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141.
142.
利用钠荧光散射激光雷达对中层顶(75~105km)高度的钠原子层进行探测,以钠原子作为示踪物,通过反演得到了该区域大气密度起伏随高度分布和随时间变化关系.结果表明,中层顶附近大气密度起伏远大于平流层和对流层,在2h内,密度起伏可达5%,3日平均Richordson数为0.46. 相似文献
143.
O-Propargylic hydroxylamines undergo smooth 5-endo-dig cyclisations upon exposure to 3 equiv of molecular iodine to give respectable yields of the corresponding 4-iodo-2,5-dihydroisoxazoles, which should find a number of applications as intermediates for syntheses amongst this useful class of heterocycles. 相似文献
144.
FuLinYAN AiXiaWANG ZhongJianJIA LeiHE 《中国化学快报》2003,14(12):1253-1254
A new isopropenyl benzofuran-type tetramer was isolated from the roots of ligularia stenocephala and its structure was established by spectroscopic methods. 相似文献
145.
We show a bridge principle for harmonic diffeomorphisms between closed surfaces with higher genus. 相似文献
146.
微光成像系统的阈值探测理论和视距探测方程的研究 总被引:8,自引:2,他引:6
研究目前文献中常见的18种微光成像系统探测方程之间的内在联系和异同之处,分析论证各种阈值探测理论和探测方程存在的问题和不足。在此基础上,从人眼的视觉理论和阈值特性出发,建立微光成像系统新的阈值探测理论模型,并分别导出微光直视系统和微光电视系统的视距探测方程。应用所导出的理论公式计算的数据与各种实际系统的实测数据进行了比较,证明新的阈值探测理论和视距探测方程是正确可靠的,且具有很高的精度。 相似文献
147.
模式耦合理论在圆周对称长周期光纤光栅建模中的应用 总被引:4,自引:0,他引:4
长周期光纤光栅是不同于光纤Bragg光栅的一种光纤光栅器件 ,根据模式耦合理论 ,长周期光纤光栅表现为前向传播的纤芯导模和同向的各阶次包层模式之间的耦合。分析研究了长周期光纤光栅轴向的模场变化。忽略轴向的模式耦合以及包层模式之间的相互耦合作用 ,并认为折射率指数的调制只存在于纤芯中 ,建立了简化的长周期光纤光栅数学模型。对圆周对称轴向均匀型长周期光纤光栅谱特性进行了仿真 ,其结果与实验结果基本吻合 ,表明了简化的数学模型的合理性 相似文献
148.
Because quantum critical systems are very sensitive to the variation of parameters around the quantum phase transition (QPT), quantum criticality has been presented as an efficient resource for metrology. In this paper, we address the issue whether the divergent feature of the inverted variance is realizable in the presence of noise when approaching the QPT. Taking the quantum Rabi model (QRM) as an example, we obtain the analytical result for the inverted variance with single-photon relaxation. We show that the inverted variance may be convergent in time due to the noise. Since the precision of the metrology is very sensitive to the noise, as a remedy, we propose squeezing the initial state to improve the precision under decoherence. In addition, we also investigate the criticality-based metrology under the influence of the two-photon relaxation. Strikingly, although the maximum inverted variance still manifests a power-law dependence on the energy gap, the exponent is positive and depends on the dimensionless coupling strength. This observation implies that the criticality may not enhance but weaken the precision in the presence of two-photon relaxation, due to the non-linearity introduced by the two-photon relaxation. 相似文献
149.
Systematic chemical profiling of a multicomponent Chinese herbal formula Huo Luo Xiao Ling Dan by ultra high performance liquid chromatography coupled with electrospray ionization quadrupoletime‐of‐flight mass spectrometry
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Fenrong Wang Yu Ai Yun Wu Wen Ma Qiaoxia Bian David Y.‐W. Lee Ronghua Dai 《Journal of separation science》2015,38(6):917-924
Huo Luo Xiao Ling Dan, a Chinese herbal formula consisting of 11 different herbs, has been used in folk medicine for the treatment of arthritis and other chronic inflammatory diseases. However, the chemical compositions of Huo Luo Xiao Ling Dan are not completely characterized. In the present study, an ultra high performance liquid chromatography coupled with electrospray ionization quadrupole time‐of‐flight mass spectrometry method in positive and negative ion modes was employed to identify biochemical constitutes in Huo Luo Xiao Ling Dan. As a result, a total of 76 compounds including alkaloids, monoterpene glycosides, iridoids, phenolic acids, and tanshinones, coumarins, lactones, flavones, and their glycosides, triterpenes, and triterpene saponins were characterized by comparing the retention time and mass spectrometry data with reference standards within 5 ppm error or by reference to the reference literature. These results would provide the basis for a further in vivo study of Huo Luo Xiao Ling Dan and information for potential new drug candidates for treating arthritis and other chronic inflammatory diseases. 相似文献
150.
Separation and purification of five alkaloids from Aconitum duclouxii by counter‐current chromatography
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Yarong Wang Shining Cai Yang Chen Xumei Zhou Jia Liu Xin Xu Qiang Xia Mao Lin Jili Zhang Weili Huang Wenjun Wang Canhui Xiang Guozhen Cui Lianfeng Du Huan He Baohui Qi 《Journal of separation science》2015,38(13):2320-2326
C19‐diterpenoid alkaloids are the main components of Aconitum duclouxii Levl. The process of separation and purification of these compounds in previous studies was tedious and time consuming, requiring multiple chromatographic steps, thus resulted in low recovery and high cost. In the present work, five C19‐diterpenoid alkaloids, namely, benzoylaconine ( 1 ), N‐deethylaconitine ( 2 ), aconitine ( 3 ), deoxyaconitine ( 4 ), and ducloudine A ( 5 ), were efficiently prepared from A. duclouxii Levl (Aconitum L.) by ethyl acetate extraction followed with counter‐current chromatography. In the process of separation, the critical conditions of counter‐current chromatography were optimized. The two‐phase solvent system composed of n‐hexane/ethyl acetate/methanol/water/NH3·H2O (25%) (1:1:1:1:0.1, v/v) was selected and 148.2 mg of 1 , 24.1 mg of 2 , 250.6 mg of 3 , 73.9 mg of 4, and 31.4 mg of 5 were obtained from 1 g total Aconitum alkaloids extract, respectively, in a single run within 4 h. Their purities were found to be 98.4, 97.2, 98.2, 96.8, and 96.6%, respectively, by ultra‐high performance liquid chromatography analysis. The presented separation and purification method was simple, fast, and efficient, and the obtained highly pure alkaloids are suitable for biochemical and toxicological investigation. 相似文献