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941.
Benzildithiosemicarbazone (BDTSC) is proposed as a sensitive and selective analytical reagent for the extractive spectrophotometric determination of copper(II). BDTSC reacts with copper(II) in the pH range 1.0-7.0 to form a yellowish complex. Beer's law is obeyed in the concentration range 0.5-0.4 microg cm(-3). The yellowish Cu(II)-BDTSC complex in chloroform shows a maximum absorbance at 380 nm, with molar absorptivity and Sandell's sensitivity values of 1.63 x 10(4) dm3 mol(-1) cm(-1) and 0.00389 microg cm(-2), respectively. A repetition of the method is checked by finding the relative standard deviation (RSD) (n = 10), which is 0.6%. The composition of the Cu(II)-BDTSC complex is established as 1:1 by slope analysis, molar ratio and Asmus' methods. An excellent linearity with a correlation coefficient value of 0.98 is obtained for the Cu(II)-BDTSC complex. The instability constant of the complex calculated from Edmond and Birnbaum's method is 7.70 x 10(-4) and that of Asmus' method is 7.66 x 10(-4), at room temperature. The method is successfully employed for the determination copper(II) in pharmaceutical and environmental samples. The reliability of the method is assured by analyzing the standard alloys (BCS 5g, 10g, 19e, 78, 32a, 207 and 179) and by inter-comparison of experimental values, using an atomic absorption spectrometer. 相似文献
942.
S. B. Gashkov 《Moscow University Mathematics Bulletin》2007,62(3):87-89
It is shown that Lozhkin’s method (1981) for minimization of the depth of formulas with a bounded number of changing types of elements in paths from input to output and Hoover-Klawe-Pippenger’s method (technical report in 1981, journal publication in 1984) for minimization of the depth of circuits with unbounded branching by insertion of trees from buffers with bounded branching of outputs for each buffer are dual to each other and can be proved by one and the same method. 相似文献
943.
944.
945.
Changes in the magnetically sensitive properties of multilayer semiconductors devices, such as planar diffusion triacs, that are related to atomic-displacement-induced defects and ionization by irradiation are considered. It is shown that irradiation may significantly raise the magnetic sensitivity of the triacs. Processes and underlying mechanisms responsible for the improvement of the magnetic sensitivity under the action of a number of galvanomagnetic effects are studied. 相似文献
946.
F. Klappenberger K. N. Alekseev K. F. Renk R. Scheuerer E. Schomburg S. J. Allen G. R. Ramian J. S. S. Scott A. Kovsh V. Ustinov A. Zhukov 《The European Physical Journal B - Condensed Matter and Complex Systems》2004,39(4):483-489
We report an experimental study indicating ultrafast creation and annihilation of space-charge domains in a semiconductor superlattice under the action of a THz field. Our experiment was performed for an InGaAs/InAlAs superlattice with the conduction electrons undergoing miniband transport. We applied to a superlattice a dc bias that was slightly smaller than a critical bias necessary for the formation of space-charge domains caused by a static negative differential conductivity. Additionally subjecting the superlattice to a strong THz field, resulted in a dc transport governed by the formation of domains if the frequency of the field was smaller than an upper frequency limit (~3 THz). From this frequency limit for the creation and annihilation of domains we determined the characteristic time of the domain buildup. Our analysis shows that the buildup time of domains in a wide miniband and heavily doped superlattice is limited by the relaxation time due to scattering of the miniband electrons at polar optic phonons. Our results are of importance for both an understanding of ultrafast dynamics of pattern formation in nanostructures and the development of THz electronic devices.Received: 25 March 2004, Published online: 23 July 2004PACS:
72.20.Ht High-field and nonlinear effects - 72.30. + q High-frequency effects; plasma effects - 73.21.Cd SuperlatticesK.N. Alekseev: Permanent address: Department of Physical Sciences, P.O. Box 3000, University of Oulu FIN-90014, Finland. 相似文献
947.
An experimental apparatus and related procedures for the determination of the effective thermal conductivity of sintered powder-metal
plates saturated with distilled water at temperatures in the range 20–150°C are discussed. The apparatus and procedures are
applied to two samples of sintered powder-metal plates, one made of nickel 200 and the other of stainless steel 316, with
porosities of 28.10 and 46.45%, respectively, and each of nominal dimensions 127 mm × 127 mm × 6.35 mm. The experimental
results are compared with corresponding predictions yielded by several correlations available in the literature. The correlations
based on experimental data for packed beds of spherical particles and also porous plates made of cold-pressed (but not sintered)
particles of angular shapes do not apply well to sintered powder-metal plates. A new correlation, which is based on extensions
of ideas contained in earlier works and provides improved predictions, is proposed. 相似文献
948.
Hyperfine structure of a hydrogen-like atom due to orbit-orbit,spin-orbit,and spin-spin interactions
A nonrelativistic model of a hydrogen-like atom is considered. This model is used to calculate corrections to the energy spectrum of the atom. The analysis is based on a Hamiltonian that includes the intratomic fields generated by the electron and the nucleus. 相似文献
949.
950.
Within the framework of free interaction theory numerical methods are used to investigate the occurrence of supersonic zones with shocks in the outer inviscid region for flow past roughness in the lower viscous sublayer, with and without the formation of local separation zones. 相似文献