Photoproduction of eta mesons off protons for 0.75 GeV<E(gamma)<3 GeV

Total and differential cross sections for the reaction p(gamma,eta)p have been measured for photon energies in the range from 750 MeV to 3 GeV. The low-energy data are dominated by the S11 wave which has two poles in the energy region below 2 GeV. Eleven nucleon resonances are observed in their decay into peta. At medium energies we find evidence for a new resonance N(2070)D15 with (M,Gamma)=(2068+/-22, 295+/-40) MeV. At gamma energies above 1.5 GeV, a strong peak in the forward direction develops, signaling the exchange of vector mesons in the t channel.     

Photoproduction of π 0 ω off protons for E γ ≤3 GeV

Differential and total cross-sections for photoproduction of γp→pπ ⁰ ω and γp→Δ ⁺ ω were determined from measurements of the CB-ELSA experiment, performed at the electron accelerator ELSA in Bonn. The measurements covered the photon energy range from the production threshold up to 3GeV.     

Si drift detector in comparison to Si(Li) detector for total reflection X-ray fluorescence analysis applications

TXRF is routinely used and suited to inspect Si wafer surfaces for possible impurities of metallic elements at the level of pg and below. Lightweight, compact sized, high-resolution Silicon drift detectors (FWHM=148 eV at 5.9 keV) electically cooled and with high throughput are ideally as the new spectrometer and for clean room application. A KETEK 5 mm² Si drift detector was compared with a NORAN 80 mm² SiLi in a previously commercially available ATOMIKA 8010 wafer analyzer. Results are presented and show that almost the same detection limits for both detector types were achieved analyzing a droplet sample containing 1 ng Ni on a Si wafer. Also, the performance to detect low Z elements like Na, excited with monochromatic Cr K radiation in a vacuum chamber was tested and detection limits of 600 pg obtained.     

Modification and validation of the pyromellitic acid electrolyte for the capillary electrophoretic determination of anions

For the determination of inorganic and organic anions, the pyromellitic acid (PMA) electrolyte is widely used. The pH adjustment of the self-prepared electrolyte was very challenging to satisfy the pH of specification of pH 7.8 +/- 0.1. A modification was proposed to provide a more simple electrolyte by buffering the PMA electrolyte with triethanolamine (TEA) only instead of adjusting the pH by NaOH and TEA. Thus, the proposed electrolyte consisted of 2.25 mmol l(-1) PMA, 0.75 mmol 1(-1) hexamethonium hydroxide and 12 mmol 1(-1) TEA. The performance of the PMA electrolyte buffered by TEA only was compared to a commercial available PMA and statistically validated in accordance with the methodology of Taguchi. No statistically significant difference could be found for both electrolytes assessing the performance and detection limits of hydrodynamic, stacking and electrokinetic injection with transient isotachophoretic preconcentration as well as repeatability of migration times, peak resolutions and peak symmetries.     

Quasifree photoproduction of eta mesons off the neutron

Quasifree photoproduction of eta mesons off nucleons bound in the deuteron has been measured with the CBELSA/TAPS detector for incident photon energies up to 2.5 GeV at the Bonn ELSA accelerator. The eta mesons have been detected in coincidence with recoil protons and recoil neutrons, which allows a detailed comparison of the quasifree n(gamma,eta)n and p(gamma,eta)p reactions. The excitation function for eta production off the neutron shows a pronounced bumplike structure at W=1.68 GeV (E{gamma} approximately 1 GeV), which is absent for the proton.     

NASICON type ionic conductors for alkali ion sensing

NASICON type ionic conductors can be used as the sensitive membrane of alkali ion sensors. The main advantages compared to the classical glass electrodes are the better selectivity and lower impedance. The mechanism of response of this type of ionic sensors is presented. The sensitivity results from a direct ionic exchange between the ceramic electrolyte and the solution which has been characterized by impedance spectroscopy. The origin of the selectivity in the NASICON framework is discussed in terms of structural and ionic exchange properties. The performance characteristics of sodium and lithium ion sensing devices are presented. Examples of biomedical applications such as the measurement of sodium concentration in the crevicular fluid and the determination of lithium in artificial serum are described. Paper presented at the 6th Euroconference on Solid State Ionics, Cetraro, Calabria, Italy, Sept. 12–19, 1999.     

Study of the reaction γp → pπ0η

The reaction γp → pπ⁰η has been studied with the CBELSA detector at the tagged photon beam of the Bonn electron stretcher facility. The reaction shows contributions from Δ⁺(1232)η , N(1535)⁺π⁰ and pa ₀(980) as intermediate states. A partial-wave analysis suggests that the reaction proceeds via formation of six Δ -resonances, Δ(1600)P ₃₃ , Δ(1920)P ₃₃ , Δ(1700)D ₃₃ , Δ(1940)D ₃₃ , Δ(1905)F ₃₅ , Δ(2360)D ₃₃ , and two nucleon resonances N(1880)P ₁₁ and N(2200)P ₁₃ , for which pole positions and decay branching ratios are given.     

Novel methods of TXRF analysis for silicon wafer surface inspection

TXRF became a standard, on-line inspection tool for controlling the cleanliness of polished Si wafers for semiconductor use. Wafer makers strive for an all-over metallic cleanliness of < 10¹⁰ atoms · cm^–2. The all-over cleanliness can be analyzed using VPD/TXRF. For VPD preparation and scanning we have developed an automatic system coupled with TXRF. With synchrotron radiation TXRF we were able to detect 13 fg of Ni in a residual microdroplet, i.e.10⁵ atoms · cm^–2. Received: 8 January 1998 / Revised: 13 July 1998 / Accepted: 30 July 1998     

Eu and Fe Mössbauer study of mechanically alloyed EuFeO3

EuFeO₃ was prepared by mechanical alloying starting from europium and iron oxides. After 20 h of milling the resulting compound is pure EuFeO₃. Samples were studied as a function of milling period using XRD, Mössbauer, SEM, and magnetic measurements. Mössbauer spectroscopy was used to probe both the transition metal and the rare-earth sites. Results are compared with previous works on EuFeO₃ prepared by different methods.