Effect of post heat treatment on microstructure and photocatalytic activities of TiO2 nanoribbons

Low-dimensional TiO₂ nanoribbons were synthesized by a simple one-step hydrothermal method. The TiO₂ nanoribbons were calcined over the temperature range 200-800 °C in order to enhance their photocatalytic properties by altering their crystal phase and increasing crystallization. Effects of hydrothermal temperature, calcinated temperature and calcination time on the formation of nanostructures have been observed and characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). The (BET) specific surface area of the samples which with different post treatments were determined by N₂ absorption-desorption experiment. In addition, photocatalytic activities of the nanoribbons were evaluated by photodegradation of organic dyes methyl orange under the radiation of UV light. The results reveal that the post-treatments have great effects on the microstructures and the photocatalytic activities of TiO₂ nanoribbons.     

基于LabVIEW的驻波法测量声速的实验模拟

利用LabVIEW编写的测量声速的实验模拟软件不仅模拟了传统物理实验的操作过程,而且还加入了数据处理模块,实验数据采集完成后即可得出实验数据处理结果,可以用于学生实验前的预习与探究,或者实验教学中的演示。     

X射线荧光光谱研究粮食中生命有机碳与碳化学循环

采用X射线荧光光谱(XRF)方法测定六种粮食:稻谷(大米)、小麦(面粉)、黄豆、小米、高粱和玉米中生命有机碳含量和化学元素组成,建立一种新方法测定它们的蛋白质含量.粮食中生命有机碳平均含量约为44%.黄豆中的蛋白质含量最高(42.74%),小米蛋白质含量28.56%,麦子蛋白质含量27.57%,玉米蛋白质含量24.99...     

色散金属光学特性分析通用时域有限差分方法

结合数字信号处理中的半解析递归卷积(SARC)算法,提出一种用于金属光学特性分析的改进半解析递归时域有限差分方法(SARC FDTD)。该方法保持了SARC算法的绝对稳定性和高精度、低内存等优点,又利用梯形近似使FDTD递推公式更加简洁,计算效率进一步提高,对于各种常用金属色散模型,均只需给出模型的极点和对应的系数,即可运用该算法的程序进行计算,具有较好的通用性。最后,通过金属的高阶Lorentz,Drude-Lorentz和Drude-CP三种常用色散模型对算法进行了验证。     

Ultraviolet band edge photorefractivity in LiNbO3:Sn crystals

The ultraviolet (UV) band edge photorefractivity of Sn-doped LiNbO(3) (LN:Sn) at 325 nm has been investigated. A sharp decrease of beam distortion, which is accompanied by a significant increase in the photoconductivity, is observed in LN:Sn crystals with Sn-doping concentrations at or above 2.0 mol%. The diffraction efficiency, the holographic recording sensitivity and response rate, and the two-wave coupling gain coefficient are greatly enhanced when the Sn-doping concentration reaches 2.0 mol% or more. Unlike LiNbO(3) doped with Hf in which the UV gratings can be erased easily by a red beam, the UV gratings in LN:Sn can withstand long-term red beam illumination. Electrons are determined to be the dominant light-induced charge carriers responsible for the UV band edge photorefraction. The observed enhancement on the UV band edge photorefractivity is found to be associated with the showup of an absorption band around 325 nm in LN:Sn crystals with Sn-doping concentrations at or above 2.0 mol%.     

Investigation of patch antennas based on crossed idiosyncratic PBG structure

The method of finite difference time domain (FDTD) was used, and characteristics of the patch antenna based on drilling periodic air holes in the substrate were studied, the results indicate that the surface waves which propagate along the surface of the substrate can be suppressed by the crossed idiosyncratic PBG (photonic crystal band-gap) structure because of its effect of forbidden-band, that it can radiate most of electromagnetic waves’ energy in the substrate significantly, and that it has lower return loss (S11) compared to the conventional patch antennas, thus, a high gain is attained, its performance is improved. Due to these advantages, the use of photonic crystal patch antennas will be extended in areas such as mobile communication, satellite communication, aviation, etc.     

Film forming kinetics and reaction mechanism of γ-glycidoxypropyltrimethoxysilane on low carbon steel surfaces

The film forming kinetics and reaction mechanism of γ-GPS on low carbon steel surfaces was investigated by FTIR-ATR, AFM, NSS and theoretical calculation method. The results from experimental section indicated that the reaction of γ-GPS on low carbon steel surfaces followed the conventional reaction mechanism, which can be described as reaction (I) (Me (Metal)-OH + HO-Si → Me-O-Si + H₂O) and reaction (II) (Si-OH + Si-OH → Si-O-Si + H₂O). During film forming process, the formation of Si-O-Fe bond (reaction (I)) exhibited oscillatory phenomenon, the condensation degree of silanol monomers (reaction (II)) increased continuously. The metal hydroxyl density had significant influence on the growth mechanisms and corrosion resisting property of γ-GPS films. The results from theoretical calculation section indicated that the patterns of reaction (I) and reaction (II) were similar, involving a nucleophilic attack on the silicon center. The formation of Si-O-Fe bond (reaction (I)) was kinetically and thermodynamically preferred, which had catalytic effect on its condensation with neighboring silanol monomers (reaction (II)). Our DFT calculations were good consistent with the experimental measurements.     

Libera BPM在BEPCⅡ调束中的应用

软件无线电技术的发展,不仅带来了现代通信领域的技术革命,同样在加速器束测领域中也带来了技术的革新.基于软件无线电技术和数字接收机架构的数字BPM首先在瑞士光源得到了成功的应用,斯洛文尼亚的Instrumentation Tchnologies公司把该项技术进行了市场化并进行了不断改进,形成了现在的Libera系列产品.它集模拟信号采集、模数转换、数字信号处理以及外同步于一体,是一个真正all-in-one的宽带测量系统.它可以完成束流位置的First Turn、Turn by Turn和COD等测量工作.在BEPCⅡ的初期调束中,在电子环和正电子环的束流闭环、储存和积累、故障查处以及同步环的注入残余振荡测量方面,Libera BPM发挥了出色的作用,加快了调束进程.     

一类相对转动非线性动力学模型的近似解

研究了一类具有非线性阻尼力和强迫周期力项的相对转动非线性动力学模型. 首先构造一个同伦映射, 其次决定方程的初始近似, 最后通过同伦映射方法得到了对应模型的任意次近似解. 关键词： 相对转动 非线性动力系统 近似解     

一类完整系统的Mei对称性与守恒量

对一类完整系统的方程给出其Mei对称性的定义和判据.如果Mei对称性是Noether对称性,则可找到Noether守恒量.如果Mei对称性是Lie对称性,则可找到Hojman型守恒量.举例说明结果的应用. 关键词： 分析力学 完整系统 Mei对称性 守恒量