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941.
M. M. Abdillahi M. S. Gharami M. A. B. Siddiqui 《Journal of Thermal Analysis and Calorimetry》1994,42(6):1275-1284
Confirmations of the successful synthesis of a particular zeolite demand investigation of the crystals by XRD, SEM, MAS-NMR and chemical analysis. In this work, we have used the DTA exothermic lattice breakdown of theA-zeolite, which gives typical peaks at around 900–1200°C for characterization. The effects ofpH, concentration, time of crystallization and temperature were studied and it was quickly and easily possible to distinguishA-zeolite formation from others originating from the synthesis matrix under different conditions by using DTA/TG analyses. The parameters were optimized for the synthesis of the zeolite and DTA measurements yielded enough information to identify theA-zeolite; this was confirmed by XRD and SEM. 相似文献
942.
Z. Szeglowski H. Bruchertseifer V. B. Brudanin G. V. Buklanov O. Constantinescu Dinh Thi Lien V. P. Domanov L. I. Guseva M. Hussonnois G. S. Tikhomirova I. Zvara Yu. Ts. Oganessian 《Journal of Radioanalytical and Nuclear Chemistry》1994,186(4):353-359
The short-lived isotopes of W and their descendants have been isolated from the products of the bombardment of144Sm with24Mg by a fast continuous ion-exchange method, using HF solution media. The feasibility of this method for isolation of element 106 is discussed. 相似文献
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949.
M. M. Eisl B. M. Reichl S. D. Böhmig H. Störi 《Fresenius' Journal of Analytical Chemistry》1994,349(1-3):194-196
Using a discrete model for the segregation kinetics based on the Darken theory of diffusion and on the regular solution model (RSM), one and two dimensional simulations of interface segregation in binary and ternary systems have been performed. The aim of the calculations was to investigate the kinetics of segregation sequences in ternary systems, the segregation kinetics in discrete systems during the initial phase and finally the kinetics of surface segregation in the region of a grain boundary intersected by the surface. 相似文献
950.
H.-J. Kluge B. A. Bushaw G. Passler K. Wendt N. Trautmann 《Fresenius' Journal of Analytical Chemistry》1994,350(4-5):323-329
Resonance ionization spectroscopy (RIS) and its combination with mass spectrometry (RIMS) have grown to become powerful techniques, which offer high sensitivity as well as elemental and isotopic selectivity. The principles of RIS and RIMS are introduced; they primarily concern the analysis of the optical spectra for the choice of efficient excitation schemes and the suitable design of the experimental apparatus. Recent applications span from studies of short-lived isotopes at on-line mass separators to a wide variety of trace analysis applications for radioactive isotopes, which can range from measurements of solar neutrino flux to environmental assessment.On leave from Pacific Northwest Laboratory, Richland, USA 相似文献