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151.
M. Hannoun N. Blažević D. Kolbah F. Kajfež 《Phosphorus, sulfur, and silicon and the related elements》2013,188(1-2):125-126
Abstract Bis(trimethylsilyl)peroxide (BSPO) can be used for chemo- and stereoselective generation of P=O group by oxygenation of P(III) centre and transformation of P=S and P=Se groups. 相似文献
152.
Active-to-absorbing phase transition subjected to the velocity fluctuations in the frozen limit case
N. V. Antonov M. Hnatich A. S. Kapustin T. Lučivjanský L. Mižišin 《Physics of Particles and Nuclei Letters》2017,14(6):944-952
The directed bond percolation process is studied in the presence of compressible velocity fluctuations with long-range correlations. We discuss a construction of a field theoretic action and a way of obtaining its large scale properties using the perturbative renormalization group. The most interesting results for the frozen velocity limit are given. 相似文献
153.
In the present paper, a new approach was developed for solving the problem of time synchronization of a set of signals obtained by different measurement techniques without a common trigger. The recorded signals were the result of sparks and bursts generated by a repetitive Marx generator. A thermal imaging camera, a high speed camera and an audio recorder were used to obtain the necessary data for synchronization and characterization. Moreover, a piezoelectric sensor was applied for shock waves characterization during the early stages of bursts. In the first place, different data with evident time shifts were acquired. Then, A set of simple operations such as maximum selection and localization, threshold comparison, Euclidean distance calculation and minimization were employed for signal analysis and pattern matching to ensure a good data synchronization, which allowed a detailed analysis of the phenomenon in the end. 相似文献
154.
V. I. Petrenko M. V. Avdeev V. M. Garamus M. Kubovcikova Z. Gažová K. Šipošová L. A. Bulavin L. Almásy V. L. Aksenov P. Kopcansky 《Physics of the Solid State》2014,56(1):129-133
The structure of filament amyloid aggregates of hen egg white lysozyme in water has been investigated by the small-angle X-ray scattering method. The experimental data are described by different cylindrical models, among which the best agreement is reached with the long helix model. A comparison of the results with the small-angle neutron scattering data reveals the influence of the heavy component of the solvent (a H2O/D2O mixture) on the structure of the filaments. 相似文献
155.
156.
Barbora Benešová Martin Kružík Gabriel Pathó 《Continuum Mechanics and Thermodynamics》2014,26(5):683-713
We design a new mesoscopic thin-film model for shape-memory materials which takes into account thermomechanical effects. Starting from a microscopic thermodynamical bulk model, we guide the reader through a suitable dimension reduction procedure followed by a scale transition valid for specimen large in area up to a limiting model which describes microstructure by means of parametrized measures. All our models obey the second law of thermodynamics and possess suitable weak solutions. This is shown for the resulting thin-film models by making the procedure described above mathematically rigorous. The main emphasis is, thus, put on modeling and mathematical treatment of joint interactions of mechanical and thermal effects accompanying phase transitions and on reduction in specimen dimensions and transition of material scales. 相似文献
157.
158.
Vladislava Mičková Silvia Ružičková Dagmar Remeteiová Martina Laubertová Marianna Dorková 《Chemical Papers》2018,72(5):1231-1238
Sampling is the most important procedure in arriving at the value of an electronic scrap. Inappropriate sampling makes other procedures, including assaying, valueless, as the sample must really represent the electronic scrap from which it was taken. The aim of this study was to develop the procedure to investigate the composition of heterogeneous printed circuit boards (PCBs) material and to show its applicability as well as its related limitations. The contents of Cu, Pb, Ni, and Zn in PCBs from wasted mobile phones were determined. Mixtures of aqua regia, hydrogen peroxide and hydrofluoric acid were applied to sample digestion. Open and closed vessel wet digestion with or without heating and microwave-assisted one was realized. For these purposes different sample amounts (0.2, 0.4, and 0.5 g) were applied and on the basis of calculated relative standard deviation values (RSD), the precision of repeated the most effective digestion was evaluated. The microwave-assisted wet digestion and mixture of aqua regia and hydrogen peroxide was found as the most effective one of the compared mixtures and applied conditions. A sample amount of 0.5 g was found as the most suitable. RSD values confirm the importance of electronic waste material sample preparation. 相似文献
159.
160.
The beta dose response and Optically Stimulated Luminescence (OSL) signal stability characteristics of human tooth enamel deproteinated by hydrazine reagent under blue photon stimulation are reported. Removal of the protein organic component of tooth enamel resulted in a higher OSL sensitivity and slower fading of OSL signals. The effect of chemical sample preparation on the enamel sample sensitivity is discussed and further steps to make this deproteinization treatment suitable for in vitro dose reconstruction studies are suggested. 相似文献