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991.
Summary A rapid and accurate LC method is described for simultaneous determination of pseudoephedrine hydrochloride (PSE), acetaminophen (AMP), dextromethorphen hydrobromide (DEX), and diphenhydramine hydrochloride (DPH) in a compound formulation. Chromatographic separation of the four drugs was achieved on a Hypersil CN column (150 mm × 4.6 mm, 5 m particle) by use of a mobile phase comprising a mixture of 3 mM ion-pairing solution, 2% aqueous triethylamine solution, and 2 M phosphoric acid, 68:48:88 (v/v), pH 3.0, delivered at 1.0 mL min–1. Compounds were detected at 215 nm and the run time was less than 10 min. The linearity, accuracy, and precision of the method were found to be acceptable over the concentration ranges 6.1–36.4 g mL–1 for PSE, 65.0–390.0 g mL–1 for AMP, 3.1–18.6 g mL–1 for DEX, and 5.0–30.0 g mL–1 for DPH. 相似文献
992.
Summary Two high-performance liquid chromatography (HPLC) techniques were developed for the determination of binding constants in
the interaction of serum albumin with L-tryptophan: internal calibration and external calibration. The results obtained were
compared with those obtained by the classical method of equilibrium dialysis and by gel filtration. While all the methods
are equally reliable, the internal and external calibration techniques seem to be superior in their simplicity, speed and
convenience. 相似文献
993.
We describe a space of functions contained inxxLx
(D)C(D G) but not necessarily inU. We give a representation of these functions as bounded multiplication operators on the Bergman spacexxLx
a
2
and identify the subspace consisting of functions which induce compact multiplication operators. We also describe a newC
*-subalgebra ofxxLx
(D) which we conjecture to be a proper super-set ofU.Most of this research was done while the second author was visiting Cleveland State University. He would like to thank the Mathematics Department for its hospitality. He would also like to thank the NNSFC for partial support. 相似文献
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999.
Alam MS Kim IJ Nemati B O'Neill JJ Romero V Severini H Sun CR Wang P Zoeller MM Crawford G Fulton R Gan KK Kagan H Kass R Lee J Malchow R Morrow F Sung M White C Whitmore J Wilson P Butler F Fu X Kalbfleisch G Lambrecht M Skubic P Snow J Bortoletto D Brown DN Dominick J McIlwain RL Miao T Miller DH Modesitt M Schaffner SF Shibata EI Shipsey IP Battle M Ernst J Kroha H Roberts S Sparks K Thorndike EH Wang C Artuso M Goldberg M Haupt T Horwitz N Kennett R Moneti GC Playfer S Rozen Y Rubin P 《Physical review D: Particles and fields》1992,46(11):4822-4827
1000.
Sun Huibin Liu Yunzuo Zhou Jiewen Wu Yaodong 《Zeitschrift für Physik A Hadrons and Nuclei》1992,342(2):141-144
Theγ-rays emitted in theβ-decay of182Ta have been reinvestigated with improved statistics in attempting to clarify the reported new levels at 1460.41, 1592.98, 1620.36, 1712.29 and 1762.91 keV in182W observed in theβ-decay of182Ta. The present study demonstrated that the fifteen newγ-rays, which were used to support the existence of the five new levels, are not relevant to theγ-decay of182Ta. Therefore the five new levels are not populated in this decay. Additionally, theγ-ray with an energy of 1035.6 keV (0 2 + →2 1 + ) deexciting theβ-band head in182W is observed for the first time in the present decay study and the previous tentative placement of the 351.0 keVγ-ray in the level scheme is confirmed by the present coincidence measurements. 相似文献