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31.
We have prepared composite magnetic core–shell particles using the process of soap-free emulsion polymerization and the co-precipitation method. The shell of the synthesized composite sphere is cobalt ferrite (CoFe2O4) nanoparticles and the core consists of poly(styrene-co-methacrylic acid) polymer. The mean crystallite sizes of the coated CoFe2O4 nanoparticles were controlled in the range of 2.4–6.7 nm by the concentration of [NH4+] and heated temperature. The magnetic properties of the core–shell spherical particles can go from superparamagnetic to ferromagnetic behavior depending on the crystalline sizes of CoFe2O4.  相似文献   
32.
The major goal of this paper is to examine the hypothesis that stock returns and return volatility are asymmetric, threshold nonlinear, functions of change in trading volume. A minor goal is to examine whether return spillover effects also display such asymmetry. Employing a double-threshold GARCH model with trading volume as a threshold variable, we find strong evidence supporting this hypothesis in five international market return series. Asymmetric causality tests lend further support to our trading volume threshold model and conclusions. Specifically, an increase in volume is positively associated, while decreasing volume is negatively associated, with the major price index in four of the five markets. The volatility of each series also displays an asymmetric reaction, four of the markets display higher volatility following increases in trading volume. Using posterior odds ratio, the proposed threshold model is strongly favored in three of the five markets, compared to a US news double threshold GARCH model and a symmetric GARCH model. We also find significant nonlinear asymmetric return spillover effects from the US market.  相似文献   
33.
Analysis of a type of nonsmooth dynamical systems   总被引:1,自引:0,他引:1  
In this paper, a class of nonsmooth dynamical systems is analyzed. Extensive simulations reveal the chaotic behavior in these systems. By introducing a parameter, a chain of systems with one end being a linear stable system and the other being a chaotic system is constructed. Then the phase transition process through the chain is investigated as the parameter varies. Difficulties involved in analyzing this class of systems are also discussed.  相似文献   
34.
The annealing at 373 K of ultrastrong, gel‐spun polyethylene (PE) has been studied. At this temperature, the fibers show no significant shrinkage. Still, a significant decrease in the mechanical properties is observed. The fibers have been analyzed with differential scanning calorimetry (DSC), temperature‐modulated differential scanning calorimetry (TMDSC), atomic force microscopy (AFM), and small‐angle X‐ray scattering (SAXS). During the annealing, the glass transition of the intermediate phase is exceeded, as shown by DSC. When split for structure analysis by AFM, the annealed fibers undergo plastic deformation around the base fibrils instead of brittle fracture. The quasi‐isothermal TMDSC experiments are compared to the minor structural changes seen with SAXS and AFM. The loss of performance of the PE fibers at 373 K is suggested to be caused by the oriented intermediate phase, and not by major changes in the structure or morphology. The overall metastable, semicrystalline structure is shown by TMDSC to posses local regions that can melt reversibly. © 2003 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 41: 403–417, 2003  相似文献   
35.
本文讨论了赋予局部有限拓扑的非空闲子集超空间的局部紧性.主要结果是:X正则,则其闭子集超空间局部紧当且仅当X可表示成一个紧空间与一个离散空间的拓扑和.  相似文献   
36.
用迈克耳逊干涉仪测量气体折射率的误差的研究   总被引:1,自引:0,他引:1  
研究在用迈克尔逊干涉仪测量气体折射率时存在的系统和方法误差,提出了误差修正方法。  相似文献   
37.
关于高阶中立型偏微分方程系统解的振动性   总被引:16,自引:0,他引:16  
近年来,由于偏泛函微分方程(组)理论在人口动力学,生物遗传工程和化学反应过程等领域中有广泛的应用,因而很多学者在偏泛函微分方程(组)解的振动性理论的研究方面做了大量工作,取得了许多成果.本文将研究一类较广泛的高阶中立型偏微分方程组  相似文献   
38.
§ 1 IntroductionThe cutwidth problem for graphs,as well as a class of optimal labeling and embed-ding problems,have significant applications in VLSI designs,network communicationsand other areas (see [2 ] ) .We shall follow the graph-theoretic terminology and notation of [1 ] .Let G=(V,E)be a simple graph with vertex set V,| V| =n,and edge set E.A labeling of G is a bijec-tion f:V→ { 1 ,2 ,...,n} ,which can by regarded as an embedding of G into a path Pn.Fora given labeling f of G,th…  相似文献   
39.
林惠文  朱文祥 《中国化学》2003,21(8):1054-1058
The structure of the title adduct comprises a phenanthroline derivative 2-phenyl-imidazo[4,5-f]1,10-phenanthroline and a methanol.The composition of the crystalline adduct was characterized as C19H12N4.CH3OH.It belongs to orthorhombic system,space group Pna21 with a=1.3693(4)nm,b=2.2988(7)nm,c=0.51338(15)nm,V=1.6160(8)nm^3.Z=4,and final R1=0.0423.wR2=0.1012 .Crystal structure shows that all the 19 carbon atoms and 4 nitrogen atoms are coplanar.The bond length data indicated that a very extensive conjugation system was formed.This conjugation makes the compound being a potentially excellent energy transformer used for luminescent materials.  相似文献   
40.
We establish some liminf theorems on the increments of a (N,d)-Gaussian process with the usual Euclidean norm, via estimating upper bounds of large deviation probabilities on the suprema of the (N,d)-Gaussian process. This revised version was published online in June 2006 with corrections to the Cover Date.  相似文献   
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