机器视觉在激光干涉测量d31中的应用

提出一种应用机器视觉技术的激光干涉法, 可以研究压电材料的逆压电系数. 在传统干涉测量法中引入机器视觉实现干涉图像灰度最佳估计, 使用数字图像处理技术, 一方面应用降噪算法有效去除激光干涉图样中的噪声, 从而确定激光干涉场的光强分布, 另一方面将干涉图样的明暗变化进一步转化为可量度的灰度变化以提高测量分辨力. 通过合理设计算法, 该方法中对位移的理论测量分辨力可以提高达一个数量级, 为干涉光波长的1/1024, 因此在逆压电系数d₃₁ 的实验测量中可以有效提高分辨力. 关键词： 机器视觉 逆压电系数 双光束干涉 数字图像处理     

氮化镓基发光二极管结构中粗化 p型氮化镓层的新型生长方法

提出了一种新型p型氮化镓粗化外延生长方法,这种生长方法的本质特征是利用低温生长的p型氮化镓作为粗化层的"晶籽"层,然后在这一层的基础上高温快速生长p型氮化镓,使粗化程度得到放大. 经实际制作尺寸为12 mil×10 mil的蓝光发光二极管器件并进行验证测试,与未进行p型氮化镓粗化的结果相比,通过这种方法粗化的发光二极管光通量可提升45%;结果同时表明,该方法有效解决了低温生长p型氮化镓带来的漏电流大,及预通镁源带来的前置电压高的问题. 关键词： 粗化 氮化镓 p型氮化镓 发光二极管     

鞘场加速机理中质子束的特性与其初始尺寸的关系

为了研究激光鞘场中质子层的尺寸对质子束特性的影响,本文应用中国工程物理研究院 激光聚变研究中心的二维Particle-In-Cell (2D-PIC)数值模拟程序Flips2D进行了相关数值模拟研究. 研究了质子束总能量随时间的变化,得出了加速持续过程与激光脉冲持续时间的关系; 研究了质子层的宽度对加速后质子束发散角和能谱的影响;研究了质子层的厚与加速后质子束 发散角和能谱的关系;得出了质子层的初始尺寸对加速后质子特性的影响规律.     

一类具幂零奇点的五次系统中心条件及极限环分支

In this paper, center conditions and bifurcation of limit cycles at the nilpotent critical point in a class of quintic polynomial differential system are investigated. With the help of computer algebra system MATHEMATICA, the first 8 quasi Lyapunov constants are deduced. As a result, the necessary and sufficient conditions to have a center are obtained. The fact that there exist 8 small amplitude limit cycles created from the three-order nilpotent critical point is also proved. Henceforth we give a lower bound of cyclicity of three-order nilpotent critical point for quintic Lyapunov systems.     

铁磁薄膜中圆偏振光感应的瞬态磁光Kerr峰的物理起源

使用飞秒时间分辨抽运-探测磁光Kerr光谱技术,实验研究了圆偏振光抽运面内磁化FePt和垂直磁化GdFeCo薄膜的磁化演化动力学,发现在时间延迟零点处均出现瞬态Kerr峰.分析了此Kerr峰的起源,指出此瞬态Kerr峰与铁磁性无关,可能起源于自由电子的顺磁磁化,而顺磁磁化的外磁场来自圆偏振抽运光的逆Faraday效应.基于顺磁磁化模型的计算结果支持此观点.基于此观点,逆Faraday效应感应的磁场脉冲宽度应该与激光脉冲宽度一致.     

有机化合物结构与性能的关系——激发能的同系线性规律

有机化合物的光谱及激发能存在着良好的同系线性规律。前文曾用HMO法对多联苯体系的同系线性规律进行了讨论,说明了对联多苯的共轭作用比间联多苯强,而后者共轭作用很弱,这可从光谱得到证实。近来,徐光宪等探讨了同系线性规律的量子化学基础,根据多烯中键长交替现象提出了MHMO法。     

Synthesis and biological evaluation of novel thalidomide analogues as potential anticancer drugs

In search of novel anticancer agents, a series of thalidomide analogs （6a-j） were designed and synthesized. Cytotoxicity of these compounds against human hepatoma cells （HepG2） was evaluated by MTT method. Compounds 6d, 6h and 6i showed significant cytotoxic activities comparable to or stronger than control 5-fluorouracil.     

PROPERTIES OF THERMO-MOLDED GLUTEN/GLYCEROL/SILICA COMPOSITES

Environmentally friendly thermosetting composites were successfully prepared by conventional blending wheat gluten as matrix,glycerol as plasticizer and silica as filler followed by thermo-molding of the mixture at 120℃.The strong interfacial interaction between silica particles and gluten proteins leaded to an increase in storage modulus and a decrease in loss factor as revealed by dynamic mechanical analysis.The moisture absorption and elongation at break decrease while Young's modulus and tensile stre...     

Fluorenyl-containing sulfonated poly(aryl ether ether ketone ketone)s (SPFEEKK) for fuel cell applications

A series of fluorenyl-containing sulfonated poly(aryl ether ether ketone ketone)s (SPFEEKK) were synthesized via aromatic nucleophilic substitution polymerization. The sulfonation content (SC) was controlled by the feed ratios of sulfonated and nonsulfonated monomers. Flexible and strong membranes in the sulfonic acid form were obtained from cast membranes in the sodium salt forms by treatment with acid. The thermal properties, water uptake, swelling ratio, water state, oxidative stability, proton conductivity and methanol permeability were investigated. All the polymers had proton conductivities greater than 1 × 10⁻² S/cm at room temperature, and the conductivity values of m-SPFEEKK-80 and p-SPFEEKK-80 were up to 1.86 × 10⁻¹ and 1.78 × 10⁻¹ S/cm at 100 °C. This series of polymers also possessed good dimensional stability in water and low methanol crossover.     

Selective Determination of Trace Mercury (II) after Preconcentration with 4-(2-Pyridylazo)-Resorcinol-Modified Nanometer-Sized SiO2 Particles from Sample Solutions

A rapid, selective method that utilize 4-(2-Pyridylazo)-resorcinol (PAR)-modified nanometer SiO₂ (nanometer SiO₂–PAR) as a new solid-phase extractant for preconcentration of trace mercury (II) has been developed. The adsorption property of nanometer SiO₂–PAR for metal ions was studied by selectively extracting different metal ions from aqueous solutions. The results revealed an excellent affinity of the nanometer SiO₂–PAR for mercury (II) in presence of interfering metal ions at pH 4. The main parameters of solid-phase extraction such as shaking time, elution and sample dilution effect were studied. The extractant shows rapid kinetic sorption, and the adsorption equilibrium of mercury (II) on nanometer SiO₂–PAR was achieved in less than 2 min. The adsorbed mercury (II) was easily eluted by 4 mL of 6 mol L⁻¹ HCl. The maximum preconcentration factor was 50. The maximum static adsorption capacity was 276 μmol g⁻¹ at pH 4. The detection limit (3σ) was 0.43 μg L⁻¹ for cold vapor atomic absorption spectrometry (CVAAS), and the relative standard deviation of the eight replicate determinations was 2.4% for the determination of 2.0 μg of Hg(II) in 100 mL water sample. The method was applied to the determination of trace mercury (II) in sample solutions with satisfactory results.