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ChujiangCai ZhigangShen MingzhuWang ShulinMa YushanXing 《中国颗粒学报》2003,1(4):156-161
This paper reports the use of a colloidal Pd^0 catalysis system to metallize the surface of precipitators separated from coal fly-ash, and metals such as Cu, Ni etc. are deposited on the precipitators surface. Alternatively, according to the characteristic surface of cenospheres, an Ag coating catalysis system is adopted to first deposit Ag on the cenospheres surface, followed, if necessary, by the deposition of other metals such as Cu, Ni, etc. on the Ag coating to produce monolayer and multilayer metal-coated cenospheres. The surface characteristics and the morphologies of the metal coatings are examined in detail with scanning electron microscopy (SEM), energy dispersive spectroscopy (EDX) and X-ray photoelectron spectroscopy (XPS) techniques. It can be shown that the quality of metal coatings derived from the Aa coatina catalysis system, is better than that of the colloidal Pd^0 catalysis system. 相似文献
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Combining color imaging with phase shifting, a technique named five-step color phase shifting is presented to determine the whole-field isoclinic parameter. Relevant theory is derived and explicit conditions for directly determining the isoclinic parameter in the range of [0,π/2] are given. The unloaded light intensity of the model is systematically studied. A color camera recorded five isoclinic images coupled with isochromatics from a plane polariscope with five different settings, respectively. Experiments have been carried out with a circular disk under diametral compression and errors have been analyzed and estimated. This technique utilizes white light, which avoids undefined isoclinics near the locations where the isochromatics exist and will have active effect on experimental stress analysis and structural strength design. 相似文献
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Summary The potential of liquid chromatography-mass spectrometry (LC-MS) has been studied for the simultaneous determination of sixteen carbamate and organophosphorus pesticides in honeybees using a traditional sample preparation protocol based on acetone extraction and dichloromethane partitioning. The performances of both atmospheric pressure chemical ionization (APCI) and electrospray (ES) interfaces were compared. APCI offered better sensitivity and specificity for a higher range of pesticides. Limits of quantification were from 0.01 to 0.17 mg kg–1, at which recoveries obtained were between 64 and 93%, except for pirimicarb that was at 13%, with relative standard deviations ranging from 7 to 20%. Fenitrothion, fenoxycarb, methiocarb and phoxim were found in bees from Valencian Community beehives at concentrations between 0.03 and 3.75 mg kg–1. 相似文献
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软x射线近贴显微技术 总被引:1,自引:0,他引:1
软x射线近贴显微技术不但可使活的生物样品成象,分辨率高于光学显微镜,而且人为的样品准备程序在该技术中都可避免。本文描述了用高功率激光打靶产生的等离子体作为软x射线源而进行的近贴显微研究,并得到了分辨率好于1μm的结果。 相似文献
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Y. H. Zhang X. H. Zhou Q. Z. Zhao X. F. Sun X. G. Lei Y. X. Guo Z. Liu X. F. Chen Y. T. Zhu S. X. Wen G. J. Yuan X. A. Liu 《Zeitschrift für Physik A Hadrons and Nuclei》1996,355(1):335-336
High spin states of the odd-odd162Lu nucleus have been studied via147Sm(19F,4nγ)162Lu reaction at 95 MeV beam energy. Level scheme for yrast band based onπ[h11/2 v[i13/2] quasiparticle configuration was established up to I π = (23?) for the first time. This band shows the signature inversion in energy before backbending generally appeared in this mass region. It is stressed that the signature splitting in162Lu is larger than that in the160Tm nucleus. 相似文献