to template ratio on the structure of nanoporous carbons and their adsorption capacities was investigated.The nanoporous carbon produced from MCM-41 mesoporous molecular sieve partially filled by sucrose shows the best methane adsorption capacity among the tested samples. 相似文献
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Smaoui S Mellouli L Lebrihi A Coppel Y Fguira LF Mathieu F 《Natural product research》2011,25(8):806-814
Thirty litres of fermentation broth was extracted from the newly isolated Streptomyces sp. strain TN17 and various separation and purification steps led to the isolation of three pure bioactive compounds (1-3). Compound 1: cyclo (L-Leu-L-Arg), a diketopiperazine 'DKP' derivative; 2: di-(2-ethylhexyl) phthalate, a phthalate derivative; and 3: cyclo 1-[2-(cyclopentanecarbonyl-3-phenyl-propionyl]-pyrrolidine-2-carboxylic acid (1-carbamoyl-propyl)-amide, a cyclic tetrapeptide derivative. The chemical structure of these three active compounds was established on the basis of spectroscopic studies (MS and NMR) and by comparison with data from the literature. According to our biological studies, the pure compounds (1-3) possess antibacterial and antifungal activities. 相似文献
34.
In this paper, we prove two-sided pointwise estimates for the Green function of a parabolic operator with singular first order term on a C1,1-cylindrical domain . Basing on these estimates, we establish the equivalence of the parabolic measure, the adjoint parabolic measure and the surface measure on the lateral boundary of . These results are first studied by some authors for certain elliptic and less general parabolic operators.
Mathematics Subject Classifications (2000) 31B25, 35B05, 35K10, 58J35. 相似文献
35.
Production possibility set (PPS) is intersection of the several halfspaces. Every halfspace corresponds with one strong or weak defining hyperplane (facet). This research proposes a method to find weak defining hyperplanes of PPS of BCC model. We state and prove some properties relative to our method. Numerical examples are provided for illustration. 相似文献
36.
F. Soleymani D.K.R. Babajee Taher Lotfi 《Journal of the Egyptian Mathematical Society》2013,21(3):346-353
An optimal method is developed for approximating the multiple zeros of a nonlinear function, when the multiplicity is known. Analysis of convergence for the proposed technique is studied to reveal the fourth-order convergence. We further investigate the dynamics of such multiple zero finders by using basins of attraction and their corresponding fractals in the complex plane. A fourth-order method will also be presented, when the multiplicity m is not known. Numerical comparisons will be made to support the underlying theory of this paper. 相似文献
37.
A. Javadi N. Mucic M. Karbaschi J.Y. Won M. Lotfi A. Dan V. Ulaganathan G. Gochev A.V. Makievski V.I. Kovalchuk N.M. Kovalchuk J. Krägel R. Miller 《The European physical journal. Special topics》2013,222(1):7-29
Liquid interfaces are met everywhere in our daily life. The corresponding interfacial properties and their modification play an important role in many modern technologies. Most prominent examples are all processes involved in the formation of foams and emulsions, as they are based on a fast creation of new surfaces, often of an immense extension. During the formation of an emulsion, for example, all freshly created and already existing interfaces are permanently subject to all types of deformation. This clearly entails the need of a quantitative knowledge on relevant dynamic interfacial properties and their changes under conditions pertinent to the technological processes. We report on the state of the art of interfacial layer characterization, including the determination of thermodynamic quantities as base line for a further quantitative analysis of the more important dynamic interfacial characteristics. Main focus of the presented work is on the experimental possibilities available at present to gain dynamic interfacial parameters, such as interfacial tensions, adsorbed amounts, interfacial composition, visco-elastic parameters, at shortest available surface ages and fastest possible interfacial perturbations. The experimental opportunities are presented along with examples for selected systems and theoretical models for a best data analysis. We also report on simulation results and concepts of necessary refinements and developments in this important field of interfacial dynamics. 相似文献
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Stability indicating method for famotidine in pharmaceuticals using porous graphitic carbon column 总被引:1,自引:0,他引:1
A simple, sensitive and rapid HPLC method was developed and validated for the simultaneous determination of famotidine (FMT) and related impurities in pharmaceuticals. Chromatographic separation was accomplished within 10 min on a porous graphitic carbon (PGC) column using 50:50 v/v ACN-water containing 0.5% pentane sulphonic acid (PSA) as the mobile phase. Separation was achieved with a flow rate of 1 mL/min and a detection wavelength of 265 nm. The calibration curves were linear over a concentration range of 1.5-100 microg/mL. The intra- and interday RSDs (n = 5) for the retention times and peak area were all less than 2%. The method was sensitive with an LOD (S/N = 3) of 0.1 microg/mL for FMT, imp. C and 0.05 microg/mL for imp. 2, A and D. All recoveries were greater than 98%. The method was demonstrated to be precise, accurate and specific with no interference from the tablet ingredients and separation of the drug peak from the peaks of the degradation products (oxidative degradation and acid and base degradation). The results indicated that the proposed method could be used for the determination of FMT in commercial dosage forms and as a stability-indicating assay. 相似文献