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51.
Mahmoodi Nosrat O. Zeydi Masoud Mohammadi Mamaghani Manouchehr Montazeri Naser 《Research on Chemical Intermediates》2017,43(4):2641-2651
Research on Chemical Intermediates - A series of new thiocarbamoyl tris-pyrazoline (tripod pyrazoline with triazine core) compounds was obtained by tris-cyclization of chalcone with... 相似文献
52.
S.N. Mahmoodi S.E. Khadem N. Jalili 《Archive of Applied Mechanics (Ingenieur Archiv)》2006,75(2-3):153-163
The nonlinear equations of motion of planar bending vibration of an inextensible viscoelastic carbon nanotube (CNT)-reinforced
cantilevered beam are derived. The viscoelastic model in this analysis is taken to be the Kelvin–Voigt model. The Hamilton
principle is employed to derive the nonlinear equations of motion of the cantilever beam vibrations. The nonlinear part of
the equations of motion consists of cubic nonlinearity in inertia, damping, and stiffness terms. In order to study the response
of the system, the method of multiple scales is applied to the nonlinear equations of motion. The solution of the equations
of motion is derived for the case of primary resonance, considering that the beam is vibrating due to a direct excitation.
Using the properties of a CNT-reinforced composite beam prototype, the results for the vibrations of the system are theoretically
and experimentally obtained and compared. 相似文献
53.
In this paper, electron beam (e-beam) reduction method is applied for the catalyst layer preparation in the growth of carbon nanotubes (CNTs). A hot cathodic electron beam facility was employed to electron bombarding of catalyst layer before stage of CNTs growth. This new method leads to reducing the diameter of particles via sputtering and evaporating the surface of catalyst. The growth of CNTs was performed on the Fe catalyst layer with SiO2 substrate in an environment of different mixed gases (H2, NH3 and C2H2) by thermal chemical vapor deposition (TCVD) system. The morphology of the electron beam reduced catalyst particles were probed by atomic force microscopy (AFM). All samples were analyzed by scanning electron microscopy (SEM) before and after growth of CNTs. SEM analyses clarified that the catalyst grains have been smaller under effect of electron beam bombardment. 相似文献
54.
Khalil Tabatabaeian Manouchehr Mamaghani Nosratollah Mahmoodi Alireza Khorshidi 《合成通讯》2013,43(11):1677-1684
Diastereoselective conjugate 1,4-addition of indoles to α,β-unsaturated carbonyl compounds (hormone steroids) using Ru(III) as catalyst is reported. It was found that RuCl3·nH2O catalyzes the Michael addition of indoles to hormone steroids, providing new 3-alkylated derivatives in good to excellent yields. 相似文献
55.
56.
Direct chemoselective oxidation of δ-lactones via highly stable benzyl radical cyclization is reported. The one-pot conversion of premade substituted 5-aryl pentanoic acid and 8-benzyl-1-naphthoic acid in the presence of K2S2Os--CuCl2 results to the δ-lactones in moderate to good yields. The advantages of this methodology is using water as a solvent and utilizing available starting materials. 相似文献
57.
A convenient, one-pot multi-component synthesis of new 2,4-disubstituted hydrazinyl-thiazoles was accomplished using different aldehydes/ketones, thiosemicarbazide, and 4-methoxy phenacyl bromide in the presence of a catalytic amount of AcOH in EtOH. Products were obtained in reasonable yields and high purity. The in vitro antioxidant activity of hydrazinyl-thiazoles was evaluated by DPPH radical scavenging activity in comparison to ascorbic acid. Synthesized thiazoles 14c and 14g possessed the lowest \(\hbox {IC}_{50}\) values. Also, hydrazinyl-thiazoles were screened for their in vitro antibacterial activity against six strains of bacteria including S. aureus, M. luteus, E. coli, Ps. aeruginosa, B. subtilis, and A. hydrophila where some products showed good antibacterial activity. Moreover, compound 14a showed anticancer activity against melanoma cancerous cell lines A375 with \(\hbox {LC}_{50}= 0.55\hbox { mg}/\hbox {mL}\), slightly selective versus normal cell lines (Hu-2) with \(\hbox {LC}_{50}= 1.19\hbox { mg}/\hbox {mL}\). 相似文献
58.
Abbas Azimi Roshan Manouchehr Mamaghani Nosrat Ollah Mahmoodi Farhad Shirini 《中国化学快报》2012,23(4):399-402
An efficient ultrasound-assisted preparation of a series of novel 4-aryl-3-methyl-4,5-dihydro-l//-pyrazolo[34-b]pyridin-6(7H)ones via the reaction of 5-amino-3-methyl-1H-pyrazole,Meldrum’s acid and various arylaldehydes using one-pot three-component approach is described.This rapid method produced the products in short reaction times(3-4 min) and excellent yields(87-95%). 相似文献
59.
In most laser material processing, material removal by different mechanisms is involved. Here, application of acoustic signals with thermoelastic (below threshold) and breakdown origin (above threshold) together with plasma plume analysis as a simple monitoring system of interaction process is suggested. In this research the interaction of pulse CO2 laser with 200 ns duration and maximum energy of 1.3 J operating at 1 Hz with austenitic stainless steel (316-L) is reported. The results showed that the non-linear point of the curve can serve as a useful indicator of melting fluence threshold (in this case ≈830 J cm−2) with corresponding temperature calculated using plasma plume analysis. Higher acoustic amplitudes and larger plasma plume volume indicates more intense interaction. Also, analysis showed that a phase explosion process with material removal (ejecta) in the form of non-adiabatic (i.e., dt ? α−1) is at play after laser pulse is ended. Also, SEM photographs show different surface quality medication at different laser intensities, which indicates the importance of recoil momentum pressure and possibly electrons and ions densities in heat transfer. Finally, electrochemical test indicate an improved corrosion resistance for laser treated samples compared to untreated ones. 相似文献
60.
In this paper, the cross section of the 4He + 64Zn and 6He + 64Zn reactions, at bombarding energies above and below the fusion barrier, has been investigated. Soft-core nucleon-nucleon interaction and the Monte Carlo method have been employed for studying the nuclear potential of the projectile-target system. One adjustable parameter has been chosen in this study. This parameter can change the depth of the soft-core potential. It has to be adjusted so that the calculated elastic scattering and fusion cross sections are in acceptable agreement with experimental data. Our results indicate that an increase in energy decreases the depth parameter of the soft-core nucleon-nucleon potential obtained from careful analysis the 4He + 64Zn and 6He + 64Zn reactions. Likewise, by comparing the results obtained from both reactions, one can observe that the calculated depth parameter for the reaction related to 6He is larger than that for 4He at the same energy, in particular at the sub-barrier energies. We try to explain this behavior. 相似文献