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561.
Lillian Roth Jutta Zagon Anke Ehlers Lothar W. Kroh Hermann Broll 《Analytical and bioanalytical chemistry》2009,394(2):529-537
A new approach for the detection of DNA target molecules is described, using capture probes and subsequent signal enhancement
by a uniform polymerase chain reaction (PCR). Peptide nucleic acid probes were immobilized in real-time PCR-compatible microtiter
plates. After hybridization of biotinylated DNA targets, detection was performed by real-time immuno-PCR, a method formerly
used for protein detection. We demonstrate the feasibility of this strategy for the qualitative detection of DNA oligonucleotides
with a detection limit (LOD) of 6 attomol. Furthermore, the method was applied to PCR-amplified samples from genetically modified
maize DNA (Mon810). A 483-bp DNA fragment was detected in mixture with 99.9% of noncomplementary DNA with a sensitivity down
to the level of attomole.
Figure 相似文献
562.
Cludia Novais Carla Pereira Adriana K. Molina ngela Liberal Maria Inês Dias Mikel Aibarro-Ortega Maria Jos Alves Ricardo C. Calhelha Isabel C.F.R. Ferreira Lillian Barros 《Molecules (Basel, Switzerland)》2021,26(6)
Medicinal and aromatic plants (MAPs), worldwide appreciated and used as condiments, dyes, and preservatives, possess several biological properties that justify their continuous application in the food industry. In the present study, the nutritional and chemical profiles, as well as the bioactive properties of four combinations of condiments, sold for seasoning poultry, meat, fish, and salads, were evaluated. Twenty-five phenolic compounds (HPLC-DAD-ESI/MS) were identified, with apigenin-O-malonyl-pentoside-hexoside as the major compound detected in all extracts. Oxalic and citric acids were identified in all mixtures (UFLC-PDA), as well as all the four tocopherol isoforms (HPLC-fluorescence). Regarding bioactivities, the mixtures for meat and salads (TBARS) and meat and poultry (OxHLIA) stood out for their antioxidant potential, whereas for the anti-inflammatory and antitumor properties, the mixtures revealing the greatest results were those for poultry and salad, respectively. In terms of antimicrobial activity, all the mixtures revealed the capacity to inhibit the growth of some bacterial strains. In brief, condiment mixtures showed to be a good source of bioactive compounds, as they confer health benefits, validating the importance of their inclusion in the human diet as a good dietary practice. 相似文献
563.
The EU maximum limit of 10 microg kg(-1) of OTA for dried vine fruits has been established since 2002 (European Commission, 2005). The presented work explore the capability of using Fourier infrared spectroscopy attenuated total reflection (FTIR-ATR) for the detection of ochratoxin A (OTA) in dried vine fruits in a range of concentration between 2 and 50 microg kg(-1) OTA. The method developed included a sample pretreatment using a C18 cartridge which was efficient for the isolation of the mycotoxin. The PLS1 analysis of the spectrum of sultanas spiked with different OTA concentrations showed a good correlation between the spectral data and reference concentration for OTA (R(2)=0.85). 相似文献
564.
Abdênago Barros Ernani Ribeiro Jr 《Bulletin of the Brazilian Mathematical Society》2014,45(2):325-341
The aim of this paper is to present some structural equations for generalized m-quasi-Einstein metrics (M n , g, ? f, λ), which was defined recently by Catino in [11]. In addition, supposing that M n is an Einstein manifold we shall show that it is a space form with a well defined potential f. Finally, we shall derive a formula for the Laplacian of its scalar curvature which will give some integral formulae for such a class of compact manifolds that permit to obtain some rigidity results. 相似文献
565.
566.
Carlos J. Braga Barros Josiney A. Souza Victor H. L. Rocha 《Bulletin of the Brazilian Mathematical Society》2015,46(2):181-204
In this paper we develop a theory of Lyapunov stability for generalized flows on principal and associated bundles. We present a study of Lyapunov stability and attraction in the total space of a principal bundle by means of the action of the structure group.We also relate limit sets, prolongations, prolongational limit sets, attracting sets and stable sets in the total space of an associated bundle to the corresponding concepts in the fibers. 相似文献
567.
568.
In this paper we explore the relations between the standard dual problem of a convex generalized fractional programming problem and the partial dual problem proposed by Barros et al. (1994). Taking into account the similarities between these dual problems and using basic duality results we propose a new algorithm to directly solve the standard dual of a convex generalized fractional programming problem, and hence the original primal problem, if strong duality holds. This new algorithm works in a similar way as the algorithm proposed in Barros et al. (1994) to solve the partial dual problem. Although the convergence rates of both algorithms are similar, the new algorithm requires slightly more restrictive assumptions to ensure a superlinear convergence rate. An important characteristic of the new algorithm is that it extends to the nonlinear case the Dinkelbach-type algorithm of Crouzeix et al. (1985) applied to the standard dual problem of a generalized linear fractional program. Moreover, the general duality results derived for the nonlinear case, yield an alternative way to derive the standard dual of a generalized linear fractional program. The numerical results, in case of quadratic-linear ratios and linear constraints, show that solving the standard dual via the new algorithm is in most cases more efficient than applying directly the Dinkelbach-type algorithm to the original generalized fractional programming problem. However, the numerical results also indicate that solving the alternative dual (Barros et al., 1994) is in general more efficient than solving the standard dual.This research was carried out at the Econometric Institute, Erasmus University Rotterdam, the Netherlands and was supported by the Tinbergen Institute Rotterdam 相似文献
569.
H.V. Keer D.L. Dickerson H. Kuwamoto H.L.C. Barros J.M. Honig 《Journal of solid state chemistry》1976,19(1):95-102
Heat capacities have been measured for single crystals of V2O3, either pure or doped with 1 and 1.4 mole% Cr2O3 and Al2O3 over the temperature range 100–700°K. V2O3 undergoes a fairly sharp transition at low temperatures (~170°K) but fails to exhibit any thermal anomaly above 300°K. The thermal behavior of (MxV1?x)2O3, M = Cr, Al, is manifested by two transitions: one at low temperatures, 170–180°K for x = 0.01 and 180–190°K for x = 0.014, and the other at high temperatures. For x = 0.01, the high-temperature (HT) anomaly extended over the range 325–345°K (Cr-doped V2O3) and 345–365°K (Al-doped V2O3), respectively. The corresponding ranges for x = 0.014 were found to be 260–280°K and 270–290°K, respectively. Further, the HT anomaly was characterized by a large hysteresis (~50°K). The values of lattice heat capacity of pure and doped V2O3 were, however, found to be almost the same and could be empirically represented by the Debye (D)?Einstein (E) function with θ values 430°K (T = 100–230°K) and 465°K (T > 230°K), respectively. Further, the enthalpy change ΔH associated with the HT anomaly in doped V2O3 (80 ≤ ΔH ≤ 510 J/mole) was 5–10 times smaller than the ΔH corresponding to the lower-temperature transition. The results cited here appear incompatible with the Mott transition model that has been invoked to explain the HT anomaly. 相似文献
570.
Gustavo M. do Nascimento Wdeson P. Barros Yoong Ahm Kim Hiroyuki Muramatsu Takuya Hayashi Morinobu Endo Noriberto A. Pradie Cristiano Fantini Marcos A. Pimenta Mildred S. Dresselhaus Humberto O. Stumpf 《Journal of Raman spectroscopy : JRS》2012,43(12):1951-1956
The electronic interactions between the [Cu(opba)]2− anions (where opba is orthophenylenebis (oxamato)) and single‐wall carbon nanotubes (SWCNTs) were investigated by resonance Raman spectroscopy. The opba can form molecular magnets, and the interactions of opba with SWCNTs can produce materials with very different magnetic/electronic properties. It is observed that the electronic interaction shows a dependence on the SWCNT diameter independent of whether they are metallic or semiconducting, although the interaction is stronger for metallic tubes. The interaction also is dependent on the amount of complex that is probably adsorbed on the carbon surface of the SWCNTs. Some charge transfer can be also occurring between the metallic complex and the SWCNTs. Copyright © 2012 John Wiley & Sons, Ltd. 相似文献