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771.
Dr. Daichi Kato Dr. Peng Song Dr. Hiroki Ubukata Haruki Taguro Dr. Cédric Tassel Dr. Kohei Miyazaki Prof. Takeshi Abe Dr. Kousuke Nakano Prof. Kenta Hongo Prof. Ryo Maezono Prof. Hiroshi Kageyama 《Angewandte Chemie (International ed. in English)》2023,62(30):e202301416
Mixed-anion compounds have attracted growing attentions, but their synthesis is challenging, making a rational search desirable. Here, we explored LaF3-LaX3 (X=Cl, Br, I) system using ab initio structure searches based on evolutionary algorithms, and predicted LaF2X and LaFX2 (X=Br, I), which are respectively isostructural with LaHBr2 and YH2I, consisting of layered La-F blocks with single and double ordered honeycomb lattices, separated by van der Waals gaps. We successfully synthesized these compounds: LaF2Br and LaFI2 crystallize in the predicted structure, while LaF2I is similar to the predicted one but with different layer stacking. LaF2I exhibits fluoride ion conductivity comparable to that of non-doped LaF3, and has the potential to show better ionic conductivity upon appropriate doping, given the theoretically lower diffusion energy barrier and the presence of soft iodine anions. This study shows the structure prediction using evolutionary algorithms will accelerate the discovery of mixed-anion compounds in future, in particular those with an ordered anion arrangement. 相似文献
772.
S.S. Miyazaki A.R. Yep F. Kolton É.B. Hermida F. Povolo E.G. Fernandes E. Chiellini 《Macromolecular Symposia》2003,197(1):57-64
Two samples of microbial poly(3-hydroxybutyrate) (PHB) having different molecular weight were used for the preparation of films to be exposed to gamma radiation. The effect of radiation on those samples with high molecular weight increased the fragility of the film. Biodegradability increased with time and reached about 95% after 18 days. Weight-loss of both samples (irradiated and non-irradiated) after 23 days were 100%, for those films with molecular weight of 265 kD. 相似文献
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Crystallization process of molten Ba(B0.9Al0.1)2O4 from supercooled pendant drop was investigated on a viewpoint of a supercooling and a solid phase formation. Molten pendant drop was crystallized by a rod touching at an crystallization temperature under an adequate degree of supercooling. Three kinds of rods were used. Each rod was made of Pt, hBN and graphite which had different wettability to the molten drop. There were three kinds of phases on a solid Ba(B0.9Al0.1)2O4, such as a high temperature crystal phase, a low temperature crystal phase and a glass phase. All phases could be formed by the present method. 相似文献