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The influence of trialkylsilyl groups on the nucleophilic reactivities of furans and thiophenes is determined by kinetic experiments. 相似文献
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Magnetic microspheres are optically encoded by doping with three luminescent dyes. The combination of a fluorophore with a nanosecond decay profile and two phosphorescent Ruthenium metal ligand complexes with a microsecond decay profile generates a characteristic signature described by three features: bead brightness, luminescent decay time and dual lifetime referencing (DLR). The beads are identified by time resolved imaging in the microsecond range. A series of fluorophores is tested and the interference of the resulting luminescent code in the red and green label detection channels is investigated. A detailed staining procedure is worked out to increase the staining efficiency of the dyes with hydrophilic character into the lipophilic polystyrene microspheres. A mathematical model is established to calculate the dye amounts that are needed for staining a bead family with a specific feature set. Nineteen bead families were prepared representing the grid points in the three planes of a cube referring to the three features. The coefficient of variation over all bead families is 7%, 1.4% and 1.6% for bead brightness, luminescence decay time and DLR, respectively. The combination of these features and the bead size as additional feature enables the creation of 840 distinguishable bead families. 相似文献
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Often, trajectories for mechanical systems are generated solving some optimization problem. Common approaches include time-optimal, energy optimal, etc., motion profiles. In order to decrease mechanical wear of real plants this profiles provide, e.g., a smooth movement (rest-to-rest) in accordance with restrictions in jerk, acceleration and velocity. There exists a number of methods, to calculate for a given trajectory the plant feed forward action and to design stabilizing controllers. In case of parameter uncertainty the control law often exhibits some adaptive part. Unfortunately, smooth trajectories tend to contain insufficient excitation for adaption and/or identification. Therefore, we propose to consider some measure for the information content concerning some unknown parameters in the trajectory optimization problem. (© 2014 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim) 相似文献