Ueber fractionirte Destillation

Ohne Zusammenfassung     

Ueber die Darstellung von Traubenzucker

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Zum qualitativen Nachweis des Acetals

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Über Derivate des Dipyridyls

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Bücherbesprechungen

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On the Application of the Auxiliary Problem Principle

The auxiliary problem principle (APP) derives from a general theory on decomposition-coordination methods establishing a comprehensive framework for both one-level and two-level methods. In this paper, the results of the two-level methods of APP are specialized for an efficient application to some engineering problems.     

Diffusion Structural Analysis Study of Titania Films Deposited by Sol-Gel Technique on Silica Glass

The diffusion structural analysis (DSA) was used to characterize microstructure changes of hydrous titania gel films under in situ conditions of heating. TG and DTA were used in order to elucidate the processes controlling the formation of anatase film during heating of hydrous titania gel film. The annealing of porosity and near surface structure defects of the dehydrated titania films was indicated by DSA in the temperature range 255–700°C as the decrease of radon release rate. It was demonstrated that the annealing was enhanced on heating in oxygen in comparison with heating in argon. The DSA experimental results were compared with model curves describing the radon diffusion mobility and the annealing of radon diffusion paths.     

Mechanisms for the SAR Imaging of the Ocean

We perform a comparative analysis of two mechanisms for the formation of a synthetic aperture radar (SAR) image of the ocean, which are related to orbital velocities on the surface. It is shown that the mechanism of fluctuations of the effective density of scatterers, which is commonly accepted at present as the physical basis for the SAR diagnostics of roughness, actually works only in the case of a sufficiently flat swell. In the presence of wind roughness, the dominant role is played by another mechanism, namely, fluctuations of the number of surface elements whose images are randomly shifted and superimposed in the image plane due to orbital velocities. In the case of a developed wind roughness propagated in the azimuthal direction, the power contributions of two above-mentioned mechanisms to the SAR imaging of the ocean differ by about two orders of magnitude.     

Spectroscopic Study of Proton-Transfer Interaction between Methylbis(1-silatranylmethyl)amine and Phenols

Acid-base interaction of phenol and 4-nitrophenol with methylbis(1-silatranylmethyl)amine in acetonitrile is completely shifted toward formation of solvation-separated ion pairs. The unusually high electron-donor power of the exocyclic nitrogen atom in the amine is due to the presence of two silatranylmethyl groups exhibiting a super-electron-donor inductive effect.