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991.
Polymer-supported ruthenium complexes ■-Phen-Ru-①,■-Phen-Ru-②,■-Phen-Ru-③,■-Phen-Ru-④, ■-Phen-Ru-⑤,■-Phen-Ru-⑥and ■-Phen-Ru-⑦were prepared using aminomethyl polystyrenes of different morphological structures as supports.A variety of alcohols were oxidized efficiently into the corresponding ketones, carboxylic acids or aldehydes with iodosylbenzene (PhIO) catalyzed by aminomethyl polystyrene-supported ruthenium complexes under mild reaction conditions in acetonitrile.The influences of morphological struct... 相似文献
992.
Sanner C Su EJ Keshet A Huang W Gillen J Gommers R Ketterle W 《Physical review letters》2011,106(1):010402
Spin fluctuations and density fluctuations are studied for a two-component gas of strongly interacting fermions along the Bose-Einstein condensate-BCS crossover. This is done by in?situ imaging of dispersive speckle patterns. Compressibility and magnetic susceptibility are determined from the measured fluctuations. This new sensitive method easily resolves a tenfold suppression of spin fluctuations below shot noise due to pairing, and can be applied to novel magnetic phases in optical lattices. 相似文献
993.
研究的是唐家山地震次生灾害引发的堰塞湖问题.首先对数字高程地图进行等高图像分析求解了堰塞湖不同高程水位对应的湖区面积,建立了蓄水量体积与堰塞湖水位高程的离散化模型,然后建立了神经网络模型和多元线性回归模型研究了北川降雨量与堰塞湖入库流量的关系,继而求解得到不同降雨量下每日堰塞湖水位高程.在研究泄洪过程时,首先通过对泄洪过程和溃坝过程内在机理的研究分别建立了正交多项式逼近模型和仿真模型得到溃坝时的溃口流量随时间变化的关系,继而分析求解得到溃坝时其他参数随时间变化的关系.针对淹没区的问题,综合数字高程地图和行政区域地图,利用数字地图计算了洪水到达各被淹没区域的时间,淹没范围,以便于确定撤离方案. 相似文献
994.
Pengbo Su Bin Han Zhongnan Zhao Qiancheng Zhang Tian Jian Lu 《Acta Mechanica Sinica》2018,34(4):667-675
A novel square honeycomb-cored sandwich beam with perforated bottom facesheet is investigated under threepoint bending,both analytically and numerically.Perforated square holes in the bottom facesheet are characterized by the area ratio of the hole to intact facesheet(perforation ratio).While for large-scale engineering applications like the decks of cargo vehicles and transportation ships,the perforations are needed to facilitate the fabrication process(e.g.,laser welding)as well as service maintenance,it is demonstrated that these perforations,when properly designed,can also enhance the resistance of the sandwich to bending.For illustration,fair comparisons among competing sandwich designs having different perforation ratios but equal mass is achieved by systematically thickening the core webs.Further,the perforated sandwich beam is designed with a relatively thick facesheet to avoid local indention failure so that it mainly fails in two competing modes:(1)bending failure,i.e.,yielding of beam cross-section and buckling of top facesheet caused by bending moment;(2)shear failure,i.e.,yielding and buckling of core webs due to shear forcing.The sensitivity of the failure loads to the ratio of core height to beam span is also discussed for varying perforation ratios.As the perfo-ration ratio is increased,the load of shear failure increases due to thickening core webs,while that of bending failure decreases due to the weakening bottom facesheet.Design of a sandwich beam with optimal perforation ratio is realized when the two failure loads are equal,leading to significantly enhanced failure load(up to 60%increase)relative to that of a non-perforated sandwich beam with equal mass. 相似文献
995.
采用短焦距透镜设计水平场景无畸变折反射全景成像系统,会使系统更加小型化,然而短焦距透镜的畸变会对系统成像产生影响。为此建立了具有径向畸变的相机模型;根据这一相机模型,研究了采用短焦距摄像头的水平场景无畸变折反射全景成像系统中,透镜畸变对系统成像的影响,结果表明短焦距透镜的畸变会对系统成像产生严重影响;为了消除透镜畸变的影响,对反射镜的设计进行了改进,在反射镜面形微分方程中包含了透镜畸变消除的参量;按新的方法,设计了一套由短焦距摄像头组成的水平场景无畸变折反射全景成像系统。 相似文献
996.
997.
在合成含有8-羟基喹啉(8HOQ)配位基单体的基础上,将其与甲基丙烯酸甲酯(MMA)共聚得到含有8-羟基喹啉侧基的聚甲基丙烯酸甲酯(PMMA8q),实现了8-羟基喹啉的高分子化;通过PMMA8q和小分子协同配体与稀土离子Eu(Ⅲ)的配位反应,制备了两个稀土高分子发光配合物:Eu(PMMA8q)(8HOQ)2(H2O)3和Eu(PMMA8q)2(TTA)(H2O)3(TTA:噻吩甲酰三氟丙酮)。利用元素分析、红外光谱方法对各阶段产物进行了表征,用荧光光谱研究了两个稀土高分子配合物的荧光特性及发光机理。 相似文献
998.
Monodisperse spherical periodic mesoporous organosilicas (PMOs) with ethane integrated in the framework were synthesized and their application as stationary phase for chromatographic separation is demonstrated. The ethane-PMOs were prepared by condensation of 1,2-bis(triethoxysilyl)ethane (BTSE) in basic condition using octadecyltrimethylammonium chloride (C(18)TMACl) as template and ethanol as co-solvent. The morphology and mesoporous structure of ethane-PMOs were controlled under different concentrations of sodium hydroxide (NaOH) and EtOH. The results of scanning electron microscopy (SEM), transmission electron microscopy (TEM), powder X-ray diffraction (XRD), nitrogen sorption measurement, Fourier transform infrared spectroscopy (FT-IR) and elemental analysis showed that ethane-PMOs have spherical morphology, uniform particle distribution, highly ordered pore structure, high surface area and narrow pore-size distribution. The column packed with these materials exhibits good permeability, high chemical stability and good selectivity of mixtures of aromatic hydrocarbons in normal phase high-performance liquid chromatography (HPLC). 相似文献
999.
This paper proposes a flexible fast profilometry based on modulation measurement. Two orthogonal gratings through a beam splitter are vertically projected on an object surface, and the measured object is placed between the imaging planes of the two gratings. Then the image of the object surface modulated by the orthogonal gratings can be obtained by a CCD camera in the same direction as the grating projection. This image is processed by the operations consisting of performing the Fourier transform, spatial frequency filtering and inverse Fourier transform. Using the modulation distributions of two grating patterns, we can reconstruct the 3D shape of the object. In the measurement process, we only need to capture one fringe pattern, so it is faster than the MMP and remains the advantages of it. In the article, the principle of this method, the setup of the measurement system, some simulations and primary experiment results are given. The simulative and experimental result proves it can restore the 3D shape of the complex object fast and comparatively accurate. Because only one fringe pattern is needed in the testing, our method has a promising extensive application prospect in real-time acquiring and dynamic measurement of 3D data of complex objects. 相似文献
1000.