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D. V. Nesterov L. S. Molochnikov A. V. Pestov E. G. Matochkina M. I. Kodess Yu. G. Yatluk 《Polymer Science Series B》2013,55(7-8):490-495
The direct addition of glycidol to chitosan in a gel medium under exposure to ultrasound afforded the chelating aminopolymer N,O-(2,3-dihydroxy)propylchitosan with a degree of substitution up to 2.3. The sorption characteristics of the crosslinked aminopolymers with respect to boron-containing ions were estimated. 相似文献
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D. V. Nesterov L. S. Molochnikov M. I. Kodess E. G. Matochkina O. V. Koryakova Yu. G. Yatluk A. V. Pestov 《Russian Journal of Applied Chemistry》2013,86(5):777-781
A procedure was developed for preparation of poly[N-(2,3-dihydroxypropyl)aminostyrene] via successive stages of nitration, reduction, and glycidol treatment of polystyrene, which gives the polymer with a maximal degree of functionalization. The composition and structure of the intermediates and end products of the polymer-analogous reactions were characterized by elemental analysis, IR spectroscopy, and solid-state 13C NMR spectroscopy. The sorption characteristics of poly[N-(2,3-dihydroxypropyl)aminostyrene] toward boroncontaining ions were assessed. 相似文献
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A. V. Pestov Yu. S. Petrova A. V. Bukharova L. K. Neudachina O. V. Koryakova E. G. Matochkina M. I. Kodess Yu. G. Yatluk 《Russian Journal of Applied Chemistry》2013,86(2):269-272
A new procedure was developed for preparation of chelate amino-containing polymer N-2-sulfoethyl chitosan by synthesis in a gel through the reaction between chitosan and sodium 2-bromoethanesulfonate, yielding a polymer with the degree of substitution of up to 0.5. The structure of the resulting polymers was confirmed by 1H NMR spectroscopy. The sorption characteristics with respect to transition and alkaline-earth metal ions were determined for the cross-linked polymers. 相似文献
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The reaction of N-unsubstituted imines of 2-hydroxyacetophenones with trichloro(trifluoro)ethylidene nitromethanes in the presence of DABCO proceeds via tandem oxa-Michael/aza-Henry additions (in dichloromethane) or aza-Michael addition (in benzene) to give 4-methyl-3-nitro-2-trichloro(trifluoro)methyl-2H-chromenes or 1,1,1-trichloro(trifluoro)-3-nitro-N-[1-(2-hydroxyaryl)ethylidene]propan-2-amines, respectively. 相似文献
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A. V. Timshina S. A. Rubtsova M. I. Kodess E. G. Matochkina P. A. Slepukhin A. V. Kuchin 《Russian Journal of Organic Chemistry》2008,44(7):1043-1048
Asymmetrical oxidation was performed of menthone dithiolane obtained in 95–98% yield by condensation of menthone with 1,2-ethanedithiol in the presence of boron trifluoride etherate. 6-Isopropyl-9-methyl-1,4-dithiaspiro[4,5]decane-1,4-dioxide (yield 5–55%) and 6-isopropyl-9-methyl-1,4-dithiaspiro[4,5]-decane-1,1,4-trioxide (yield 65–70%) were synthesized. Chemical structures of compounds obtained were proved by XRD analysis, NMR and IR spectroscopy. 相似文献