微波消解ICP-AES法测定鸡肌肉无机元素

采用微波密闭消解电感耦合等离子发射光谱法(ICP-AES)对鸡肌肉中K,Ca,Na,Mg,P,S,Fe,Cu,Mn和Zn等12种无机元素含量进行了测定。采用HNO₃-H₂O₂混合酸溶体系对待测样品进行消解。结果表明该方法的相对标准偏差均在5%以下;通过添加标准回收实验,回收率在92.5%～110%。与传统方法相比,该方法具有良好的准确度和精密度,高度灵敏性,能同时测定多种元素等优点,可满足样品检测要求,可为鸡肌肉无机元素快速检测提供科学依据。     

Multiple Entropy Measures for Multi-particle Pure Quantum State

We propose to use a set of averaged entropies, the multiple entropymeasures (MEMS), to partially quantify quantum entanglement ofmultipartite quantum state. The MEMS is vector-like with m=[N/2]components: [S₁, S₂,..., S_m], and the $i$-th component S_i is the geometric mean of i-qubits partial entropy of the system. The S_i measures how strong an arbitrary i qubits from the system are correlated with the rest of the system. It satisfies the conditions for a good entanglement measure. We have analyzed the entanglement properties of the GHZ-state, the W-states, and cluster-states under MEMS.     

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利用静电探针阵列对HL-2A边缘等离子体径向和极向速度进行了测量,获得了最后闭合磁面附近湍流的雷诺协强〈(v)r(v)θ〉以及(v)r和(v)θ间相位差的剖面.实验表明,虽然(v)r、(v)θ的幅值对雷诺协强的大小会有影响,但雷诺协强的变化趋势主要取决于二者相位差的变化;另一方面,欧姆放电以及不同电子回旋加热功率L模放电条件下的实验结果显示,密度扰动引起的粒子输运所带来的极向动量输运的贡献与雷诺协强项对极向动量输运的贡献是可比的.这表明在分析湍流引起的动量输运时必须考虑粒子输运的贡献.     

湍流雷诺协强及密度扰动对极向动量输运影响的实验研究

利用静电探针阵列对HL-2A边缘等离子体径向和极向速度进行了测量,获得了最后闭合磁面附近湍流的雷诺协强 以及 和 间相位差的剖面。实验表明,虽然 、 的幅值对雷诺协强的大小会有影响,但雷诺协强的变化趋势主要取决于二者相位差的变化;另一方面,欧姆放电以及不同电子回旋加热功率L模放电条件下的实验结果显示,密度扰动引起的粒子输运所带来的极向动量输运的贡献与雷诺协强项对极向动量输运的贡献是可比的。这表明在分析湍流引起的动量输运时必须考虑粒子输运的贡献。     

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在建的HL-2M装置的环向场线圈采用了比特板式结构,介绍了采用封闭多边形电流丝模型计算分析HL-2M装置环向场线圈电磁场和纹波情况;环向场线圈电流与环向场引起的电磁力以及与极向场产生的倾覆力也做了计算.计算结果对环向场线圈的设计具有一定的参考意义.     

发动机叶片扭转和弯曲变形同步测量新方法

扭转和弯曲变形测量可以确定叶片弯扭变形耦合的特征,为叶片弯扭耦合分析提供可用的试验手段。本文提出了一种发动机叶片扭转和弯曲变形同步测量的新方法,其中,扭转角度测量方法能更加灵活地应用于测量叶片类形状不规则构件的扭转变形,而弯曲变形测量方法解决了叶片变形方向未知且存在弯扭耦合时的叶片变形测量问题,从而可实现对叶片截面扭转和弯曲变形的同步测量。对上述测量方法进行了专门的验证试验,结果表明:与传统方法测量结果相比,扭转角度测量偏差小于1%,挠度测量偏差小于2%,满足工程测量精度要求。     

完全图$K_{2m}$书本表示的唯一性

In the present paper we discuss some properties of book presentation of spatial graphs, and prove that the book presentation of minimum sheets of a complete graph K2m with even vertices is unique up to sheet translation and ambient isotopy. We also show this is true for K7.     

双锰卟啉应用于钼酸根电位传感器的研究

以[MnT(p-CH3)PP]2O为活性物质、以o-NPOE为增塑剂PVC膜制成的新型高效电位型传感器来测定MoO42-离子浓度。该电极具有线性能斯特斜率为30.5的响应特征,其工作浓度范围为2.1×10-6~1.0×10-1mol/L,pH范围为5.0~12.5,响应时间不超过15 s,对常见干扰离子有较高的选择性,并被应用于实际样品中MoO42-含量的测定。     

Synthesis,Crystal Structure and Antimicrobial Activity of a New Ternary Copper(Ⅱ) Complex with p-Chlorophenoxyacetic Acid and 2-Amino Benzothiazole

A novel ternary complex of Cu(pcpa)2(aben)2 (pcpa=p-chlorophenoxyacetic acid anion,aben=2-amino benzothiazole) was synthesized by the reaction of copper acetate,2-amino benzothiazole and p-chlorophenoxyacetic acid.Elemental analysis,IR,UV and X-ray single-crystal diffraction were carried out to determine the composition and crystal structure.The crystal crystalli-zes in the monoclinic system,space group C2/c with a=25.795(4),b=7.384(3),c =17.741(6),β=107.47(2)°,C30H24Cl2CuN4O6S2,Mr=735.09,V=3223.2(18) 3,Z=4,Dc=1.515 Mg/m3,λ(MoKα)=0.71073 ,μ=1.022 mm-1,F(000)=1500,the final R=0.0464 and wR=0.1244.A total of 3218 unique reflections were collected,of which 2228 with I 2σ(I) were observed.The Cu(II) atom is four-coordinated with two carboxylate oxygen atoms of the two pcpa ligands and two nitrogen atoms in thiazole rings of two aben ligands.The analysis of crystal structure shows intermolecular and intramolecular hydrogen bonds between amino-nitrogen atoms of the two aben ligands and carboxylate oxygen atoms of the two pcpa ligands.The antimicrobial properties of the title complex and its two free ligands were tested against representative bacterial and fungal strains.Results show that the antibacterial activity of the complex is less than or equal to that of 2-amino benzothiazole,but for yeasts and moulds,it exhibits excellent inhibitory effect better than that of its two free ligands.     

Ti-Hf合金的结构和吸氘热力学性质

采用磁悬浮法制备了4种TiHfx,(x=0.13,0.26,0.52,1.03)二元合金。利用X射线衍射技术对纯钛、纯铪和4种成分Ti-Hf二元合金吸氘前后的物相结构、晶胞参数和吸氘特性进行了研究。Ti-Hf合金吸氘前均为六方密堆结构,饱和吸氘后形成较单一的面心四方ε相氘化物。随Hf含量增加,Ti-Hf合金及其ε相氘化物的晶胞参数均呈增大趋势。压强-组成等温线显示,Hf含量增加将导致氘化物室温平衡压升高,Ti-Hf合金热力学性质趋近于H-Hf体系,Hf对Ti-Hf合金氘化物热力学性质起主导作用。Hf掺杂显著降低了Ti吸氘的体膨胀,从而有望缓解由于体胀导致的氢脆现象。